Investigation of grafted mesoporous silicon sponge using hyperpolarized 129 Xe NMR spectroscopy

Mao, Yougang; Kim, Dokyoung; Hopson, Russell; Sailor, Michael J.; Wang, Li-Qiong

doi:10.1557/jmr.2018.226

Title: Investigation of grafted mesoporous silicon sponge using hyperpolarized ¹²⁹ Xe NMR spectroscopy

Journal Article · Thu Jul 19 00:00:00 EDT 2018 · Journal of Materials Research

DOI:https://doi.org/10.1557/jmr.2018.226· OSTI ID:1541932

Mao, Yougang; Kim, Dokyoung; Hopson, Russell; Sailor, Michael J.; Wang, Li-Qiong

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Research Organization:: Brown Univ., Providence, RI (United States)

Sponsoring Organization:: USDOE Office of Science (SC)

DOE Contract Number:: SC0007074

OSTI ID:: 1541932

Journal Information:: Journal of Materials Research, Vol. 33, Issue 17; ISSN 0884-2914

Publisher:: Materials Research Society

Country of Publication:: United States

Language:: English

References (30)

Nuclear shielding of trapped xenon obtained by proton-enhanced, magic-angle spinning xenon-129 NMR spectroscopy Ripmeester, John A. Journal of the American Chemical Society, Vol. 104, Issue 1 https://doi.org/10.1021/ja00365a053	journal	January 1982
Mesoporous silicon sponge as an anti-pulverization structure for high-performance lithium-ion battery anodes Li, Xiaolin; Gu, Meng; Hu, Shenyang Nature Communications, Vol. 5, Issue 1 https://doi.org/10.1038/ncomms5105	journal	July 2014
Polarization of the nuclear spins of noble-gas atoms by spin exchange with optically pumped alkali-metal atoms Happer, W.; Miron, E.; Schaefer, S. Physical Review A, Vol. 29, Issue 6 https://doi.org/10.1103/PhysRevA.29.3092	journal	June 1984
A ¹²⁹ Xe NMR Study of Functionalized Ordered Mesoporous Silica Moudrakovski, Igor L.; Terskikh, Victor V.; Ratcliffe, Christopher I. The Journal of Physical Chemistry B, Vol. 106, Issue 23 https://doi.org/10.1021/jp014585a	journal	June 2002
In Situ TEM Study of Lithiation Behavior of Silicon Nanoparticles Attached to and Embedded in a Carbon Matrix Gu, Meng; Li, Ying; Li, Xiaolin ACS Nano, Vol. 6, Issue 9 https://doi.org/10.1021/nn303312m	journal	August 2012
Chemical Vapor Deposited Silicon∕Graphite Compound Material as Negative Electrode for Lithium-Ion Batteries Holzapfel, M.; Buqa, H.; Krumeich, F. Electrochemical and Solid-State Letters, Vol. 8, Issue 10 https://doi.org/10.1149/1.2030448	journal	January 2005
129Xe nuclear magnetic resonance studies of the porous structure of silica gels Terskikh, Victor V.; Mudrakovskii, Igor L.; Mastikhin, Vjatcheslav M. Journal of the Chemical Society, Faraday Transactions, Vol. 89, Issue 23 https://doi.org/10.1039/ft9938904239	journal	January 1993
Nano- and bulk-silicon-based insertion anodes for lithium-ion secondary cells Kasavajjula, Uday; Wang, Chunsheng; Appleby, A. John Journal of Power Sources, Vol. 163, Issue 2, p. 1003-1039 https://doi.org/10.1016/j.jpowsour.2006.09.084	journal	January 2007
The failure mechanism of nano-sized Si-based negative electrodes for lithium ion batteries Oumellal, Y.; Delpuech, N.; Mazouzi, D. Journal of Materials Chemistry, Vol. 21, Issue 17 https://doi.org/10.1039/c1jm10213c	journal	January 2011
High‐volume production of laser‐polarized ¹²⁹ Xe Driehuys, B.; Cates, G. D.; Miron, E. Applied Physics Letters, Vol. 69, Issue 12 https://doi.org/10.1063/1.117022	journal	September 1996
Grand Canonical Monte Carlo Simulations of the ¹²⁹ Xe NMR Line Shapes of Xenon Adsorbed in (±)-[Co(en) ₃ ]Cl ₃ Sears, Devin N.; Wasylishen, Roderick E.; Ueda, Takahiro The Journal of Physical Chemistry B, Vol. 110, Issue 23 https://doi.org/10.1021/jp061655a	journal	June 2006
A review of the electrochemical performance of alloy anodes for lithium-ion batteries Zhang, Wei-Jun Journal of Power Sources, Vol. 196, Issue 1 https://doi.org/10.1016/j.jpowsour.2010.07.020	journal	January 2011
