Implementation of cryogenic tender X-ray HR-XANES spectroscopy at the ACT station of the CAT-ACT bea

Schacherl, Bianca; Prussmann, Tim; Dardenne, Kathy; Hardock, Kirsten; Krepper, Volker; Rothe, Jorg; Vitova, Tonya; Geckeis, Horst

doi:10.1107/S1600577521012650

Implementation of cryogenic tender X-ray HR-XANES spectroscopy at the ACT station of the CAT-ACT bea

Journal Article · 01 January 2022 · J. Synchrotron Rad.

DOI:https://doi.org/10.1107/S1600577521012650· OSTI ID:1838527

Schacherl, Bianca; Prussmann, Tim; Dardenne, Kathy; Hardock, Kirsten; Krepper, Volker; Rothe, Jorg; Vitova, Tonya; Geckeis, Horst

Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: DOE - Office Of Science; FOREIGN

OSTI ID:: 1838527

Journal Information:: J. Synchrotron Rad., Vol. 29, Issue (1)

Country of Publication:: United States

Language:: ENGLISH

References (48)

The Application of HEXS and HERFD XANES for Accurate Structural Characterisation of Actinide Nanomaterials: The Case of ThO ₂ Amidani, Lucia; Vaughan, Gavin B. M.; Plakhova, Tatiana V. Chemistry – A European Journal, Vol. 27, Issue 1 https://doi.org/10.1002/chem.202003360	journal	November 2020
Pu Coexists in Three Oxidation States in a Borosilicate Glass: Implications for Pu Solubility Bahl, Sebastian; Peuget, Sylvain; Pidchenko, Ivan Inorganic Chemistry, Vol. 56, Issue 22 https://doi.org/10.1021/acs.inorgchem.7b02118	journal	October 2017
Uranium-Induced Changes in Crystal-Field and Covalency Effects of Th ⁴⁺ in Th _{1– x} U _x O ₂ Mixed Oxides Probed by High-Resolution X-ray Absorption Spectroscopy Bao, Hongliang; Duan, Peiquan; Zhou, Jing Inorganic Chemistry, Vol. 57, Issue 18 https://doi.org/10.1021/acs.inorgchem.8b01142	journal	August 2018
Recent advances in the study of the UO2–PuO2 phase diagram at high temperatures Böhler, R.; Welland, M. J.; Prieur, D. Journal of Nuclear Materials, Vol. 448, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2014.02.029	journal	May 2014
Multiconfigurational nature of 5f orbitals in uranium and plutonium intermetallics Booth, C. H.; Jiang, Y.; Wang, D. L. Proceedings of the National Academy of Sciences, Vol. 109, Issue 26 https://doi.org/10.1073/pnas.1200725109	journal	June 2012
Delocalization and occupancy effects of 5f orbitals in plutonium intermetallics using L3-edge resonant X-ray emission spectroscopy Booth, C. H.; Medling, S. A.; Jiang, Yu Journal of Electron Spectroscopy and Related Phenomena, Vol. 194 https://doi.org/10.1016/j.elspec.2014.03.004	journal	June 2014
Two-dimensional Wide-Angle X-ray Scattering on a Cm-doped borosilicate glass in a beryllium container Bouty, Olivier; Ramond, Laure; Dardenne, Kathy Journal of Synchrotron Radiation, Vol. 28, Issue 1 https://doi.org/10.1107/S1600577520015258	journal	January 2021
Resonant X-Ray Fluorescence Spectroscopy of Correlated Systems: A Probe of Charge-Transfer Excitations Butorin, S. M.; Mancini, D. C.; Guo, J. -H. Physical Review Letters, Vol. 77, Issue 3 https://doi.org/10.1103/PhysRevLett.77.574	journal	July 1996
Local Symmetry Effects in Actinide 4f X-ray Absorption in Oxides Butorin, Sergei M.; Modin, Anders; Vegelius, Johan R. Analytical Chemistry, Vol. 88, Issue 8 https://doi.org/10.1021/acs.analchem.5b04380	journal	March 2016
