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Operando Methods in Electrocatalysis

Journal Article · · ACS Catalysis
 [1];  [1];  [1];  [1];  [1];  [2];  [1];  [1];  [1];  [2];  [3];  [1]
  1. Department of Chemistry and Chemical Biology, Cornell University, Ithaca, New York 14853, United States
  2. School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853, United States; Cornell High Energy Synchrotron Source (CHESS), Cornell University, Ithaca, New York 14853, United States
  3. School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853, United States; Kavli Institute at Cornell for Nanoscale Science, Ithaca, New York 14853, United States

Not provided.

Research Organization:
Cornell Univ., Ithaca, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC)
DOE Contract Number:
SC0019445
OSTI ID:
1853280
Journal Information:
ACS Catalysis, Vol. 11, Issue 3; ISSN 2155-5435
Publisher:
American Chemical Society (ACS)
Country of Publication:
United States
Language:
English

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Study of the electrocatalytic influence of Pt/Ru and Ru on the oxidation of residues of small organic molecules journal December 1994
Composition and activity of high surface area PtRu catalysts towards adsorbed CO and methanol electrooxidation— journal August 2002
Nanoparticle Size Effects on Methanol Electrochemical Oxidation on Carbon Supported Platinum Catalysts journal October 2006
Influence of Anion Adsorption on the Parallel Reaction Pathways in the Oscillatory Electro-oxidation of Methanol journal July 2013
Transport Effects in the Electrooxidation of Methanol Studied on Nanostructured Pt/Glassy Carbon Electrodes journal March 2010
Effect of mass transfer and solution composition on the quantification of reaction kinetics by differential electrochemical mass spectrometry journal May 2021
The effect of alcohol concentration on the mass signal of CO2 detected by differential mass spectrometry journal November 2014
The Influence of Reactive Side Products in Electrocatalytic Reactions: Methanol Oxidation as Case Study journal August 2013
Pt-Rich core /Sn-Rich subsurface /Pt skin Nanocubes As Highly Active and Stable Electrocatalysts for the Ethanol Oxidation Reaction journal February 2018
Elementary steps of ethanol oxidation on Pt in sulfuric acid as evidenced by isotope labelling journal October 1985
A dems and FTir spectroscopic investigation of adsorbed ethanol on polycrystalline platinum journal March 1994
The influence of the surface structure on the adsorption of ethene, ethanol and cyclohexene as studied by DEMS journal January 1995
Electrooxidation of ethanol at polycrystalline and platinum stepped single crystals: A study by differential electrochemical mass spectrometry journal November 2010
Quantitative DEMS study of ethanol oxidation: effect of surface structure and Sn surface modification journal January 2012
Influence of H- and OH-adsorbates on the ethanol oxidation reaction – a DEMS study journal January 2015
Ethanol oxidation on shape-controlled platinum nanoparticles at different pHs: A combined in situ IR spectroscopy and online mass spectrometry study journal February 2016
The influence of mass-transport conditions on the ethanol oxidation reaction (EOR) mechanism of Pt/C electrocatalysts journal January 2016
Support materials for PEMFC and DMFC electrocatalysts—A review journal June 2012
Carbon Corrosion in Proton-Exchange Membrane Fuel Cells: Effect of the Carbon Structure, the Degradation Protocol, and the Gas Atmosphere journal March 2015
Analysis of oxygen sources and reaction pathways of carbon support corrosion at the cathode in PEMFC using oxygen-18 DEMS journal September 2010
Investigation of Pt catalytic effects on carbon support corrosion of the cathode catalyst in PEM fuel cells using DEMS spectra journal June 2009
Model study on the stability of carbon support materials under polymer electrolyte fuel cell cathode operation conditions journal May 2009
Online Monitoring of Electrochemical Carbon Corrosion in Alkaline Electrolytes by Differential Electrochemical Mass Spectrometry journal December 2019
