skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Ultrasonic Characterization of Texture in Rolled Aluminium Correlated with Electron Backscatter Diffraction Measurements

Abstract

Electron Backscatter Diffraction (EBSD) is a microscopic technique that provides detailed crystallographic orientation and microstructural information, allowing for accurate measurement of such properties like average grain size. In order to validate and better understand what information an ultrasonic technique can give us we are correlating the ultrasonic measurements with those from EBSD. It generates an appreciation of the limitations of both techniques, and what each can reasonably deliver. We describe a technique to extrapolate the three independent orientation distribution coefficients (ODCs) for cubic structures W400, W420 and W440 from the Bunge-Euler angle data from EBSD scans. Preliminary EBSD results for thin rolled aluminium sheet are discussed and compared to the ODCs determined on the same sample using an ultrasonic EMAT-EMAT S0 Lamb wave measurement system.

Authors:
; ;  [1]
  1. University of Warwick, Dept. of Physics, Coventry. CV4 7AL (United Kingdom)
Publication Date:
OSTI Identifier:
21054937
Resource Type:
Journal Article
Resource Relation:
Journal Name: AIP Conference Proceedings; Journal Volume: 894; Journal Issue: 1; Conference: Conference on review of progress in quantitative nondestructive evaluation, Portland, OR (United States), 30 Jul - 4 Aug 2006; Other Information: DOI: 10.1063/1.2718107; (c) 2007 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; ALUMINIUM; ALUMINIUM ALLOYS; BACKSCATTERING; CRYSTAL LATTICES; CRYSTALLOGRAPHY; DISTRIBUTION; ELECTRON DIFFRACTION; ELECTRONS; GRAIN SIZE; ORIENTATION; SURFACES; TEXTURE; ULTRASONIC TESTING