Chemical Reduction of Actinides Probed by Resonant Inelastic X-ray Scattering Butorin, Sergei M.; Shuh, David K.; Kvashnina, Kristina O. Analytical Chemistry, Vol. 85, Issue 23 https://doi.org/10.1021/ac4020534	journal	November 2013
Insights into the sonochemical synthesis and properties of salt-free intrinsic plutonium colloids Dalodière, Elodie; Virot, Matthieu; Morosini, Vincent Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/srep43514	journal	March 2017
Np(IV)/Np(V) valence determinations from Np L3 edge XANES/EXAFS Denecke, M.; Dardenne, K.; Marquardt, C. Talanta, Vol. 65, Issue 4 https://doi.org/10.1016/j.talanta.2004.08.034	journal	February 2005
Resonant inelastic X-ray scattering using a miniature dispersive Rowland refocusing spectrometer Ditter, Alexander S.; Holden, William M.; Cary, Samantha K. Journal of Synchrotron Radiation, Vol. 27, Issue 2 https://doi.org/10.1107/S1600577520001022	journal	February 2020
A three-crystal spectrometer for high-energy resolution fluorescence-detected X-ray absorption spectroscopy and X-ray emission spectroscopy at SSRF: Three-crystal spectrometer for HERFD-XAS and XES at SSRF Duan, Peiquan; Gu, Songqi; Cao, Hanjie X-Ray Spectrometry, Vol. 46, Issue 1 https://doi.org/10.1002/xrs.2719	journal	October 2016
In-situ high-energy-resolution X-ray absorption spectroscopy for UO2 oxidation at SSRF Duan, Pei-Quan; Bao, Hong-Liang; Li, Jiong Nuclear Science and Techniques, Vol. 28, Issue 1 https://doi.org/10.1007/s41365-016-0155-x	journal	November 2016
Extreme multi-valence states in mixed actinide oxides Epifano, E.; Naji, M.; Manara, D. Communications Chemistry, Vol. 2, Issue 1 https://doi.org/10.1038/s42004-019-0161-0	journal	May 2019
The missing pieces of the PuO ₂ nanoparticle puzzle Gerber, Evgeny; Romanchuk, Anna Yu.; Pidchenko, Ivan Nanoscale, Vol. 12, Issue 35 https://doi.org/10.1039/D0NR03767B	journal	January 2020
Resonant x-ray emission spectroscopy at the L 3 edge of americium up to 23 GPa Heathman, S.; Rueff, J. -P.; Simonelli, L. Physical Review B, Vol. 82, Issue 20 https://doi.org/10.1103/PhysRevB.82.201103	journal	November 2010
Ultra-Small Plutonium Oxide Nanocrystals: An Innovative Material in Plutonium Science Hudry, Damien; Apostolidis, Christos; Walter, Olaf Chemistry - A European Journal, Vol. 20, Issue 33 https://doi.org/10.1002/chem.201402008	journal	July 2014
Speciation Change of Uranyl in Lithium Borate Glasses Hunault, Myrtille O. J. Y.; Lelong, Gérald; Cormier, Laurent Inorganic Chemistry, Vol. 58, Issue 10 https://doi.org/10.1021/acs.inorgchem.9b00305	journal	April 2019
NpSe ₂ : a Binary Chalcogenide Containing Modulated Selenide Chains and Ambiguous‐Valent Metal Jin, Geng Bang; Malliakas, Christos D.; Hu, Yung‐Jin Angewandte Chemie International Edition, Vol. 58, Issue 45 https://doi.org/10.1002/anie.201910353	journal	November 2019
Chemical State of Complex Uranium Oxides Kvashnina, K. O.; Butorin, S. M.; Martin, P. Physical Review Letters, Vol. 111, Issue 25 https://doi.org/10.1103/PhysRevLett.111.253002	journal	December 2013
A Novel Metastable Pentavalent Plutonium Solid Phase on the Pathway from Aqueous Plutonium(VI) to PuO ₂ Nanoparticles Kvashnina, Kristina O.; Romanchuk, Anna Yu.; Pidchenko, Ivan Angewandte Chemie International Edition, Vol. 58, Issue 49 https://doi.org/10.1002/anie.201911637	journal	December 2019
