Comparing non-destructive 3D X-ray computed tomography with destructive optical microscopy for microstructural characterization of fiber reinforced composites
Abstract
Due to their lightweight, relatively high stiffness properties, and formability into complex shapes, discontinuous fiber composites are advantageous for producing small and medium size components. Improved characterization techniques and post-processing methodologies are required for more reliable quantification of the microstructure and defect distributions in these materials, in order to employ model-based approaches to assess their structural integrity. This work compares a non-destructive X-ray approach with a destructive optical microscopy approach for characterizing the microstructural attributes, specifically the fiber volume fraction, porosity volume fraction, fiber orientation distribution, and fiber length distribution of discontinuous glass fibers in a polypropylene matrix. Additionally, a method for destructively determining the ambiguous components of the orientation tensor (related to the sign ambiguity of the out-of-plane angle in a destructive cross-sectional cut of a fiber) over a large surface area is included. It was found that fiber volume fraction and average fiber aspect ratio matched well, while fiber orientation and porosity detection had small but notable differences. The differences in the detection capabilities of each technique are quantified and discussed shedding light on the specific advantages and disadvantages of each approach, and enabling engineers to quantify uncertainty in their microstructural characterization measurements especially as they relate tomore »
- Authors:
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- U.S. Department of Defense (DOD) - Defense Advanced Research Projects Agency (DARPA); USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1618439
- DOE Contract Number:
- AC02-06CH11357
- Resource Type:
- Journal Article
- Journal Name:
- Composites Science and Technology
- Additional Journal Information:
- Journal Volume: 184
- Country of Publication:
- United States
- Language:
- English
- Subject:
- Non-destructive testing; Optical microscopy; Short-fiber composites
Citation Formats
Hanhan, Imad, Agyei, Ronald, Xiao, Xianghui, and Sangid, Michael D. Comparing non-destructive 3D X-ray computed tomography with destructive optical microscopy for microstructural characterization of fiber reinforced composites. United States: N. p., 2019.
Web. doi:10.1016/j.compscitech.2019.107843.
Hanhan, Imad, Agyei, Ronald, Xiao, Xianghui, & Sangid, Michael D. Comparing non-destructive 3D X-ray computed tomography with destructive optical microscopy for microstructural characterization of fiber reinforced composites. United States. https://doi.org/10.1016/j.compscitech.2019.107843
Hanhan, Imad, Agyei, Ronald, Xiao, Xianghui, and Sangid, Michael D. 2019.
"Comparing non-destructive 3D X-ray computed tomography with destructive optical microscopy for microstructural characterization of fiber reinforced composites". United States. https://doi.org/10.1016/j.compscitech.2019.107843.
@article{osti_1618439,
title = {Comparing non-destructive 3D X-ray computed tomography with destructive optical microscopy for microstructural characterization of fiber reinforced composites},
author = {Hanhan, Imad and Agyei, Ronald and Xiao, Xianghui and Sangid, Michael D.},
abstractNote = {Due to their lightweight, relatively high stiffness properties, and formability into complex shapes, discontinuous fiber composites are advantageous for producing small and medium size components. Improved characterization techniques and post-processing methodologies are required for more reliable quantification of the microstructure and defect distributions in these materials, in order to employ model-based approaches to assess their structural integrity. This work compares a non-destructive X-ray approach with a destructive optical microscopy approach for characterizing the microstructural attributes, specifically the fiber volume fraction, porosity volume fraction, fiber orientation distribution, and fiber length distribution of discontinuous glass fibers in a polypropylene matrix. Additionally, a method for destructively determining the ambiguous components of the orientation tensor (related to the sign ambiguity of the out-of-plane angle in a destructive cross-sectional cut of a fiber) over a large surface area is included. It was found that fiber volume fraction and average fiber aspect ratio matched well, while fiber orientation and porosity detection had small but notable differences. The differences in the detection capabilities of each technique are quantified and discussed shedding light on the specific advantages and disadvantages of each approach, and enabling engineers to quantify uncertainty in their microstructural characterization measurements especially as they relate to model based structural integrity activities.},
doi = {10.1016/j.compscitech.2019.107843},
url = {https://www.osti.gov/biblio/1618439},
journal = {Composites Science and Technology},
number = ,
volume = 184,
place = {United States},
year = {Sun Nov 10 00:00:00 EST 2019},
month = {Sun Nov 10 00:00:00 EST 2019}
}
Works referenced in this record:
Effect of screw design on fiber damage in extrusion compounding and composite properties
journal, June 1995
- Ramani, Karthik; Bank, Dave; Kraemer, Nick
- Polymer Composites, Vol. 16, Issue 3
A Study of Fibre Attrition in the Processing of Long Fibre Reinforced Thermoplastics
journal, November 1987
- Bailey, R.; Kraft, H.
