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Title: Metal nanofoams via a facile microwave-assisted solvothermal process


A novel, facile, non-hazardous, low temperature/pressure microwave solvothermal method of producing pure copper, silver, and nickel metal nanofoams is presented.

 [1]; ORCiD logo [1]
  1. Materials Science and Engineering Program & Texas Materials Institute; University of Texas at Austin; Austin; USA
Publication Date:
Research Org.:
Univ. of Texas, Austin, TX (United States)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
DOE Contract Number:  
Resource Type:
Journal Article
Journal Name:
Additional Journal Information:
Journal Volume: 53; Journal Issue: 5; Journal ID: ISSN 1359-7345
Royal Society of Chemistry
Country of Publication:
United States

Citation Formats

Kreder, K. J., and Manthiram, A. Metal nanofoams via a facile microwave-assisted solvothermal process. United States: N. p., 2017. Web. doi:10.1039/c6cc08322f.
Kreder, K. J., & Manthiram, A. Metal nanofoams via a facile microwave-assisted solvothermal process. United States. doi:10.1039/c6cc08322f.
Kreder, K. J., and Manthiram, A. Sun . "Metal nanofoams via a facile microwave-assisted solvothermal process". United States. doi:10.1039/c6cc08322f.
title = {Metal nanofoams via a facile microwave-assisted solvothermal process},
author = {Kreder, K. J. and Manthiram, A.},
abstractNote = {A novel, facile, non-hazardous, low temperature/pressure microwave solvothermal method of producing pure copper, silver, and nickel metal nanofoams is presented.},
doi = {10.1039/c6cc08322f},
journal = {ChemComm},
issn = {1359-7345},
number = 5,
volume = 53,
place = {United States},
year = {2017},
month = {1}

Works referenced in this record:

High rate capabilities Fe3O4-based Cu nano-architectured electrodes for lithium-ion battery applications
journal, June 2006

  • Taberna, P. L.; Mitra, S.; Poizot, P.
  • Nature Materials, Vol. 5, Issue 7, p. 567-573
  • DOI: 10.1038/nmat1672

Three-dimensional bicontinuous ultrafast-charge and -discharge bulk battery electrodes
journal, March 2011

  • Zhang, Huigang; Yu, Xindi; Braun, Paul V.
  • Nature Nanotechnology, Vol. 6, Issue 5, p. 277-281
  • DOI: 10.1038/nnano.2011.38

Three-Dimensionally Engineered Porous Silicon Electrodes for Li Ion Batteries
journal, February 2012

  • Gowda, Sanketh R.; Pushparaj, Victor; Herle, Subramanya
  • Nano Letters, Vol. 12, Issue 12
  • DOI: 10.1021/nl302114j

Three-dimensional electrodes and battery architectures
journal, July 2011

  • Arthur, Timothy S.; Bates, Daniel J.; Cirigliano, Nicolas
  • MRS Bulletin, Vol. 36, Issue 7
  • DOI: 10.1557/mrs.2011.156

High-power lithium ion microbatteries from interdigitated three-dimensional bicontinuous nanoporous electrodes
journal, April 2013

  • Pikul, James H.; Gang Zhang, Hui; Cho, Jiung
  • Nature Communications, Vol. 4, Article No. 1732
  • DOI: 10.1038/ncomms2747

Metal Foam as Positive Electrode Current Collector for LiFePO 4 -Based Li-Ion Battery
journal, October 2013

  • Yang, Gui Fu; Song, Jae Sun; Kim, Hyung Yoon
  • Japanese Journal of Applied Physics, Vol. 52, Issue 10S
  • DOI: 10.7567/JJAP.52.10MB13

Construction of High-Capacitance 3D CoO@Polypyrrole Nanowire Array Electrode for Aqueous Asymmetric Supercapacitor
journal, April 2013

  • Zhou, Cheng; Zhang, Yangwei; Li, Yuanyuan
  • Nano Letters, Vol. 13, Issue 5
  • DOI: 10.1021/nl400378j

A Nanostructured Electrochromic Supercapacitor
journal, January 2012

  • Wei, Di; Scherer, Maik R. J.; Bower, Chris
  • Nano Letters, Vol. 12, Issue 4
  • DOI: 10.1021/nl2042112

One-pot synthesis of nanotube-based hierarchical copper silicate hollow spheres
journal, January 2008

  • Wang, Yongqiang; Wang, Guozhong; Wang, Hongqiang
  • Chemical Communications, Issue 48
  • DOI: 10.1039/b816751f

Three-Dimensional Metal Scaffold Supported Bicontinuous Silicon Battery Anodes
journal, May 2012

  • Zhang, Huigang; Braun, Paul V.
  • Nano Letters, Vol. 12, Issue 6
  • DOI: 10.1021/nl204551m

3-D Integrated All-Solid-State Rechargeable Batteries
journal, December 2007

  • Notten, P. H. L.; Roozeboom, F.; Niessen, R. A. H.
  • Advanced Materials, Vol. 19, Issue 24
  • DOI: 10.1002/adma.200702398