Studying the Kinetics of Crystalline Silicon Nanoparticle Lithiation with In Situ Transmission Electron Microscopy McDowell, Matthew T.; Ryu, Ill; Lee, Seok Woo Advanced Materials, Vol. 24, Issue 45 https://doi.org/10.1002/adma.201202744	journal	September 2012
Thermally Induced Silane Dehydrocoupling on Silicon Nanostructures Kim, Dokyoung; Joo, Jinmyoung; Pan, Youlin Angewandte Chemie International Edition, Vol. 55, Issue 22 https://doi.org/10.1002/anie.201601010	journal	April 2016
Materials Challenges Facing Electrical Energy Storage Whittingham, M. Stanley MRS Bulletin, Vol. 33, Issue 4 https://doi.org/10.1557/mrs2008.82	journal	April 2008
Hyperpolarized 129Xe nuclear magnetic resonance study of mesoporous silicon sponge materials Mao, Yougang; Kim, Dokyoung; Joo, Jinmyoung Journal of Materials Research, Vol. 32, Issue 16 https://doi.org/10.1557/jmr.2017.151	journal	May 2017
Noble-Gas NMR Detection through Noble-Gas-Rubidium Hyperfine Contact Interaction Grover, B. C. Physical Review Letters, Vol. 40, Issue 6 https://doi.org/10.1103/PhysRevLett.40.391	journal	February 1978
Reversible Cycling of Crystalline Silicon Powder Obrovac, M. N.; Krause, L. J. Journal of The Electrochemical Society, Vol. 154, Issue 2 https://doi.org/10.1149/1.2402112	journal	January 2007
Probing Porosity and Pore Interconnectivity in Crystalline Mesoporous TiO ₂ Using Hyperpolarized ¹²⁹ Xe NMR Wang, Li-Qiong; Wang, Donghai; Liu, Jun The Journal of Physical Chemistry C, Vol. 113, Issue 16 https://doi.org/10.1021/jp809740e	journal	March 2009
Application of xenon-129 NMR to the study of microporous solids Ripmeester, J. A.; Ratcliffe, C. I. The Journal of Physical Chemistry, Vol. 94, Issue 19 https://doi.org/10.1021/j100382a061	journal	September 1990
A High Precision Coulometry Study of the SEI Growth in Li/Graphite Cells Smith, A. J.; Burns, J. C.; Zhao, Xuemei Journal of The Electrochemical Society, Vol. 158, Issue 5 https://doi.org/10.1149/1.3557892	journal	January 2011
Size Control of Porous Silicon Nanoparticles by Electrochemical Perforation Etching Qin, Zhengtao; Joo, Jinmyoung; Gu, Luo Particle & Particle Systems Characterization, Vol. 31, Issue 2 https://doi.org/10.1002/ppsc.201300244	journal	August 2013
Long-Term Low-Rate Cycling of LiCoO ₂ /Graphite Li-Ion Cells at 55°C Smith, A. J.; Dahn, Hannah M.; Burns, J. C. Journal of The Electrochemical Society, Vol. 159, Issue 6 https://doi.org/10.1149/2.056206jes	journal	January 2012
Size-Dependent Fracture of Silicon Nanoparticles During Lithiation Liu, Xiao Hua; Zhong, Li; Huang, Shan ACS Nano, Vol. 6, Issue 2 https://doi.org/10.1021/nn204476h	journal	January 2012
Building better batteries Armand, M.; Tarascon, J.-M. Nature, Vol. 451, Issue 7179, p. 652-657 https://doi.org/10.1038/451652a	journal	February 2008
Who will drive electric vehicles, olivine or spinel? Park, Ok Kyung; Cho, Yonghyun; Lee, Sanghan Energy & Environmental Science, Vol. 4, Issue 5 https://doi.org/10.1039/c0ee00559b	journal	January 2011
Optical Pumping System Design for Large Production of Hyperpolarized ${}^{129}{Xe}$ Ruset, I. C.; Ketel, S.; Hersman, F. W. Physical Review Letters, Vol. 96, Issue 5 https://doi.org/10.1103/PhysRevLett.96.053002	journal	February 2006
A General Correlation for the ¹²⁹ Xe NMR Chemical Shift−Pore Size Relationship in Porous Silica-Based Materials Terskikh, Victor V.; Moudrakovski, Igor L.; Breeze, Steven R. Langmuir, Vol. 18, Issue 15 https://doi.org/10.1021/la025714x	journal	July 2002
¹²⁹ Xe NMR study of xenon adsorbed on Y zeolites Ito, Taro; Fraissard, Jacques The Journal of Chemical Physics, Vol. 76, Issue 11 https://doi.org/10.1063/1.442917	journal	June 1982
Analysis of porosity in porous silicon using hyperpolarized 129Xe two-dimensional exchange experiments Knagge, Kevin; Smith, Jay R.; Smith, Luis J. Solid State Nuclear Magnetic Resonance, Vol. 29, Issue 1-3 https://doi.org/10.1016/j.ssnmr.2005.10.001	journal	February 2006

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