Measurement of the phonon density of states of PuO 2 ( + 2 % Ga): A critical test of theory Manley, M. E.; Jeffries, J. R.; Said, A. H. Physical Review B, Vol. 85, Issue 13 https://doi.org/10.1103/PhysRevB.85.132301	journal	April 2012
Phonon density of states of α - and δ -plutonium by inelastic x-ray scattering Manley, M. E.; Said, A. H.; Fluss, M. J. Physical Review B, Vol. 79, Issue 5 https://doi.org/10.1103/PhysRevB.79.052301	journal	February 2009
Indication of single-crystal PuO 2 oxidation from O 1 s x-ray absorption spectra Modin, A.; Yun, Y.; Suzuki, M. -T. Physical Review B, Vol. 83, Issue 7 https://doi.org/10.1103/PhysRevB.83.075113	journal	February 2011
Sorption of Sr, Co and Zn on illite: Batch experiments and modelling including Co in-diffusion measurements on compacted samples Montoya, V.; Baeyens, B.; Glaus, M. A. Geochimica et Cosmochimica Acta, Vol. 223 https://doi.org/10.1016/j.gca.2017.11.027	journal	February 2018
Nanoscale mechanism of UO2 formation through uranium reduction by magnetite Pan, Zezhen; Bártová, Barbora; LaGrange, Thomas Nature Communications, Vol. 11, Issue 1 https://doi.org/10.1038/s41467-020-17795-0	journal	August 2020
Synthesis, Structural, and Electronic Properties of K ₄ Pu ^VI O ₂ (CO ₃ ) _3(cr) : An Environmentally Relevant Plutonium Carbonate Complex Pidchenko, Ivan; März, Juliane; Hunault, Myrtille O. J. Y. Inorganic Chemistry, Vol. 59, Issue 17 https://doi.org/10.1021/acs.inorgchem.0c01335	journal	August 2020
Probing Covalency in the UO ₃ Polymorphs by U M ₄ edge HR- XANES Podkovyrina, Y.; Pidchenko, I.; Prüßmann, T. Journal of Physics: Conference Series, Vol. 712 https://doi.org/10.1088/1742-6596/712/1/012092	journal	May 2016
Further insights into the chemistry of the Bi–U–O system Popa, Karin; Prieur, Damien; Manara, Dario Dalton Transactions, Vol. 45, Issue 18 https://doi.org/10.1039/C6DT00735J	journal	January 2016
Structural investigations of PuIII phosphate by X-ray diffraction, MAS-NMR and XANES spectroscopy Popa, Karin; Raison, Philippe E.; Martel, Laura Journal of Solid State Chemistry, Vol. 230 https://doi.org/10.1016/j.jssc.2015.07.002	journal	October 2015
Fifteen Years of Radionuclide Research at the KIT Synchrotron Source in the Context of the Nuclear Waste Disposal Safety Case Rothe, Jörg; Altmaier, Marcus; Dagan, Ron Geosciences, Vol. 9, Issue 2 https://doi.org/10.3390/geosciences9020091	journal	February 2019
The INE-Beamline for actinide science at ANKA Rothe, J.; Butorin, S.; Dardenne, K. Review of Scientific Instruments, Vol. 83, Issue 4 https://doi.org/10.1063/1.3700813	journal	April 2012
Pressure-induced f -electron delocalization in the U-based strongly correlated compounds U Pd 3 and U Pd 2 Al 3 : Resonant inelastic x-ray scattering and first-principles calculations Rueff, J. -P.; Raymond, S.; Yaresko, A. Physical Review B, Vol. 76, Issue 8 https://doi.org/10.1103/PhysRevB.76.085113	journal	August 2007
ROBL-II at ESRF: a synchrotron toolbox for actinide research Scheinost, Andreas C.; Claussner, Juergen; Exner, Joerg Journal of Synchrotron Radiation, Vol. 28, Issue 1 https://doi.org/10.1107/S1600577520014265	journal	January 2021