DEMS and Online Mass Spectrometry Studies of the Carbon Support Corrosion under Various Polymer Electrolyte Membrane Fuel Cell Operating Conditions journal January 2018
On the Role of the Support in Pt Anode Catalyst Degradation under Simulated H 2 Fuel Starvation Conditions journal January 2018
A Mechanistic Differential Electrochemical Mass Spectrometry (DEMS) and in situ Fourier Transform Infrared Investigation of Dimethoxymethane Electro-Oxidation at Platinum journal June 2011
The kinetics of the oxidation and reduction of H2O2 at a Pt electrode: A differential electrochemical mass spectrometric study journal December 2016
Oxidation of the Partly Oxidized Ethylene Glycol Oxidation Products Glycolaldehyde, Glyoxal, Glycolic Acid, Glyoxylic Acid, and Oxalic Acid on Pt Electrodes: A Combined ATR-FTIRS and DEMS Spectroelectrochemical Study journal June 2013
Mechanistic studies on boron-doped diamond: Oxidation of small organic molecules journal November 2013
Structural principles to steer the selectivity of the electrocatalytic reduction of aliphatic ketones on platinum journal March 2019
Photoelectrochemical Properties of (In,Ga)N Nanowires for Water Splitting Investigated by in Situ Electrochemical Mass Spectroscopy journal May 2013
Probing Edge Site Reactivity of Oxidic Cobalt Water Oxidation Catalysts journal March 2016
How many surface atoms in Co 3 O 4 take part in oxygen evolution? Isotope labeling together with differential electrochemical mass spectrometry journal January 2017
Oxygen Evolution Reaction Dynamics, Faradaic Charge Efficiency, and the Active Metal Redox States of Ni–Fe Oxide Water Splitting Electrocatalysts journal April 2016
Water Oxidation Catalysis by Co(II) Impurities in Co(III) 4 O 4 Cubanes journal December 2014
Progress and Perspectives of Electrochemical CO 2 Reduction on Copper in Aqueous Electrolyte journal April 2019
Coupling of a scanning flow cell with online electrochemical mass spectrometry for screening of reaction selectivity journal October 2014
Direct Observation of the Local Reaction Environment during the Electrochemical Reduction of CO 2 journal April 2018
In Situ Porous Structure Characterization of Electrodes for Energy Storage and Conversion by EQCM-D: a Review journal April 2017
In Situ Real-Time Mechanical and Morphological Characterization of Electrodes for Electrochemical Energy Storage and Conversion by Electrochemical Quartz Crystal Microbalance with Dissipation Monitoring journal January 2018
The Quartz Microbalance: A Novel Approach to the In-Situ Investigation of Interfacial Phenomena at the Solid/Liquid Junction[New Analytical Methods(40)] journal April 1990
Measurement of interfacial processes at electrode surfaces with the electrochemical quartz crystal microbalance journal September 1992
Experimental aspects of use of the quartz crystal microbalance in solution journal October 1985
Calibration of the Electrochemical Quartz Crystal Microbalance journal September 1991
Dependence of the reliability of electrochemical quartz-crystal nanobalance mass responses on the calibration constant, Cf : analysis of three procedures for its determination journal May 2003
Vibrating Powders: Electrochemical Quartz Crystal Microbalance Study of IrO 2 and Pt/C Catalyst Layers for Voltage Reversal Tolerant Anodes in Fuel Cells journal September 2019
Simultaneous determination of both the calibration constant in an electrochemical quartz crystal microbalance and the active surface area of a polycrystalline gold electrode journal January 2000
EQCM Study of the Electrodeposition of Pt-WO 3 and Its Catalytic Activity towards the ORR journal October 2010
Electrodeposition of Pt - Rare Earth Alloys as ORR Catalysts for Fuel Cells journal August 2016
Electrochemical and spontaneous deposition of ruthenium at platinum electrodes for methanol oxidation: an electrochemical quartz crystal microbalance study journal August 2001
Preparation of a thin-film Pt electrocatalyst by MnO2 electrodeposition and galvanic replacement reaction for oxidation of methanol journal November 2019
