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Title: Reflector Selection for the Indexing of Electron Backscatter Diffraction Patterns

Journal Article · · Microscopy and Microanalysis
 [1];  [2]; ORCiD logo [3]
  1. EDAX, Draper, UT (United States)
  2. Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Carnegie Mellon Univ., Pittsburgh, PA (United States)
  3. Carnegie Mellon Univ., Pittsburgh, PA (United States)

Abstract We propose a new methodology for ranking the reflectors used in traditional Hough-based indexing of electron backscatter diffraction (EBSD) patterns. Instead of kinematic X-ray or electron structure factors (Fhkl) currently utilized, we propose the integrated Kikuchi band intensity parameter (βhkl) based on integrated dynamical electron backscatter intensities. The proposed parameter is compared with the traditional kinematical intensity, $$I_{hkl}^{{\rm kin}} $$, as well as the average Hough transform peak intensity, $$I_{hkl}^{{\rm HSP}} $$ and used to index EBSD patterns for a number of different material systems of varying unit cell complexities including nickel, silicon, rutile, and forsterite. For elemental structures, βhkl closely follows the kinematical ranking. However, significant ranking differences arise for more complex unit cells, with the βhkl parameter showing a better correlation with the integrated Hough intensities. Lastly, Hough-based indexing of a simulated forsterite data set showed an appreciable improvement in the median confidence index (0.15 to 0.35) whenβhklis used instead of $$I_{hkl}^{{\rm kin}} $$ for ranking the reflectors.

Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
Grant/Contract Number:
AC52-07NA27344
OSTI ID:
1575868
Report Number(s):
LLNL-JRNL-762497; 951235
Journal Information:
Microscopy and Microanalysis, Vol. 25, Issue 3; ISSN 1431-9276
Publisher:
Microscopy Society of America (MSA)Copyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 3 works
Citation information provided by
Web of Science

References (17)

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Advanced Computing in Electron Microscopy book January 1998
New uniform grids on the sphere journal September 2010
Dynamical effects of anisotropic inelastic scattering in electron backscatter diffraction journal November 2008
Dirac–Fock calculations of X-ray scattering factors and contributions to the mean inner potential for electron scattering journal July 1994
An accurate parameterization for scattering factors, electron densities and electrostatic potentials for neutral atoms that obey all physical constraints journal October 2014
A method for accurate localisation of EBSD pattern centres journal January 2011
Principles of depth-resolved Kikuchi pattern simulation for electron backscatter diffraction: KIKUCHI PATTERN SIMULATION FOR EBSD journal December 2009
Dynamical Electron Backscatter Diffraction Patterns. Part I: Pattern Simulations journal June 2013
Relativistic Hartree–Fock X-ray and electron atomic scattering factors at high angles journal November 1989
Orientation sampling for dictionary-based diffraction pattern indexing methods journal November 2016
The analytical representation of atomic scattering amplitudes for electrons journal March 1962
Introduction to Conventional Transmission Electron Microscopy journal October 2003
Advanced Computing in Electron Microscopy book January 2020
Introduction to Conventional Transmission Electron Microscopy journal October 2003

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