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Title: Johann Spectrometer for High Resolution X-ray Spectroscopy

Abstract

A newly designed vacuum Johann spectrometer with a large focusing analyzer crystal for inelastic x-ray scattering and high resolution fluorescence spectroscopy has been installed at the DORIS III storage ring. Spherically bent crystals with a maximum diameter of 125 mm, and cylindrically bent crystals are employed as dispersive optical elements. Standard radius of curvature of the crystals is 1000 mm, however, the design of the mechanical components also facilitates measurements with smaller and larger bending radii. Up to four crystals are mounted on a revolving crystal changer which enables crystal changes without breaking the vacuum. The spectrometer works at fixed Bragg angle. It is preferably designed for the measurements in non-scanning mode with a broad beam spot, and offers a large flexibility to set the sample to the optimum position inside the Rowland circle. A deep depletion CCD camera is employed as a position sensitive detector to collect the energy-analyzed photons on the circumference of the Rowland circle. The vacuum in the spectrometer tank is typically 10-6 mbar. The sample chamber is separated from the tank either by 25 {mu}m thick Kapton windows, which allows samples to be measured under ambient conditions, or by two gate valves. The spectrometer ismore » currently installed at wiggler beamline W1 whose working range is 4-10.5 keV with typical flux at the sample of 5x1010photons/s/mm2. The capabilities of the spectrometer are illustrated by resonant inelastic experiments on 3d transition metals and rare earth compounds, and by chemical shift measurements on chromium compounds.« less

Authors:
;  [1]; ; ;  [2];  [3]
  1. Institut fuer Anorganische und Analytische Chemie, Justus-Liebig-Universitaet Giessen, Heinrich-Buff-Ring 58, 35392 Giessen (Germany)
  2. Hamburger Synchrotron Strahlungslabor (HASYLAB) am Deutsches Elektronen Synchrotron (DESY), Notkestrasse 85, 22607 Hamburg (Germany)
  3. Martin-Luther-Universitaet Halle-Wittenberg, Fachbereich Physik, Friedemann-Bach-Platz, 06108 Halle(Saale) (Germany)
Publication Date:
OSTI Identifier:
21049347
Resource Type:
Journal Article
Resource Relation:
Journal Name: AIP Conference Proceedings; Journal Volume: 879; Journal Issue: 1; Conference: 9. international conference on synchrotron radiation instrumentation, Daegu (Korea, Republic of), 28 May - 2 Jun 2006; Other Information: DOI: 10.1063/1.2436408; (c) 2007 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; BRAGG REFLECTION; CHARGE-COUPLED DEVICES; CHEMICAL SHIFT; CHROMIUM COMPOUNDS; CRYSTALS; FLUORESCENCE SPECTROSCOPY; KEV RANGE; POSITION SENSITIVE DETECTORS; RARE EARTH COMPOUNDS; RESOLUTION; STORAGE RINGS; TRANSITION ELEMENTS; X-RAY DIFFRACTION; X-RAY FLUORESCENCE ANALYSIS; X-RAY SPECTROSCOPY

Citation Formats

Machek, Pavel, Froeba, Michael, Welter, Edmund, Caliebe, Wolfgang, Brueggmann, Ulf, and Draeger, Guenter. Johann Spectrometer for High Resolution X-ray Spectroscopy. United States: N. p., 2007. Web. doi:10.1063/1.2436408.
Machek, Pavel, Froeba, Michael, Welter, Edmund, Caliebe, Wolfgang, Brueggmann, Ulf, & Draeger, Guenter. Johann Spectrometer for High Resolution X-ray Spectroscopy. United States. doi:10.1063/1.2436408.
Machek, Pavel, Froeba, Michael, Welter, Edmund, Caliebe, Wolfgang, Brueggmann, Ulf, and Draeger, Guenter. Fri . "Johann Spectrometer for High Resolution X-ray Spectroscopy". United States. doi:10.1063/1.2436408.
@article{osti_21049347,
title = {Johann Spectrometer for High Resolution X-ray Spectroscopy},
author = {Machek, Pavel and Froeba, Michael and Welter, Edmund and Caliebe, Wolfgang and Brueggmann, Ulf and Draeger, Guenter},
abstractNote = {A newly designed vacuum Johann spectrometer with a large focusing analyzer crystal for inelastic x-ray scattering and high resolution fluorescence spectroscopy has been installed at the DORIS III storage ring. Spherically bent crystals with a maximum diameter of 125 mm, and cylindrically bent crystals are employed as dispersive optical elements. Standard radius of curvature of the crystals is 1000 mm, however, the design of the mechanical components also facilitates measurements with smaller and larger bending radii. Up to four crystals are mounted on a revolving crystal changer which enables crystal changes without breaking the vacuum. The spectrometer works at fixed Bragg angle. It is preferably designed for the measurements in non-scanning mode with a broad beam spot, and offers a large flexibility to set the sample to the optimum position inside the Rowland circle. A deep depletion CCD camera is employed as a position sensitive detector to collect the energy-analyzed photons on the circumference of the Rowland circle. The vacuum in the spectrometer tank is typically 10-6 mbar. The sample chamber is separated from the tank either by 25 {mu}m thick Kapton windows, which allows samples to be measured under ambient conditions, or by two gate valves. The spectrometer is currently installed at wiggler beamline W1 whose working range is 4-10.5 keV with typical flux at the sample of 5x1010photons/s/mm2. The capabilities of the spectrometer are illustrated by resonant inelastic experiments on 3d transition metals and rare earth compounds, and by chemical shift measurements on chromium compounds.},
doi = {10.1063/1.2436408},
journal = {AIP Conference Proceedings},
number = 1,
volume = 879,
place = {United States},
year = {Fri Jan 19 00:00:00 EST 2007},
month = {Fri Jan 19 00:00:00 EST 2007}
}