Devices and process for high-pressure magic angle spinning nuclear magnetic resonance

Hoyt, David W.; Sears, Jesse A.; Turcu, Romulus V. F.; Rosso, Kevin M.; Hu, Jian Zhi

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance

Patent · 04 December 2017

OSTI ID:1411403

Hoyt, David W.; Sears, Jesse A.; Turcu, Romulus V. F.; Rosso, Kevin M.; Hu, Jian Zhi

A high-pressure magic angle spinning (MAS) rotor is detailed that includes a high-pressure sample cell that maintains high pressures exceeding 150 bar. The sample cell design minimizes pressure losses due to penetration over an extended period of time.

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Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC05-76RL01830

Assignee:: Battelle Memorial Institute (Richland, WA)

Patent Number(s):: 9,835,698

Application Number:: 14/165,215

OSTI ID:: 1411403

Country of Publication:: United States

Language:: English

References (14)

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High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning Sakellariou, D.; Goff, G. Le; Jacquinot, J.-F. Nature, Vol. 447, Issue 7145, p. 694-697 https://doi.org/10.1038/nature05897	journal	June 2007
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Chemistry in superacids. 12. Carbonic acid and its mono- and diprotonation: NMR, ab initio, and IGLO investigation Rasul, Golam; Reddy, V. Prakash; Zdunek, Leszek Z. Journal of the American Chemical Society, Vol. 115, Issue 6, p. 2236-2238 https://doi.org/10.1021/ja00059a020	journal	March 1993
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¹³C High-Pressure CPMAS NMR Characterization of the Molecular Motion of Polystyrene Plasticized by CO₂ Gas Miyoshi, Toshikazu; Takegoshi, K.; Terao, Takehiko Macromolecules, Vol. 30, Issue 21, p. 6582-6585 https://doi.org/10.1021/ma961891r	journal	October 1997
High-pressure magic angle spinning nuclear magnetic resonance Hoyt, David W.; Turcu, Romulus V. F.; Sears, Jesse A. Journal of Magnetic Resonance, Vol. 212, Issue 2, p. 378-385 https://doi.org/10.1016/j.jmr.2011.07.019	journal	October 2011
Microcoil High-Resolution Magic Angle Spinning NMR Spectroscop Janssen, Hans; Brinkmann, Andreas; van Eck, Ernst R. H. Journal of the American Chemical Society, Vol. 128, Issue 27, p. 8722-8723 https://doi.org/10.1021/ja061350+		June 2006
Metal Carbonation of Forsterite in Supercritical CO₂ and H₂O Using Solid State ²⁹Si, ¹³C NMR Spectroscopy Kwak, Ja Hun; Hu, Jian Zhi; Hoyt, David W. The Journal of Physical Chemistry C, Vol. 114, Issue 9, p. 4126-4134 https://doi.org/10.1021/jp1001308	journal	February 2010
¹²⁹Xe n.m.r. study of free volume and phase separation of the polystyrene/poly(vinyl methyl ether) blend Miyoshi, Toshikazu; Takegoshi, K.; Terao, Takehiko Polymer, Vol. 38, Issue 21, p. 5475-5480 https://doi.org/10.1016/S0032-3861(97)00086-4	journal	October 1997
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Nuclear Induction Bloch, F.; Hansen, W. W.; Packard, Martin Physical Review, Vol. 69, Issue 3-4, p. 127-127 https://doi.org/10.1103/PhysRev.69.127	journal	February 1946

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