Characterization of mechanical deformation in aluminum by optical second harmonic generation

Rellaford, Kaylee N.; Averett, Shawn C.; Farnsworth, Alexander J.; Adams, Derrik D.; Smith, Scott D.; Fullwood, David T.; Patterson, James E.

doi:10.1088/1361-6501/abe668

Characterization of mechanical deformation in aluminum by optical second harmonic generation

Journal Article · 28 April 2021 · Measurement Science and Technology

DOI:https://doi.org/10.1088/1361-6501/abe668· OSTI ID:1851718

Rellaford, Kaylee N. ^[1]; Averett, Shawn C.; Farnsworth, Alexander J.; Adams, Derrik D.; Smith, Scott D.; Fullwood, David T.;

OSTI

Abstract

Second harmonic generation (SHG), a laser-based surface technique, was used to characterize near-surface defect evolution associated with mechanical deformation in 2024-T3 aluminum due to tensile loads. Electron backscatter diffraction (EBSD) measurements were also performed to determine the geometrically necessary dislocation density before and after tensile deformation. Comparison of the EBSD and SHG results found that dislocation density and SHG signal are inversely proportional; tensile deformation in the plastic regime led to an increase in dislocation density and a decrease in SHG response. A similar trend was seen in the SHG results on as-received (unpolished) Al samples; SHG response decreases with extent of plastic deformation. This study suggests that SHG has potential as a nondestructive evaluation technique.

Research Organization:: Brigham Young Univ., Provo, UT (United States)

Sponsoring Organization:: USDOE Office of Science (SC)

DOE Contract Number:: SC0012587;

OSTI ID:: 1851718

Journal Information:: Measurement Science and Technology, Journal Name: Measurement Science and Technology Journal Issue: 7 Vol. 32; ISSN 0957-0233

Publisher:: IOP Publishing

Country of Publication:: United States

Language:: English

References (29)

