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Title: Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors

Abstract

A method includes positioning a porous structure in a pressure cell; injecting an inert pressure medium within the pressure cell; and pressurizing the pressure cell to a pressure that thermodynamically favors a crystalline phase of the porous structure over an amorphous phase of the porous structure to transition the amorphous phase of the porous structure into the crystalline phase of the porous structure.

Inventors:
; ; ;
Publication Date:
Research Org.:
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1600291
Patent Number(s):
10,479,933
Application Number:
15/595,706
Assignee:
Lawrence Livermore National Security, LLC (Livermore, CA)
DOE Contract Number:  
AC52-07NA27344
Resource Type:
Patent
Resource Relation:
Patent File Date: 05/15/2017
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS

Citation Formats

Pauzauskie, Peter J., Crowhurst, Jonathan C., Worsley, Marcus A., and Satcher, Jr., Joe H. Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors. United States: N. p., 2019. Web.
Pauzauskie, Peter J., Crowhurst, Jonathan C., Worsley, Marcus A., & Satcher, Jr., Joe H. Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors. United States.
Pauzauskie, Peter J., Crowhurst, Jonathan C., Worsley, Marcus A., and Satcher, Jr., Joe H. Tue . "Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors". United States. https://www.osti.gov/servlets/purl/1600291.
@article{osti_1600291,
title = {Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors},
author = {Pauzauskie, Peter J. and Crowhurst, Jonathan C. and Worsley, Marcus A. and Satcher, Jr., Joe H.},
abstractNote = {A method includes positioning a porous structure in a pressure cell; injecting an inert pressure medium within the pressure cell; and pressurizing the pressure cell to a pressure that thermodynamically favors a crystalline phase of the porous structure over an amorphous phase of the porous structure to transition the amorphous phase of the porous structure into the crystalline phase of the porous structure.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2019},
month = {11}
}

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