Citation Formats

Essex, S. D., Potter, M. D. G., and Dixon, S.. Ultrasonic Characterization of Texture in Rolled Aluminium Correlated with Electron Backscatter Diffraction Measurements. United States: N. p., 2007. Web. doi:10.1063/1.2718107.
Essex, S. D., Potter, M. D. G., & Dixon, S.. Ultrasonic Characterization of Texture in Rolled Aluminium Correlated with Electron Backscatter Diffraction Measurements. United States. doi:10.1063/1.2718107.
Essex, S. D., Potter, M. D. G., and Dixon, S.. Wed . "Ultrasonic Characterization of Texture in Rolled Aluminium Correlated with Electron Backscatter Diffraction Measurements". United States. doi:10.1063/1.2718107.
@article{osti_21054937,
title = {Ultrasonic Characterization of Texture in Rolled Aluminium Correlated with Electron Backscatter Diffraction Measurements},
author = {Essex, S. D. and Potter, M. D. G. and Dixon, S.},
abstractNote = {Electron Backscatter Diffraction (EBSD) is a microscopic technique that provides detailed crystallographic orientation and microstructural information, allowing for accurate measurement of such properties like average grain size. In order to validate and better understand what information an ultrasonic technique can give us we are correlating the ultrasonic measurements with those from EBSD. It generates an appreciation of the limitations of both techniques, and what each can reasonably deliver. We describe a technique to extrapolate the three independent orientation distribution coefficients (ODCs) for cubic structures W400, W420 and W440 from the Bunge-Euler angle data from EBSD scans. Preliminary EBSD results for thin rolled aluminium sheet are discussed and compared to the ODCs determined on the same sample using an ultrasonic EMAT-EMAT S0 Lamb wave measurement system.},
doi = {10.1063/1.2718107},
journal = {AIP Conference Proceedings},
number = 1,
volume = 894,
place = {United States},
year = {Wed Mar 21 00:00:00 EDT 2007},
month = {Wed Mar 21 00:00:00 EDT 2007}
}
  • The texture (preferred grain orientation) of metal sheet plays a central role in determining the material's response to subsequent deformation. Recent advances in inferring forming characteristics from ultrasonic velocity measurements are reviewed. After a brief discussion of the underlying physical principles, progress towards the prediction of the normal anisotropy of steel sheet, a parameter that is important in determining the ability of the sheet to be deeply drawn into a variety of shapes such as those used in automobile door panels, is reviewed. Less well developed applications such as the prediction of the earing behavior of aluminum sheet and ofmore » the Kearns texture parameters of hexagonal metal sheet and tubing are then summarized. The paper concludes with a discussion of possible directions of future research.« less
  • The evolution of microstructure and texture during cross-rolling and annealing was investigated by electron backscatter diffraction in a ferritic–austenitic duplex stainless steel. For this purpose an alloy with nearly equal volume fraction of the two phases was deformed by multi-pass cross-rolling process up to 90% reduction in thickness. The rolling and transverse directions were mutually interchanged in each pass by rotating the sample by 90° around the normal direction. In order to avoid deformation induced phase transformation and dynamic strain aging, the rolling was carried out at an optimized temperature of 898 K (625 °C) at the warm-deformation range. Themore » microstructure after cross warm-rolling revealed a lamellar structure with alternate arrangement of the bands of two phases. Strong brass and rotated brass components were observed in austenite in the steel after processing by cross warm-rolling. The ferrite in the cross warm-rolling processed steel showed remarkably strong RD-fiber (RD//< 011 >) component (001)< 011 >. The development of texture in the two phases after processing by cross warm-rolling could be explained by the stability of the texture components. During isothermal annealing of the 90% cross warm-rolling processed material the lamellar morphology was retained before collapse of the lamellar structure to the mutual interpenetration of the phase bands. Ferrite showed recovery resulting in annealing texture similar to the deformation texture. In contrast, the austenite showed primary recrystallization without preferential orientation selection leading to the retention of deformation texture. The evolution of deformation and annealing texture in the two phases of the steel was independent of one another. - Highlights: • Effect of cross warm-rolling on texture formation is studied in duplex steel. • Brass texture in austenite and (001)<110 > in ferrite are developed. • Ferrite shows recovery during annealing retaining the (001)<110 > component. • Austenite shows recrystallization during annealing retaining the deformation texture. • The deformation of recrystallization of two phases is independent of one other.« less
  • The relationships between the martensitic phase transformation kinetics, texture evolution, and the microstructure development in the parent austenite phase were studied for a 304L stainless steel that exhibits the transformation-induced plasticity effect under biaxial loading conditions at ambient temperature. The applied loading paths included: pure torsion, simultaneous biaxial torsion/tension, simultaneous biaxial torsion/compression, and stepwise loading of tension followed by torsion (i.e., first loading by uniaxial tension and then by pure torsion in sequence). Synchrotron X-ray and electron backscatter diffraction techniques were used to measure the evolution of the phase fractions, textures, and microstructures as a function of the applied strains.more » The influence of loading character and path on the changes in martensitic phase transformation kinetics is discussed in the context of (1) texture-transformation relationship and the preferred transformation of grains belonging to certain texture components over the others, (2) effects of axial strains on shear band evolutions, and (3) volume changes associated with martensitic transformation.« less
  • Here we report that the relationships between the martensitic phase transformation kinetics, texture evolution, and the microstructure development in the parent austenite phase were studied for a 304L stainless steel that exhibits the transformation-induced plasticity effect under biaxial loading conditions at ambient temperature. The applied loading paths included: pure torsion, simultaneous biaxial torsion/tension, simultaneous biaxial torsion/compression, and stepwise loading of tension followed by torsion (i.e., first loading by uniaxial tension and then by pure torsion in sequence). Synchrotron X-ray and electron backscatter diffraction techniques were used to measure the evolution of the phase fractions, textures, and microstructures as a functionmore » of the applied strains. The influence of loading character and path on the changes in martensitic phase transformation kinetics is discussed in the context of (1) texture-transformation relationship and the preferred transformation of grains belonging to certain texture components over the others, (2) effects of axial strains on shear band evolutions, and (3) volume changes associated with martensitic transformation.« less
  • Abstract not provided.