Fabrication of High-Aspect-Ratio Electrode Arrays for Three-Dimensional Microbatteries
journal, August 2007

  • Chamran, Fardad; Yeh, Yuting; Min, Hong-Seok
  • Journal of Microelectromechanical Systems, Vol. 16, Issue 4
  • DOI: 10.1109/JMEMS.2007.901638

Fabrication and properties of a carbon/polypyrrole three-dimensional microbattery
journal, April 2008

Electrochemical Fabrication of Low Density Metal Foam with Mono-Dispersed-Sized Micro- and Submicro-Meter Pore
journal, May 2006

  • Nagai, Keiji; Wada, Daisuke; Nakai, Mitsuo
  • Fusion Science and Technology, Vol. 49, Issue 4
  • DOI: 10.13182/FST06-A1186

Ultralow-Density Nanostructured Metal Foams:  Combustion Synthesis, Morphology, and Composition
journal, May 2006

  • Tappan, B. C.; Huynh, M. H.; Hiskey, M. A.
  • Journal of the American Chemical Society, Vol. 128, Issue 20
  • DOI: 10.1021/ja056550k

Nanoporous Metal Foams
journal, May 2010

  • Tappan, Bryce C.; Steiner, Stephen A.; Luther, Erik P.
  • Angewandte Chemie International Edition, Vol. 49, Issue 27
  • DOI: 10.1002/anie.200902994

Dextran templating for the synthesis of metallic and metal oxide sponges
journal, May 2003

  • Walsh, Dominic; Arcelli, Laura; Ikoma, Toshiyuki
  • Nature Materials, Vol. 2, Issue 6
  • DOI: 10.1038/nmat903

Preparation of Macroporous Metal Films from Colloidal Crystals
journal, September 1999

  • Jiang, Peng; Cizeron, Joel; Bertone, Jane F.
  • Journal of the American Chemical Society, Vol. 121, Issue 34, p. 7957-7958
  • DOI: 10.1021/ja991321h

A Chemical Synthesis of Periodic Macroporous NiO and Metallic Ni
journal, August 1999

Evolution of nanoporosity in dealloying
journal, March 2001

  • Erlebacher, Jonah; Aziz, Michael J.; Karma, Alain
  • Nature, Vol. 410, Issue 6827, p. 450-453
  • DOI: 10.1038/35068529

Nanoporous Metals with Controlled Multimodal Pore Size Distribution
journal, July 2003

  • Ding, Yi; Erlebacher, Jonah
  • Journal of the American Chemical Society, Vol. 125, Issue 26
  • DOI: 10.1021/ja035318g

Smelting in the age of nano: iron aerogels
journal, January 2009

  • Leventis, Nicholas; Chandrasekaran, Naveen; Sotiriou-Leventis, Chariklia
  • J. Mater. Chem., Vol. 19, Issue 1
  • DOI: 10.1039/B815985H

BTA Copper Complexes
journal, October 2005

  • Friedrich, Manfred; Gálvez-Ruiz, Juan Carlos; Klapötke, Thomas M.
  • Inorganic Chemistry, Vol. 44, Issue 22
  • DOI: 10.1021/ic050657r

Copper Bis(1-methyl-5-nitriminotetrazolate): A Promising New Primary Explosive
journal, October 2007

  • Geisberger, Georg; Klapötke, Thomas M.; Stierstorfer, Jörg
  • European Journal of Inorganic Chemistry, Vol. 2007, Issue 30
  • DOI: 10.1002/ejic.200700395

Ni/Ni 3 C Core–Shell Nanochains and Its Magnetic Properties: One-Step Synthesis at Low Temperature
journal, April 2008

  • Zhou, Wei; Zheng, Kun; He, Lin
  • Nano Letters, Vol. 8, Issue 4
  • DOI: 10.1021/nl073291j

Controlled Synthesis and Morphology-Dependent Electromagnetic Properties of Hierarchical Cobalt Assemblies
journal, August 2010

  • Wang, Chao; Han, Xijiang; Zhang, Xiaolin
  • The Journal of Physical Chemistry C, Vol. 114, Issue 35
  • DOI: 10.1021/jp1050386

Noble Metal Aerogels—Synthesis, Characterization, and Application as Electrocatalysts
journal, January 2015

  • Liu, Wei; Herrmann, Anne-Kristin; Bigall, Nadja C.
  • Accounts of Chemical Research, Vol. 48, Issue 2
  • DOI: 10.1021/ar500237c

Polyol synthesis of nanoparticles: status and options regarding metals, oxides, chalcogenides, and non-metal elements
journal, January 2015

  • Dong, H.; Chen, Y. -C.; Feldmann, C.
  • Green Chemistry, Vol. 17, Issue 8
  • DOI: 10.1039/C5GC00943J

Preparation of hexagonal close-packed nickel nanoparticles via a thermal decomposition approach using nickel acetate tetrahydrate as a precursor
journal, May 2009

Controlling Combustion Wave Propagation for Transition Metal/Alloy/Cermet Foam Synthesis
journal, April 2008