Investigation of temperature approximation methods during flash sintering of ZnO

Charalambous, Harry; Jha, Shikhar Krishn; Lay, Ryan T.; Cabales, Avaniek; Okasinski, John; Tsakalakos, Thomas

doi:10.1016/j.ceramint.2017.12.250

Title: Investigation of temperature approximation methods during flash sintering of ZnO

Journal Article · Thu Jan 04 00:00:00 EST 2018 · Ceramics International

DOI:https://doi.org/10.1016/j.ceramint.2017.12.250· OSTI ID:1466312

Charalambous, Harry ^[1]; Jha, Shikhar Krishn ^[1]; Lay, Ryan T. ^[1]; Cabales, Avaniek ^[1]; Okasinski, John ^[2]; Tsakalakos, Thomas ^[1]

Rutgers Univ., New Brunswick, NJ (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)

The lattice expansion in ZnO, using in-situ X ray diffraction, has been investigated during flash sintering with varying current densities. While current flow through the specimen enhances the kinetics of sintering for ZnO, the temperature is not high enough to claim thermal runaway or localized melting. Unlike the case of yttria stabilized zirconia [1,2], experimental temperature approximations predict comparable specimen temperature to conventional sintering temperature of ZnO. Microstructural analysis supports the findings of the in-situ temperature approximations. In comparison with black body radiation, a gap between theoretical value and measured value was found due to flaws in the theoretical model. In addition, a new type of flash sintering was introduced, with current ramp, to avoid the power spike which has been the source of much debate about the transition from voltage to current control. In conclusion, the advantage of this method is in the controlled sintering kinetics thus avoiding the channeling found in dielectric materials [3].

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: US Department of the Navy, Office of Naval Research (ONR); USDOE

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1466312

Alternate ID(s):: OSTI ID: 1691773

Journal Information:: Ceramics International, Vol. 44, Issue 6; ISSN 0272-8842

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 47 works

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The effects of external fields in ceramic sintering Jha, Shikhar K.; Phuah, Xin Li; Luo, Jian Journal of the American Ceramic Society https://doi.org/10.1111/jace.16061	journal	September 2018
Reactive flash sintering: MgO and α‐Al ₂ O ₃ transform and sinter into single‐phase polycrystals of MgAl ₂ O ₄ Yoon, Bola; Yadav, Devinder; Ghose, Sanjit Journal of the American Ceramic Society https://doi.org/10.1111/jace.15974	journal	October 2018
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36 MATERIALS SCIENCE
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