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Title: Heteronuclear Correlation SSNMR Spectroscopy with Indirect Detection under Fast Magic-Angle Spinning [Book Chapter]

Abstract

The main focus of this chapter is to address experimental strategies on the subject by providing a hands-on guide to fast MAS experiments, with a particular focus on indirect detection. Although our experience is limited to our respective laboratories in Ames and Yokohama, we hope that our descriptions of experimental setups and optimization procedures are sufficiently general to be applicable to all modern instruments. The chapter is organized as follows. Section 2 below introduces briefly the fast MAS technology and its main advantages. In Section 3, we describe the hardware associated with this remarkable technology and provide practical advices on its use, including procedures for loading and unloading the samples, maintaining the probe, reducing t 1 noise, etc. In Section 4, we describe the principles and hands-on aspects of experiments involving the indirect detection of spin-1/2 and 14N nuclei

Authors:
 [1];  [1];  [1]
  1. Ames Laboratory (AMES), Ames, IA (United States)
Publication Date:
Research Org.:
Ames Laboratory (AMES), Ames, IA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1415040
Report Number(s):
IS-B-5216
DOE Contract Number:
AC02-07CH11358
Resource Type:
Book
Resource Relation:
Related Information: In: Modern Methods in Solid-state NMR: A Practitioner's Guide, 2018, ISBN 978-1-78262-854-5 (see http://pubs.rsc.org/en/content/ebook/978-1-78262-854-5 )
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY

Citation Formats

Kobayshi, Takeshi, Nishiyama, Yusuke, and Pruski, Marek. Heteronuclear Correlation SSNMR Spectroscopy with Indirect Detection under Fast Magic-Angle Spinning [Book Chapter]. United States: N. p., 2018. Web.
Kobayshi, Takeshi, Nishiyama, Yusuke, & Pruski, Marek. Heteronuclear Correlation SSNMR Spectroscopy with Indirect Detection under Fast Magic-Angle Spinning [Book Chapter]. United States.
Kobayshi, Takeshi, Nishiyama, Yusuke, and Pruski, Marek. Mon . "Heteronuclear Correlation SSNMR Spectroscopy with Indirect Detection under Fast Magic-Angle Spinning [Book Chapter]". United States. doi:.
@article{osti_1415040,
title = {Heteronuclear Correlation SSNMR Spectroscopy with Indirect Detection under Fast Magic-Angle Spinning [Book Chapter]},
author = {Kobayshi, Takeshi and Nishiyama, Yusuke and Pruski, Marek},
abstractNote = {The main focus of this chapter is to address experimental strategies on the subject by providing a hands-on guide to fast MAS experiments, with a particular focus on indirect detection. Although our experience is limited to our respective laboratories in Ames and Yokohama, we hope that our descriptions of experimental setups and optimization procedures are sufficiently general to be applicable to all modern instruments. The chapter is organized as follows. Section 2 below introduces briefly the fast MAS technology and its main advantages. In Section 3, we describe the hardware associated with this remarkable technology and provide practical advices on its use, including procedures for loading and unloading the samples, maintaining the probe, reducing t1 noise, etc. In Section 4, we describe the principles and hands-on aspects of experiments involving the indirect detection of spin-1/2 and 14N nuclei},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Mon Jan 01 00:00:00 EST 2018},
month = {Mon Jan 01 00:00:00 EST 2018}
}

Book:
Other availability
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