A von Hamos x-ray spectrometer based on a segmented-type diffraction crystal for single-shot x-ray emission spectroscopy and time-resolved resonant inelastic x-ray scattering studies Szlachetko, J.; Nachtegaal, M.; de Boni, E. Review of Scientific Instruments, Vol. 83, Issue 10 https://doi.org/10.1063/1.4756691	journal	October 2012
Photoelectron Spectroscopy of Plutonium at the Advanced Light Source Tobin, J. G.; Arena, D. A.; Chung, B. Journal of Nuclear Science and Technology, Vol. 39, Issue sup3 https://doi.org/10.1080/00223131.2002.10875417	journal	November 2002
Electron spectroscopy of the oxidation and aging of U and Pu Tobin, J. G.; Shuh, D. K. Journal of Electron Spectroscopy and Related Phenomena, Vol. 205 https://doi.org/10.1016/j.elspec.2015.09.001	journal	November 2015
Actinide and lanthanide speciation with high-energy resolution X-ray techniques Vitova, T.; Denecke, M. A.; Göttlicher, J. Journal of Physics: Conference Series, Vol. 430 https://doi.org/10.1088/1742-6596/430/1/012117	journal	April 2013
Polarization Dependent High Energy Resolution X-ray Absorption Study of Dicesium Uranyl Tetrachloride Vitova, Tonya; Green, Jennifer C.; Denning, Robert G. Inorganic Chemistry, Vol. 54, Issue 1 https://doi.org/10.1021/ic5020016	journal	December 2014
High energy resolution x-ray absorption spectroscopy study of uranium in varying valence states Vitova, T.; Kvashnina, K. O.; Nocton, G. Physical Review B, Vol. 82, Issue 23 https://doi.org/10.1103/PhysRevB.82.235118	journal	December 2010
Dehydration of the Uranyl Peroxide Studtite, [UO ₂ (η ² -O ₂ )(H ₂ O) ₂ ]·2H ₂ O, Affords a Drastic Change in the Electronic Structure: A Combined X-ray Spectroscopic and Theoretical Analysis Vitova, Tonya; Pidchenko, Ivan; Biswas, Saptarshi Inorganic Chemistry, Vol. 57, Issue 4 https://doi.org/10.1021/acs.inorgchem.7b02326	journal	February 2018
The role of the 5f valence orbitals of early actinides in chemical bonding Vitova, T.; Pidchenko, I.; Fellhauer, D. Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/ncomms16053	journal	July 2017
Competitive Reaction of Neptunium(V) and Uranium(VI) in Potassium–Sodium Carbonate-Rich Aqueous Media: Speciation Study with a Focus on High-Resolution X-ray Spectroscopy Vitova, Tonya; Pidchenko, Ivan; Schild, Dieter Inorganic Chemistry, Vol. 59, Issue 1 https://doi.org/10.1021/acs.inorgchem.9b02463	journal	December 2019
An EXAFS and HR-XANES study of the uranyl peroxides [UO ₂ (η ² -O ₂ )(H ₂ O) ₂ ]·nH ₂ O (n = 0, 2) and uranyl (oxy)hydroxide [(UO ₂ ) ₄ O(OH) ₆ ]·6H ₂ O Walshe, Aurora; Prüßmann, Tim; Vitova, Tonya Dalton Trans., Vol. 43, Issue 11 https://doi.org/10.1039/C3DT52437J	journal	January 2014
Interfacial Interactions between Np(V) and Manganese Oxide Minerals Manganite and Hausmannite Wilk, P. A.; Shaughnessy, D. A.; Wilson, R. E. Environmental Science & Technology, Vol. 39, Issue 8 https://doi.org/10.1021/es040080x	journal	March 2005
CAT-ACT—A new highly versatile x-ray spectroscopy beamline for catalysis and radionuclide science at the KIT synchrotron light facility ANKA Zimina, A.; Dardenne, K.; Denecke, M. A. Review of Scientific Instruments, Vol. 88, Issue 11 https://doi.org/10.1063/1.4999928	journal	November 2017

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