skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Investigation of Ultrahigh-Pressure Phase Transitions in Metals with a Toroidal Diamond Anvil Cell

Technical Report ·
DOI:https://doi.org/10.2172/1573173· OSTI ID:1573173
 [1]
  1. Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Static compression experiments over 4 Mbar are rare, yet critical for developing accurate fundamental physics and chemistry models, relevant to a range of topics including modeling planetary interiors. Within this project we developed a toroidal diamond anvil geometry, crafted into single crystal diamonds with focused ion beam, with 9 μm culet proved capable of achieving pressures in excess of 5 megabars. The toroidal surface prevents gasket outflow and provides a means to stabilize the central culet. We have reached a maximum pressure of ~6.15 Mbar using Re as in-situ pressure marker, a pressure regime typically accessed only by double-stage diamond anvils and dynamic compression platforms. Moreover, utilizing these anvils for studying various transition metals the designs has proven to be a reliable platform, enabling routine static high-pressure studies in the 3 to 5 megabar pressure regime.

Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
DOE Contract Number:
AC52-07NA27344
OSTI ID:
1573173
Report Number(s):
LLNL-TR-795799; 997218
Country of Publication:
United States
Language:
English