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Title: Experiments and simulations on solidification microstructure for Inconel 718 in powder bed fusion electron beam additive manufacturing

Journal Article · · Additive Manufacturing

Previous research on the powder bed fusion electron beam additive manufacturing of Inconel 718 has established a definite correlation between the processing conditions and the solidification microstructure of components. However, the direct role of physical phenomena such as fluid flow and vaporization on determining the solidification morphology have not been investigated quantitatively. In this work, we investigate the transient and spatial evolution of the fusion zone geometry, temperature gradients, and solidification growth rates during pulsed electron beam melting of the powder bed with a focus on the role of key physical phenomena. The effect of spot density during pulsing, which relates to the amount of heating of the build area during processing, on the columnar-to-equiaxed transition of the solidification structure was studied both experimentally and theoretically. Predictions and the evaluation of the role of heat transfer and fluid flow were established using existing solidification theories combined with transient, three-dimensional numerical heat transfer and fluid flow modeling. Metallurgical characteristics of the alloy’s solidification are extracted from the transient temperature fields, and microstructure is predicted and validated using optical images and electron backscattered diffraction data from the experimental results. Simulations show that the pure liquid region solidified quickly, creating a large two-phase, mushy region that exists during the majority of solidification. While conductive heat transfer dominates in the mushy region, both the pool geometry and the solidification parameters are affected by convective heat transfer. Lastly, increased spot density during processing is shown to increase the time of solidification, lowering temperature gradients and increasing the probability of equiaxed grain formation.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1494899
Journal Information:
Additive Manufacturing, Vol. 25, Issue C; ISSN 2214-8604
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 70 works
Citation information provided by
Web of Science

References (36)

Thermographic Microstructure Monitoring in Electron Beam Additive Manufacturing journal March 2017
Site specific control of crystallographic grain orientation through electron beam additive manufacturing journal November 2014
Localized melt-scan strategy for site specific control of grain size and primary dendrite arm spacing in electron beam additive manufacturing journal November 2017
The metallurgy and processing science of metal additive manufacturing journal March 2016
Crystallographic texture engineering through novel melt strategies via electron beam melting: Inconel 718 journal October 2014
Additive Manufacturing of Nickel Superalloys: Opportunities for Innovation and Challenges Related to Qualification journal June 2018
Steady state columnar and equiaxed growth of dendrites and eutectic journal July 1984
Theory of microstructural development during rapid solidification journal May 1986
The effect of welding conditions on stray grain formation in single crystal welds – theoretical analysis journal January 2005
Single-crystal laser deposition of superalloys: processing–microstructure maps journal April 2001
Numerical modeling of heat-transfer and the influence of process parameters on tailoring the grain morphology of IN718 in electron beam additive manufacturing journal June 2016
Lattice Boltzmann model for thermal free surface flows with liquid–solid phase transition journal February 2011
Influence of the Scanning Strategy on the Microstructure and Mechanical Properties in Selective Electron Beam Melting of Ti-6Al-4V: Influence of the Scanning Strategy on the Microstructure … journal April 2015
Mesoscopic simulation of selective beam melting processes journal June 2011
Evolution of solidification texture during additive manufacturing journal November 2015
Grain structure evolution in Inconel 718 during selective electron beam melting journal June 2016
Additive manufacturing of metallic components – Process, structure and properties journal March 2018
Physical processes in fusion welding journal January 1995
Heat and fluid flow in additive manufacturing—Part I: Modeling of powder bed fusion journal July 2018
Heat transfer and material flow during laser assisted multi-layer additive manufacturing journal September 2014
Probing temperature during laser spot welding from vapor composition and modeling journal November 2003
A heat-transfer and fluid-flow-based model to obtain a specific weld geometry using various combinations of welding variables journal August 2005
Heat transfer and fluid flow during laser spot welding of 304 stainless steel journal May 2003
Mechanisms of selective laser sintering and heat transfer in Ti powder journal December 2003
The physical properties of alloys in the liquid and ?mushy? states journal September 1996
Total hemispherical emissivity of Inconel 718 journal June 2015
Mathematical simulation of the influence of ion-compensation, self-magnetic field and scattering on an electron beam during welding journal June 2001
Effects of oxygen and sulfur on alloying element vaporization rates during laser welding journal December 1988
Metal vaporization from weld pools journal September 1984
Macrotransport-solidification kinetics modeling of equiaxed dendritic growth: Part II. Computation problems and validation on INCONEL 718 superalloy castings journal December 1996
Macrotransport-solidification kinetics modeling of equiaxed dendritic growth: Part I. Model development and discussion journal December 1996
Nucleation ahead of the advancing interface in directional solidification journal June 1997
Columnar to equiaxed transition in solidification processing journal January 2001
Characterisation of electron beams at different focus settings and work distances in multiple welders using the enhanced modified Faraday cup journal February 2007
Dimensionless numbers in additive manufacturing journal February 2017
Modeling of heat transfer and fluid flow during gas tungsten arc spot welding of low carbon steel journal March 2003

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