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Title: Ultra-low blaze angle gratings for synchrotron and free electron laser applications

Journal Article · · Optics Express
DOI:https://doi.org/10.1364/OE.26.022011· OSTI ID:1463933

We have developed a method for the manufacture of x-ray diffraction gratings with arbitrarily small blaze angles. These gratings are made by a process in which a high blaze angle grating made by anisotropic etching of Si (111) is subjected to planarization and reactive ion etching. Differential etching of the planarization medium and silicon ensures reduction of the blaze angle. Repeated application of this process leads to gratings of increasing perfection with an arbitrarily small blaze angle. This opens the way to highly efficient low line density gratings, to damage resistant gratings for ultra-high power applications such as free electron lasers, and for extension of the use of gratings into the hard x-ray energy range for dispersive spectroscopy.

Research Organization:
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
AC02-05CH11231
OSTI ID:
1463933
Alternate ID(s):
OSTI ID: 1480808
Journal Information:
Optics Express, Journal Name: Optics Express Vol. 26 Journal Issue: 17; ISSN 1094-4087
Publisher:
Optical Society of AmericaCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 10 works
Citation information provided by
Web of Science

References (12)

Gratings for synchrotron and FEL beamlines: a project for the manufacture of ultra-precise gratings at Helmholtz Zentrum Berlin journal January 2018
Refraction effects in soft x-ray multilayer blazed gratings journal January 2016
Planarization during spin coating journal May 1992
Investigating the interaction of x-ray free electron laser radiation with grating structure journal January 2012
X-ray diffraction gratings: Precise control of ultra-low blaze angle via anisotropic wet etching journal July 2016
Fabrication and characterization of a new high density Sc/Si multilayer sliced grating conference August 2008
Large area nanoimprint enables ultra-precise x-ray diffraction gratings journal January 2017
Towards 10 meV resolution: The design of an ultrahigh resolution soft X-ray RIXS spectrometer journal November 2016
On symmetric X-ray beam splitting with high efficiency by use of reflection gratings with rectangular profile in the extreme off-plane configuration journal January 2015
Development of coherent scattering and diffractive imaging and the COSMIC facility at the Advanced Light Source journal March 2013
Gratings with Blaze Angles Down to 0.1° for Photon Energies up to 10 keV
  • Heidemann, K. F.; Nelles, B.; Lenke, R.
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436104
conference January 2007
From Soft to Hard X-ray with a Single Grating Monochromator
  • Cocco, D.; Bianco, A.; Kaulich, B.
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436107
conference January 2007

Cited By (1)

On smart optimization of blazed soft X-ray gratings journal June 2019

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