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Title: High-temperature stability of epitaxial, non-isostructural Mo/NbN superlattices

Journal Article · · Journal of Materials Research
DOI:https://doi.org/10.1557/JMR.2000.0082· OSTI ID:20216020
 [1];  [2];  [3];  [4];  [3];  [2]
  1. Advanced Coating Technology Group and Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois, and Physics Department, Linkoeping University, (Sweden)
  2. Advanced Coating Technology Group and Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois (United States)
  3. Physics Department, Linkoeping University, (Sweden)
  4. Los Alamos National Laboratory, Los Alamos, New Mexico (United States)

The effect of 1000 degree sign C vacuum annealing on the structure and hardness of epitaxial Mo/NbN superlattice thin films was studied. The intensity of superlattice satellite peaks, measured by x-ray diffraction, decreased during annealing while new peaks corresponding to a MoNbN ternary phase appeared. The results are consistent with the Mo-Nb-N phase diagram, which shows no mutual solubility between Mo, NbN, and MoNbN. Even after 3-h anneals and a loss of most of the superlattice peak intensity, the room-temperature hardness was the same as for as-deposited superlattices. The retained hardness suggests that a residual nanocomposite structure is retained even after the formation of the ternary structure. (c) 2000 Materials Research Society.

OSTI ID:
20216020
Journal Information:
Journal of Materials Research, Vol. 15, Issue 2; Other Information: PBD: Feb 2000; ISSN 0884-2914
Country of Publication:
United States
Language:
English

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