Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Storage and Diffusion of Carbon and Nitrogen in Crustal Materials

Technical Report ·
DOI:https://doi.org/10.2172/1830223· OSTI ID:1830223
 [1];  [2];  [2]
  1. Syracuse Univ., NY (United States). Dept. of Earth and Environmental Sciences
  2. Rensselaer Polytechnic Inst., Troy, NY (United States)

Nitrogen is a primary constituent of Earth’s atmosphere and an essential component of many biological processes. Recent developments in understanding N incorporation into silicate minerals suggest that the solid earth and lithosphere could provide a substantial reservoir for the planetary N budget. Furthermore, determining the concentration and distribution of low abundances of N in silicates presents a significant challenge in microanalysis. We tested capabilities for high spatial resolution quantification of low levels of N using EPMA with the goal of developing standards to be used in coupled N and noble gas analyses of silicate minerals. We investigated the concentration and distribution of N in a suite of ammonium-bearing silicate minerals that reflect the dominant N-bearing phases of the lithosphere: tobelite, buddingtonite, ammonioleucite, tsaregorodtsevite, and hyalophane. These minerals form during NH4-rich alteration of K-bearing silicate minerals, and the bonding environment of N in each mineral is likely to differ based on crystal structure. Using an optimized analytical routine for N quantification enables sensitivity approaching 0.02 weight% N and high-resolution quantitative mapping of sub-micron variations in N contents.

Research Organization:
Syracuse Univ., NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC)
DOE Contract Number:
SC0016246
OSTI ID:
1830223
Report Number(s):
1773849
Resource Relation:
Related Information: Nachlas, William, Baldwin, Suzanne, Thomas, Jay, and Ackerson, Michael. Investigation of N in Ammonium-bearing Silicates with Electron Probe Microanalysis (EPMA). United States: N. p., 2020. Web. doi:10.1017/s1431927620013203.
Country of Publication:
United States
Language:
English