- International Polymer Processing, Vol. 2, Issue 2
Techniques for compounding glass fiber-reinforced thermoplastics
journal, January 1977
- Stade, K.
- Polymer Engineering and Science, Vol. 17, Issue 1
Short predicting the strength and toughness of fiber composites
journal, December 1999
- Kardos, J. L.; Halpin, J. C.
- Macromolecular Symposia, Vol. 147, Issue 1
Behavior of discontinuous fiber composites: Fiber orientation
journal, January 1982
- Byron Pipes, R.; McCullough, Roy L.; Taggart, David G.
- Polymer Composites, Vol. 3, Issue 1
Fiber orientation and mechanical properties of short-fiber-reinforced injection-molded composites: Simulated and experimental results
journal, October 1993
- Gupta, Mahesh; Wang, K. K.
- Polymer Composites, Vol. 14, Issue 5
Effects of fiber length and fiber orientation distributions on the tensile strength of short-fiber-reinforced polymers
journal, January 1996
- Fu, S.
- Composites Science and Technology, Vol. 56, Issue 10
The Measurement of Porosity in Composite Materials Using Infrared Thermography
journal, December 1992
- Connolly, Mark P.
- Journal of Reinforced Plastics and Composites, Vol. 11, Issue 12
Characterization of fiber orientation in short‐fiber composites
journal, March 1984
- McGee, S. H.; McCullough, R. L.
- Journal of Applied Physics, Vol. 55, Issue 5
Unambiguous orientation in short fiber composites over small sampling area in a center-gated disk
journal, January 2012
- Vélez-García, Gregorio M.; Wapperom, Peter; Baird, Donald G.
- Composites Part A: Applied Science and Manufacturing, Vol. 43, Issue 1
Thermoelastic properties of short-fibre-reinforced thermoplastics
journal, May 1999
- Mlekusch, B.
- Composites Science and Technology, Vol. 59, Issue 6
Stereological measurement and error estimates for three-dimensional fiber orientation
journal, February 1992
- Bay, Randy S.; Tucker, Charles L.
- Polymer Engineering and Science, Vol. 32, Issue 4
Effects of processing conditions on the fiber length distribution and mechanical properties of glass fiber reinforced nylon-6
journal, February 2002
- Yilmazer, Ulku; Cansever, Murat
- Polymer Composites, Vol. 23, Issue 1
Fiber Length and Orientation in Long-Fiber Injection-Molded Thermoplastics — Part I: Modeling of Microstructure and Elastic Properties
journal, January 2008
- Nguyen, Ba Nghiep; Bapanapalli, Satish K.; Holbery, James D.
- Journal of Composite Materials, Vol. 42, Issue 10
Tensile properties of short-glass-fiber- and short-carbon-fiber-reinforced polypropylene composites
journal, October 2000
- Fu, S. -Y; Lauke, B.; Mäder, E.
- Composites Part A: Applied Science and Manufacturing, Vol. 31, Issue 10
Reliability in the characterization of fiber length distributions of injection molded long carbon fiber composites
journal, August 2017
- Sharma, Bhisham N.; Kijewski, Seth A.; Fifield, Leonard S.
- Polymer Composites, Vol. 39, Issue 12
A model for fiber length attrition in injection-molded long-fiber composites
journal, August 2013
- Phelps, Jay H.; Abd El-Rahman, Ahmed I.; Kunc, Vlastimil
- Composites Part A: Applied Science and Manufacturing, Vol. 51
Unambiguous Determination of 3D Fiber Orientation Distribution in Thermoplastic Composites Using SAM Image of Elliptical Mark and Interference Fringe
journal, February 2005
- Kawamura, Munehiro; Ikeda, Satoshi; Morita, Satoru
- Journal of Composite Materials, Vol. 39, Issue 4
Characterization of fiber orientation in short fiber reinforced composites with an image processing technique
journal, September 2002
- Lee, Yong Hoon; Lee, Seok Won; Youn, Jae Ryoun
- Materials Research Innovations, Vol. 6, Issue 2
Large‐area, high‐resolution image analysis of composite materials
journal, February 1997
- Davidson, N. C.; Clarke, A. R.; Archenhold, G.
