Effects of irradiation spectrum on the microstructural and mechanical properties of bulk metallic glasses

Brechtl, Jamieson; Crespillo, Miguel L.; Agarwal, Shradha; Bei, Hongbin; Zinkle, Steven J.

doi:10.1016/j.jnucmat.2020.152084

Title: Effects of irradiation spectrum on the microstructural and mechanical properties of bulk metallic glasses

Journal Article · Mon Mar 02 00:00:00 EST 2020 · Journal of Nuclear Materials

DOI:https://doi.org/10.1016/j.jnucmat.2020.152084· OSTI ID:1609044

Brechtl, Jamieson ^[1]; Crespillo, Miguel L. ^[2]; Agarwal, Shradha ^[2];

^[3]; Zinkle, Steven J. ^[4]

Univ. of Tennessee, Knoxville, TN (United States); Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Univ. of Tennessee, Knoxville, TN (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States)

Zr_52.5Cu_17.9Ni_14.6Al₁₀Ti₅ (BAM-11) and Cu60Zr₂₀Hf₁₀Ti₁₀ bulk metallic glass (BMG) specimens were ion irradiated to characterize and compare their irradiation induced microstructural and mechanical property evolution. For the ion irradiations, samples of each BMG were exposed to 9 MeV Ni³⁺ and 5.5 MeV C⁺ ions to a midrange (~1.5 μm depth) dose of 0.5 displacements per atom (dpa) at temperatures ranging from room temperature to 360 °C in order to examine potential effects associated with low (5.5 MeV C) and high (9 MeV Ni) average primary knock on energies. BAM-11 BMG samples were also irradiated by neutrons (E > 0.1 MeV) at ~70 °C to a fluence of 1.4 × 10²⁰ n/cm² (dose of 0.1 dpa). Importantly, no pronounced irradiation spectrum effects were observed for the nanoindentation mechanical properties of the two BMGs following ion irradiation. However, significant softening was observed in the BAM-11 BMG sample irradiated by neutrons, while annealing of the unirradiated samples led to a marked increase in hardening. Finally, results of the nanoindentation experiments indicate that softening is caused by irradiation induced creation of free volume defects, while the hardening is caused by their annihilation.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Fusion Energy Sciences (FES)

Grant/Contract Number:: AC05-00OR22725; SC0006661

OSTI ID:: 1609044

Alternate ID(s):: OSTI ID: 1604806

Journal Information:: Journal of Nuclear Materials, Vol. 533, Issue C; ISSN 0022-3115

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 3 works

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