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Title: Uncertainty propagation for the coulometric measurement of the plutonium concentration in CRM126 solution provided by JAEA

Abstract

This GUM WorkbenchTM propagation of uncertainty is for the coulometric measurement of the plutonium concentration in a Pu standard material (C126) supplied as individual aliquots that were prepared by mass. The C126 solution had been prepared and as aliquoted as standard material. Samples are aliquoted into glass vials and heated to dryness for distribution as dried nitrate. The individual plutonium aliquots were not separated chemically or otherwise purified prior to measurement by coulometry in the F/H Laboratory. Hydrogen peroxide was used for valence adjustment.

Authors:
 [1]
  1. Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)
Publication Date:
Research Org.:
Savannah River Site (SRS), Aiken, SC (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1407930
Report Number(s):
SRNL-L4600-2017-00085
TRN: US1800030
DOE Contract Number:
AC09-08SR22470
Resource Type:
Technical Report
Country of Publication:
United States
Language:
English
Subject:
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS; PLUTONIUM; SOLUTIONS; CONCENTRATION RATIO; JAEA

Citation Formats

Morales-Arteaga, Maria. Uncertainty propagation for the coulometric measurement of the plutonium concentration in CRM126 solution provided by JAEA. United States: N. p., 2017. Web. doi:10.2172/1407930.
Morales-Arteaga, Maria. Uncertainty propagation for the coulometric measurement of the plutonium concentration in CRM126 solution provided by JAEA. United States. doi:10.2172/1407930.
Morales-Arteaga, Maria. Tue . "Uncertainty propagation for the coulometric measurement of the plutonium concentration in CRM126 solution provided by JAEA". United States. doi:10.2172/1407930. https://www.osti.gov/servlets/purl/1407930.
@article{osti_1407930,
title = {Uncertainty propagation for the coulometric measurement of the plutonium concentration in CRM126 solution provided by JAEA},
author = {Morales-Arteaga, Maria},
abstractNote = {This GUM WorkbenchTM propagation of uncertainty is for the coulometric measurement of the plutonium concentration in a Pu standard material (C126) supplied as individual aliquots that were prepared by mass. The C126 solution had been prepared and as aliquoted as standard material. Samples are aliquoted into glass vials and heated to dryness for distribution as dried nitrate. The individual plutonium aliquots were not separated chemically or otherwise purified prior to measurement by coulometry in the F/H Laboratory. Hydrogen peroxide was used for valence adjustment.},
doi = {10.2172/1407930},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Nov 07 00:00:00 EST 2017},
month = {Tue Nov 07 00:00:00 EST 2017}
}

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