Multi-frequency ferromagnetic resonance investigation of nickel nanocubes encapsulated in diamagnetic magnesium oxide matrix

Nellutla, Saritha; Nori, Sudhakar; Singamaneni, Srinivasa R.; Prater, John T.; Narayan, Jagdish; Smirnov, Alex I.

doi:10.1063/1.4971869

Title: Multi-frequency ferromagnetic resonance investigation of nickel nanocubes encapsulated in diamagnetic magnesium oxide matrix

Journal Article · Thu Dec 15 00:00:00 EST 2016 · Journal of Applied Physics

DOI:https://doi.org/10.1063/1.4971869· OSTI ID:1465126

Nellutla, Saritha ^[1]; Nori, Sudhakar ^[2]; Singamaneni, Srinivasa R. ^[3]; Prater, John T. ^[4]; Narayan, Jagdish ^[2];

^[5]

Bridgewater State Univ., Bridgewater, MA (United States). Dept. of Chemical Sciences
North Carolina State Univ., Raleigh, NC (United States). Center for Advanced Materials and Smart Structures and Dept. of Materials Science and Engineering
North Carolina State Univ., Raleigh, NC (United States). Center for Advanced Materials and Smart Structures and Dept. of Materials Science and Engineering; US Army Research Office (ARO), Durham, NC (United States). Materials Science Division; Univ. of Texas, El Paso, TX (United States). Dept. of Physics
US Army Research Office (ARO), Durham, NC (United States). Materials Science Division
North Carolina State Univ., Raleigh, NC (United States). Dept. of Chemistry

For this, partially aligned nickel nanocubes were grown epitaxially in a diamagnetic magnesium oxide (MgO:Ni) host and studied by a continuous wave ferromagnetic resonance (FMR) spectroscopy at the X-band (9.5 GHz) from ca. 117 to 458 K and then at room temperature for multiple external magnetic fields/resonant frequencies from 9.5 to 330 GHz. In contrast to conventional magnetic susceptibility studies that provided data on the bulk magnetization, the FMR spectra revealed the presence of three different types of magnetic Ni nanocubes in the sample. Specifically, three different ferromagnetic resonances were observed in the X-band spectra: a line 1 assigned to large nickel nanocubes, a line 2 corresponding to the nanocubes exhibiting saturated magnetization even at ca. 0.3 T field, and a high field line 3 (g_eff ~ 6.2) tentatively assigned to small nickel nanocubes likely having their hard magnetization axis aligned along or close to the direction of the external magnetic field. Based on the analysis of FMR data, the latter nanocubes possess an anisotropic internal magnetic field of at least ~1.0 T in magnitude.

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Research Organization:: North Carolina State University, Raleigh, NC (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF); North Carolina Biotechnology Center (NCBC), Durham, NC (United States); National Institutes of Health (NIH)

Contributing Organization:: National High Magnetic Field Lab. (NHMFL), Tallahassee, FL (United States)

Grant/Contract Number:: FG02-02ER15354; S10RR023614; CHE-0840501; 2009-IDG-1015; DMR 1157490

OSTI ID:: 1465126

Alternate ID(s):: OSTI ID: 1336479

Journal Information:: Journal of Applied Physics, Vol. 120, Issue 22; ISSN 0021-8979

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 2 works

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77 NANOSCIENCE AND NANOTECHNOLOGY
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
36 MATERIALS SCIENCE
ferromagnetism
magnetic moments
nanoparticles
linewidths
nickel
ferromagnetic resonance
magnetic anisotropy
magnetic fields
diamagnetism

Title: Multi-frequency ferromagnetic resonance investigation of nickel nanocubes encapsulated in diamagnetic magnesium oxide matrix

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