- Journal of Microscopy, Vol. 185, Issue 2
3d Characterization of wood Based Fibrous Materials: an Application
journal, March 2006
- Lux, Jérôme; Delisée, Christine; Thibault, Xavier
- Image Analysis & Stereology, Vol. 25, Issue 1
3d Directional Mathematical Morphology for Analysis of Fiber Orientations
journal, November 2009
- Altendorf, Hellen; Jeulin, Dominique
- Image Analysis & Stereology, Vol. 28, Issue 3
Measurement of fibre–fibre contact in three-dimensional images of fibrous materials obtained from X-ray synchrotron microtomography
journal, May 2011
- Malmberg, F.; Lindblad, J.; Östlund, C.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 637, Issue 1
Direct observation and measurement of fiber architecture in short fiber-polymer composite foam through micro-CT imaging
journal, October 2004
- Shen, Hongbin; Nutt, Steven; Hull, David
- Composites Science and Technology, Vol. 64, Issue 13-14
X-ray microtomography
journal, December 2010
- Landis, Eric N.; Keane, Denis T.
- Materials Characterization, Vol. 61, Issue 12
A supervised iterative approach to 3D microstructure reconstruction from acquired tomographic data of heterogeneous fibrous systems
journal, December 2018
- Agyei, Ronald F.; Sangid, Michael D.
- Composite Structures, Vol. 206
X-ray computed tomography of polymer composites
journal, March 2018
- Garcea, S. C.; Wang, Y.; Withers, P. J.
- Composites Science and Technology, Vol. 156
Quantifying fibre reorientation during axial compression of a composite through time-lapse X-ray imaging and individual fibre tracking
journal, November 2018
- Emerson, Monica Jane; Wang, Ying; Withers, Philip John
- Composites Science and Technology, Vol. 168
Analysis of fibre orientation distribution in short fibre reinforced polymers: A comparison between optical and tomographic methods
journal, November 2012
- Bernasconi, A.; Cosmi, F.; Hine, P. J.
- Composites Science and Technology, Vol. 72, Issue 16
The Use of Tensors to Describe and Predict Fiber Orientation in Short Fiber Composites
journal, November 1987
- Advani, Suresh G.; Tucker, Charles L.
- Journal of Rheology, Vol. 31, Issue 8
Hydrostatically extruded glass-fiber-reinforced polyoxymethylene. I: The development of fiber and matrix orientation
journal, October 1996
- Hine, P. J.; Davidson, N.; Duckett, R. A.
- Polymer Composites, Vol. 17, Issue 5
Fibre orientation in short-fibre-reinforced thermoplastics II. Quantitative measurements by image analysis
journal, March 1999
- Mlekusch, B.
- Composites Science and Technology, Vol. 59, Issue 4
TomoPy: a framework for the analysis of synchrotron tomographic data
journal, August 2014
- Gürsoy, Dogˇa; De Carlo, Francesco; Xiao, Xianghui
- Journal of Synchrotron Radiation, Vol. 21, Issue 5
Trainable Weka Segmentation: a machine learning tool for microscopy pixel classification
journal, March 2017
- Arganda-Carreras, Ignacio; Kaynig, Verena; Rueden, Curtis
- Bioinformatics, Vol. 33, Issue 15
Viscosity of curved fibers in suspension
journal, January 2002
- Joung, C. G.; Phan-Thien, N.; Fan, X. J.
- Journal of Non-Newtonian Fluid Mechanics, Vol. 102, Issue 1
Prediction of elastic properties for curved fiber polymer composites
journal, January 2008
- Bapanapalli, Satish; Nguyen, Ba Nghiep
- Polymer Composites, Vol. 29, Issue 5
Works referencing / citing this record:
ModLayer: A MATLAB GUI Drawing Segmentation Tool for Visualizing and Classifying 3D Data
journal, November 2019
- Hanhan, Imad; Sangid, Michael D.
- Integrating Materials and Manufacturing Innovation, Vol. 8, Issue 4
Predicting Microstructural Void Nucleation in Discontinuous Fiber Composites through Coupled in-situ X-ray Tomography Experiments and Simulations
journal, February 2020
- Hanhan, Imad; Agyei, Ronald F.; Xiao, Xianghui
- Scientific Reports, Vol. 10, Issue 1