Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper

Shin, Yongsoon; Li, Xiaohong S; Wang, Chongmin; Coleman, James E; Exarhos, Gregory J

doi:10.1002/adma.200306661

Title: Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper

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Abstract

An aqueous-based, inexpensive, TiO2 precursor, Tyzor-LA, and cellulose paper have been used to prepare TiC via carbothermal reduction in an Ar flow. The hierarchical cellulose structures were also completely maintained through the agglomeration of 10-50nm TiC nanoparticles, and the lattice parameter of TiC increased with the increase of reaction temperature, while the oxygen content in the sample decreased (0.24wt% at 1500 C).

Authors:: Shin, Yongsoon; Li, Xiaohong S; Wang, Chongmin; Coleman, James E; Exarhos, Gregory J

Publication Date:: Mon Jul 19 00:00:00 EDT 2004

Research Org.:: Pacific Northwest National Lab., Richland, WA (US), Environmental Molecular Sciences Laboratory (US)

Sponsoring Org.:: US Department of Energy (US)

OSTI Identifier:: 15009999

Report Number(s):: PNNL-SA-41057
5107a; KC0201050; TRN: US200433%%416

DOE Contract Number:: AC05-76RL01830

Resource Type:: Journal Article

Journal Name:: Advanced Materials

Additional Journal Information:: Journal Volume: 16; Journal Issue: 14; Other Information: PBD: 19 Jul 2004

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; AGGLOMERATION; CELLULOSE; LATTICE PARAMETERS; PRECURSOR; SYNTHESIS; TITANIUM CARBIDES; TITANIUM OXIDES; ENVIRONMENTAL MOLECULAR SCIENCES LABORATORY; CARBOTHERMAL SYNTHESIS; MINERALIZATION; POWDERS; WOOD

Citation Formats


                    Shin, Yongsoon, Li, Xiaohong S, Wang, Chongmin, Coleman, James E, and Exarhos, Gregory J. Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper.  United States: N. p., 2004. 
        Web.  doi:10.1002/adma.200306661.

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                    Shin, Yongsoon, Li, Xiaohong S, Wang, Chongmin, Coleman, James E, & Exarhos, Gregory J. Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper.  United States.  https://doi.org/10.1002/adma.200306661

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                    Shin, Yongsoon, Li, Xiaohong S, Wang, Chongmin, Coleman, James E, and Exarhos, Gregory J. 2004.  
        "Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper".  United States.  https://doi.org/10.1002/adma.200306661.

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@article{osti_15009999,

  title        = {Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper},

  author       = {Shin, Yongsoon and Li, Xiaohong S and Wang, Chongmin and Coleman, James E and Exarhos, Gregory J},

  abstractNote = {An aqueous-based, inexpensive, TiO2 precursor, Tyzor-LA, and cellulose paper have been used to prepare TiC via carbothermal reduction in an Ar flow. The hierarchical cellulose structures were also completely maintained through the agglomeration of 10-50nm TiC nanoparticles, and the lattice parameter of TiC increased with the increase of reaction temperature, while the oxygen content in the sample decreased (0.24wt% at 1500 C).},

  doi          = {10.1002/adma.200306661},

  url          = {https://www.osti.gov/biblio/15009999},
  journal      = {Advanced Materials},
number       = 14,

  volume       = 16,

  place        = {United States},

  year         = {Mon Jul 19 00:00:00 EDT 2004},

  month        = {Mon Jul 19 00:00:00 EDT 2004}

}

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