Preparation of a Pt thin-film modified electrode for alkaline electrocatalytic oxidation of methanol by Cu(OH)2 electrodeposition and galvanic replacement reaction journal January 2020
Growth and Activation of an Amorphous Molybdenum Sulfide Hydrogen Evolving Catalyst journal August 2013
Catalytic characterization of hollow silver/palladium nanoparticles synthesized by a displacement reaction journal September 2009
Electrochemically Driven Cation Exchange Enables the Rational Design of Active CO 2 Reduction Electrocatalysts journal March 2020
Electrophoretic deposition improves catalytic performance of Co 3 O 4 nanoparticles for oxygen reduction/oxygen evolution reactions journal January 2015
Dissolution of noble metals and their alloys studied by electrochemical quartz crystal microbalance journal April 2006
EQCM Study on Dissolution of Ruthenium in Sulfuric Acid journal January 2008
Electrochemical quartz crystal microbalance analysis of CO-tolerance at PtFe alloy electrodes journal August 2002
Assessment of Platinum Dissolution from a Pt/C Fuel Cell Catalyst: An Electrochemical Quartz Crystal Microbalance Study journal January 2010
EQCM Investigation of Electrochemical Deposition and Stability of Co–Pi Oxygen Evolution Catalyst of Solar Energy Storage journal April 2013
Electrodeposited Co-Doped Fe3O4 Thin Films as Efficient Catalysts for the Oxygen Evolution Reaction journal August 2016
Long-term electrocatalytic N 2 fixation by MOF-derived Y-stabilized ZrO 2 : insight into the deactivation mechanism journal January 2020
Electrochemical quartz crystal microbalance measurements of CO adsorption and oxidation on Pt in various electrolytes journal January 1998
Electrochemical study on the adsorption of carbon oxides and oxidation of their adsorption products on platinum group metals and alloys journal January 2008
Analysis of the electrochemical quartz crystal microbalance response during oxidation of carbon oxides adsorption products on platinum group metals and alloys journal September 2009
Electrochemical quartz crystal microbalance analysis of the CO oxidation reaction at Pt alloy electrodes journal November 2011
Oxidation of glucose at electrodeposited platinum electrodes in alkaline solution journal January 1993
Chemisorption and oxidation of methanol at polycrystalline Pt in acid solutions journal February 1994
Measurement of the Ru Surface Content of Electrocodeposited PtRu Electrodes with the Electrochemical Quartz Crystal Microbalance:  Implications for Methanol and CO Electrooxidation journal January 1996
Electrochemical Quartz Crystal Microbalance Analysis of the Oxygen Reduction Reaction on Pt-Based Electrodes. Part 1: Effect of Adsorbed Anions on the Oxygen Reduction Activities of Pt in HF, HClO 4 , and H 2 SO 4 Solutions journal May 2011
Electrochemical Quartz Crystal Microbalance Analysis of the Oxygen Reduction Reaction on Pt-Based Electrodes. Part 2: Adsorption of Oxygen Species and ClO 4 Anions on Pt and Pt–Co Alloy in HClO 4 Solutions journal January 2014
Controlled electrodeposited cobalt phases for efficient OER catalysis, RRDE and eQCM studies journal August 2019
Dynamic Characterization of Inter- and Intralamellar Domains of Cobalt-Based Layered Double Hydroxides upon Electrochemical Oxidation journal October 2016
High performance nano-Ni/Graphite electrode for electro-oxidation in direct alkaline ethanol fuel cells journal September 2016
Nickel nanoparticles grown by successive ionic layer adsorption and reaction method for ethanol electrooxidation and electrochemical quartz crystal microbalance study journal January 2019
Electrochemical Quartz Microbalance characterization of Ni(OH)2-based thin film electrodes journal May 2006
Quantitative Resolution of Complex Stoichiometric Changes during Electrochemical Cycling by Density Functional Theory-Assisted Electrochemical Quartz Crystal Microbalance journal March 2020
An Electrochemical Quartz Crystal Microbalance Study of a Prospective Alkaline Anion Exchange Membrane Material for Fuel Cells: Anion Exchange Dynamics and Membrane Swelling journal March 2014