High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization
Abstract
Changes in bulk crystallization behavior following devitrification at high pressure are investigated for a Fe78B13Si9 composition metallic glass using in-situ energy dispersive x-ray powder diffraction. Crystallization with time was evaluated for a series of measurements to a maximum pressure of 5.63 ± 0.15 GPa for the Fe78B13Si9 glass. Pressure was found to strongly affect onset bulk crystallization temperature Tx. Here, crystallization at each pressure was found to progress in two stages. In the first stage, α-Fe precipitates and in the second Fe2B forms while α-Fe continues to crystallize. Complementary high pressure room temperature studies were conducted.
- Authors:
-
- Univ. of Alabama, Birmingham, AL (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Sponsoring Org.:
- National Science Foundation (NSF); USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division
- OSTI Identifier:
- 1440609
- Alternate Identifier(s):
- OSTI ID: 1439763
- Grant/Contract Number:
- DMR-1608682; NA0001974; AC02-06CH11357
- Resource Type:
- Journal Article: Accepted Manuscript
- Journal Name:
- Journal of Applied Physics
- Additional Journal Information:
- Journal Volume: 123; Journal Issue: 21; Journal ID: ISSN 0021-8979
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- ENGLISH
- Subject:
- 36 MATERIALS SCIENCE; Crystallography; Metal oxides; Chemical elements; Glassy dynamics; Amorphous materials; Diffraction; Transition metals; Scanning electron microscopy; Alloys; X-rays
Citation Formats
Stemshorn, Andrew K., Vohra, Yogesh K., and Smith, Spencer J. High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization. United States: N. p., 2018.
Web. doi:10.1063/1.5024941.
Stemshorn, Andrew K., Vohra, Yogesh K., & Smith, Spencer J. High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization. United States. https://doi.org/10.1063/1.5024941
Stemshorn, Andrew K., Vohra, Yogesh K., and Smith, Spencer J. 2018.
"High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization". United States. https://doi.org/10.1063/1.5024941. https://www.osti.gov/servlets/purl/1440609.
@article{osti_1440609,
title = {High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization},
author = {Stemshorn, Andrew K. and Vohra, Yogesh K. and Smith, Spencer J.},
abstractNote = {Changes in bulk crystallization behavior following devitrification at high pressure are investigated for a Fe78B13Si9 composition metallic glass using in-situ energy dispersive x-ray powder diffraction. Crystallization with time was evaluated for a series of measurements to a maximum pressure of 5.63 ± 0.15 GPa for the Fe78B13Si9 glass. Pressure was found to strongly affect onset bulk crystallization temperature Tx. Here, crystallization at each pressure was found to progress in two stages. In the first stage, α-Fe precipitates and in the second Fe2B forms while α-Fe continues to crystallize. Complementary high pressure room temperature studies were conducted.},
doi = {10.1063/1.5024941},
url = {https://www.osti.gov/biblio/1440609},
journal = {Journal of Applied Physics},
issn = {0021-8979},
number = 21,
volume = 123,
place = {United States},
year = {Thu May 31 00:00:00 EDT 2018},
month = {Thu May 31 00:00:00 EDT 2018}
}
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