Review of Second Harmonic Generation Measurement Techniques for Material State Determination in Metals Matlack, K. H.; Kim, J. -Y.; Jacobs, L. J. Journal of Nondestructive Evaluation, Vol. 34, Issue 1 https://doi.org/10.1007/s10921-014-0273-5	journal	November 2014
Combining multiple NDT methods to improve testing effectiveness Lim, Malcolm K.; Cao, Honggang Construction and Building Materials, Vol. 38 https://doi.org/10.1016/j.conbuildmat.2011.01.011	journal	January 2013
Variable strain rate sensitivity in an aluminum alloy: Response and constitutive modeling Khan, Akhtar S.; Liu, Haowen International Journal of Plasticity, Vol. 36 https://doi.org/10.1016/j.ijplas.2012.02.001	journal	September 2012
Non-destructive indication of plastic deformation of cold-rolled stainless steel by magnetic adaptive testing Vértesy, G.; Tomáš, I.; Mészáros, I. Journal of Magnetism and Magnetic Materials, Vol. 310, Issue 1 https://doi.org/10.1016/j.jmmm.2006.08.001	journal	March 2007
A comparison of EBSD based strain indicators for the study of Fe-3Si steel subjected to cyclic loading Schayes, Claire; Bouquerel, Jérémie; Vogt, Jean-Bernard Materials Characterization, Vol. 115 https://doi.org/10.1016/j.matchar.2016.03.020	journal	May 2016
Lower-bound dislocation density mapping in microcoined tantalum using high-resolution electron backscatter diffraction Randall, Greg C.; Hansen, Kameron R.; Jackson, Brian Materials Characterization, Vol. 153 https://doi.org/10.1016/j.matchar.2019.04.033	journal	July 2019
A round robin EBSD measurement for quantitative assessment of small plastic strain Kamaya, Masayuki; Sakakibara, Yohei; Yoda, Rika Materials Characterization, Vol. 170 https://doi.org/10.1016/j.matchar.2020.110662	journal	December 2020
An investigation of geometrically necessary dislocations and back stress in large grained tantalum via EBSD and CPFEM Hansen, Landon T.; Fullwood, David T.; Homer, Eric R. Materials Science and Engineering: A, Vol. 772 https://doi.org/10.1016/j.msea.2019.138704	journal	January 2020
Interplay of dislocation substructure and elastic strain evolution in additively manufactured Inconel 625 Small, Kathryn A.; Clayburn, Zach; DeMott, Ryan Materials Science and Engineering: A, Vol. 785 https://doi.org/10.1016/j.msea.2020.139380	journal	May 2020
Relative SHG measurements of metal thin films: Gold, silver, aluminum, cobalt, chromium, germanium, nickel, antimony, titanium, titanium nitride, tungsten, zinc, silicon and indium tin oxide Che, Franklin; Grabtchak, Serge; Whelan, William M. Results in Physics, Vol. 7 https://doi.org/10.1016/j.rinp.2017.01.012	journal	January 2017
Estimations of bulk geometrically necessary dislocation density using high resolution EBSD Ruggles, T. J.; Fullwood, D. T. Ultramicroscopy, Vol. 133 https://doi.org/10.1016/j.ultramic.2013.04.011	journal	October 2013
A Review of Strain Analysis Using Electron Backscatter Diffraction Wright, Stuart I.; Nowell, Matthew M.; Field, David P. Microscopy and Microanalysis, Vol. 17, Issue 3 https://doi.org/10.1017/S1431927611000055	journal	March 2011
A Low-Cost Beam-Scanning Second Harmonic Generation Microscope with Application for Agrochemical Development and Testing Grubbs, Benjamin A.; Etter, Nicholas P.; Slaughter, Wesley E. Analytical Chemistry, Vol. 91, Issue 18 https://doi.org/10.1021/acs.analchem.9b02304	journal	August 2019
Surface properties probed by second-harmonic and sum-frequency generation Shen, Y. R. Nature, Vol. 337, Issue 6207 https://doi.org/10.1038/337519a0	journal	February 1989
Defect-enhanced second-harmonic generation in (SimGen)p superlattices Zhang, Chun; Xiao, Xudong; Wang, N. Applied Physics Letters, Vol. 72, Issue 17 https://doi.org/10.1063/1.121279	journal	April 1998
Second-harmonic generation studies of implantation defects depth profile in hydrogen implanted garnet film Bonda, A.; Uba, S.; Uba, L. Applied Physics Letters, Vol. 105, Issue 19 https://doi.org/10.1063/1.4901900	journal	November 2014
Characterization of metal fatigue by optical second harmonic generation Arnolds, Heike; Kakoulli, Anthony; Shah, Komalben Applied Physics Letters, Vol. 111, Issue 13 https://doi.org/10.1063/1.4995694	journal	September 2017
Nondestructive characterization of the level of plastic deformation by thermoelectric power measurements in cold-rolled Ti–6Al–4V samples Carreon, H.; Medina, A. Nondestructive Testing and Evaluation, Vol. 22, Issue 4 https://doi.org/10.1080/10589750701546960	journal	December 2007
Determination of elastic strain fields and geometrically necessary dislocation distributions near nanoindents using electron back scatter diffraction Wilkinson, Angus J.; Randman, David Philosophical Magazine, Vol. 90, Issue 9 https://doi.org/10.1080/14786430903304145	journal	March 2010
Optical Second-Harmonic Generation in Reflection from Media with Inversion Symmetry Bloembergen, N.; Chang, R. K.; Jha, S. S. Physical Review, Vol. 174, Issue 3 https://doi.org/10.1103/PhysRev.174.813	journal	October 1968
Analysis of second-harmonic generation at metal surfaces Sipe, J. E.; So, V. C. Y.; Fukui, M. Physical Review B, Vol. 21, Issue 10 https://doi.org/10.1103/PhysRevB.21.4389	journal	May 1980
Observation of rotational anisotropy in the second-harmonic generation from a metal surface Tom, H. W. K.; Aumiller, G. D. Physical Review B, Vol. 33, Issue 12 https://doi.org/10.1103/PhysRevB.33.8818	journal	June 1986
Second-harmonic generation at simple metal surfaces Liebsch, A.; Schaich, W. L. Physical Review B, Vol. 40, Issue 8 https://doi.org/10.1103/PhysRevB.40.5401	journal	September 1989
Study of Si(111) Surfaces by Optical Second-Harmonic Generation: Reconstruction and Surface Phase Transformation Heinz, T. F.; Loy, M. M. T.; Thompson, W. A. Physical Review Letters, Vol. 54, Issue 1 https://doi.org/10.1103/PhysRevLett.54.63	journal	January 1985
Nondestructive proximate testing of plastic deformations by differential thermal EMF measurements Soldatov, A. A.; Seleznev, A. I.; Fiks, I. I. Russian Journal of Nondestructive Testing, Vol. 48, Issue 3 https://doi.org/10.1134/S1061830912030060	journal	March 2012
Use of a single-mode fiber coupler for second-harmonic-generation microscopy Fu, Ling; Gan, Xiaosong; Gu, Min Optics Letters, Vol. 30, Issue 4 https://doi.org/10.1364/OL.30.000385	journal	January 2005
Strain dependence of second-harmonic generation in silicon Schriever, Clemens; Bohley, Christian; Wehrspohn, Ralf B. Optics Letters, Vol. 35, Issue 3 https://doi.org/10.1364/OL.35.000273	journal	January 2010
New Tools for Surface Second-Harmonic Generation Simpson, Garth J. Applied Spectroscopy, Vol. 55, Issue 1 https://doi.org/10.1366/0003702011951245	journal	January 2001
Combined Damage Index to Detect Plastic Deformation in Metals Using Acoustic Emission and Nonlinear Ultrasonics Zhang, Lu; Oskoe, Sepideh; Li, Hongyu Materials, Vol. 11, Issue 11 https://doi.org/10.3390/ma11112151	journal	November 2018

Similar Records

Characterization of mechanical deformation in aluminum by optical second harmonic generation

Journal Article · 2021 · Measurement Science and Technology · OSTI ID:1865467

Influence of Noise-Generating Factors on Cross-Correlation Electron Backscatter Diffraction (EBSD) Measurement of Geometrically Necessary Dislocations (GNDs)

Journal Article · 2017 · Microscopy and Microanalysis · OSTI ID:1534404

Quantitative investigation of the tensile plastic deformation characteristic and microstructure for friction stir welded 2024 aluminum alloy

Journal Article · 2012 · Materials Characterization · OSTI ID:22163150

Related Subjects

Engineering
Instruments & Instrumentation

Characterization of mechanical deformation in aluminum by optical second harmonic generation

Citation Formats

References (29)

Similar Records

Related Subjects