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Title: Fiducial marker application method for position alignment of in situ multimodal X-ray experiments and reconstructions

Abstract

An evolving suite of X-ray characterization methods are presently available to the materials community, providing a great opportunity to gain new insight into material behavior and provide critical validation data for materials models. Two critical and related issues are sample repositioning during anin situexperiment and registration of multiple data sets after the experiment. To address these issues, a method is described which utilizes a focused ion-beam scanning electron microscope equipped with a micromanipulator to apply gold fiducial markers to samples for X-ray measurements. The method is demonstrated with a synchrotron X-ray experiment involvingin situloading of a titanium alloy tensile specimen.

Authors:
 [1];  [2];  [3];  [4];  [4];  [2];  [5];  [1]
  1. Air Force Research Lab. (AFRL), Wright-Patterson AFB, OH (United States)
  2. Carnegie Mellon Univ., Pittsburgh, PA (United States)
  3. Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
  4. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
  5. Air Force Research Lab. (AFRL), Wright-Patterson AFB, OH (United States); Nutonian Inc., Somerville, MA (United States)
Publication Date:
Research Org.:
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1399703
Report Number(s):
LLNL-JRNL-738585
Journal ID: ISSN 1600-5767; JACGAR; TRN: US1702969
Grant/Contract Number:  
AC52-07NA27344
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
Journal of Applied Crystallography (Online)
Additional Journal Information:
Journal Name: Journal of Applied Crystallography (Online); Journal Volume: 49; Journal Issue: 2; Journal ID: ISSN 1600-5767
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
42 ENGINEERING; 36 MATERIALS SCIENCE; 47 OTHER INSTRUMENTATION; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats

Shade, Paul A., Menasche, David B., Bernier, Joel V., Kenesei, Peter, Park, Jun-Sang, Suter, Robert M., Schuren, Jay C., and Turner, Todd J.. Fiducial marker application method for position alignment of in situ multimodal X-ray experiments and reconstructions. United States: N. p., 2016. Web. doi:10.1107/S1600576716001989.
Shade, Paul A., Menasche, David B., Bernier, Joel V., Kenesei, Peter, Park, Jun-Sang, Suter, Robert M., Schuren, Jay C., & Turner, Todd J.. Fiducial marker application method for position alignment of in situ multimodal X-ray experiments and reconstructions. United States. doi:10.1107/S1600576716001989.
Shade, Paul A., Menasche, David B., Bernier, Joel V., Kenesei, Peter, Park, Jun-Sang, Suter, Robert M., Schuren, Jay C., and Turner, Todd J.. Tue . "Fiducial marker application method for position alignment of in situ multimodal X-ray experiments and reconstructions". United States. doi:10.1107/S1600576716001989. https://www.osti.gov/servlets/purl/1399703.
@article{osti_1399703,
title = {Fiducial marker application method for position alignment of in situ multimodal X-ray experiments and reconstructions},
author = {Shade, Paul A. and Menasche, David B. and Bernier, Joel V. and Kenesei, Peter and Park, Jun-Sang and Suter, Robert M. and Schuren, Jay C. and Turner, Todd J.},
abstractNote = {An evolving suite of X-ray characterization methods are presently available to the materials community, providing a great opportunity to gain new insight into material behavior and provide critical validation data for materials models. Two critical and related issues are sample repositioning during anin situexperiment and registration of multiple data sets after the experiment. To address these issues, a method is described which utilizes a focused ion-beam scanning electron microscope equipped with a micromanipulator to apply gold fiducial markers to samples for X-ray measurements. The method is demonstrated with a synchrotron X-ray experiment involvingin situloading of a titanium alloy tensile specimen.},
doi = {10.1107/S1600576716001989},
journal = {Journal of Applied Crystallography (Online)},
number = 2,
volume = 49,
place = {United States},
year = {Tue Mar 01 00:00:00 EST 2016},
month = {Tue Mar 01 00:00:00 EST 2016}
}

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Cited by: 6 works
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Works referenced in this record:

An introduction to three-dimensional X-ray diffraction microscopy
journal, October 2012