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Title: Building with ions: towards direct write of platinum nanostructures using in situ liquid cell helium ion microscopy

Abstract

Direct write with liquid precursor using an helium ion beam, allows fabrication of nanostructures with sub-15 nm resolution and high chemical purity.

Authors:
ORCiD logo [1]; ORCiD logo [1];  [1];  [2];  [1];  [3]; ORCiD logo [1];  [1]; ORCiD logo [1];  [1]
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States); The Proctor and Gamble Company Winton Hill Business Center, Cincinnati, OH (United States)
  3. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States)
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Oak Ridge Leadership Computing Facility (OLCF)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
1394460
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
Nanoscale
Additional Journal Information:
Journal Volume: 9; Journal Issue: 35; Journal ID: ISSN 2040-3364
Publisher:
Royal Society of Chemistry
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY

Citation Formats

Ievlev, Anton V., Jakowski, Jacek, Burch, Matthew J., Iberi, Vighter, Hysmith, Holland, Joy, David C., Sumpter, Bobby G., Belianinov, Alex, Unocic, Raymond R., and Ovchinnikova, Olga S. Building with ions: towards direct write of platinum nanostructures using in situ liquid cell helium ion microscopy. United States: N. p., 2017. Web. doi:10.1039/c7nr04417h.
Ievlev, Anton V., Jakowski, Jacek, Burch, Matthew J., Iberi, Vighter, Hysmith, Holland, Joy, David C., Sumpter, Bobby G., Belianinov, Alex, Unocic, Raymond R., & Ovchinnikova, Olga S. Building with ions: towards direct write of platinum nanostructures using in situ liquid cell helium ion microscopy. United States. doi:10.1039/c7nr04417h.
Ievlev, Anton V., Jakowski, Jacek, Burch, Matthew J., Iberi, Vighter, Hysmith, Holland, Joy, David C., Sumpter, Bobby G., Belianinov, Alex, Unocic, Raymond R., and Ovchinnikova, Olga S. Wed . "Building with ions: towards direct write of platinum nanostructures using in situ liquid cell helium ion microscopy". United States. doi:10.1039/c7nr04417h. https://www.osti.gov/servlets/purl/1394460.
@article{osti_1394460,
title = {Building with ions: towards direct write of platinum nanostructures using in situ liquid cell helium ion microscopy},
author = {Ievlev, Anton V. and Jakowski, Jacek and Burch, Matthew J. and Iberi, Vighter and Hysmith, Holland and Joy, David C. and Sumpter, Bobby G. and Belianinov, Alex and Unocic, Raymond R. and Ovchinnikova, Olga S.},
abstractNote = {Direct write with liquid precursor using an helium ion beam, allows fabrication of nanostructures with sub-15 nm resolution and high chemical purity.},
doi = {10.1039/c7nr04417h},
journal = {Nanoscale},
issn = {2040-3364},
number = 35,
volume = 9,
place = {United States},
year = {2017},
month = {8}
}

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Cited by: 4 works
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Works referenced in this record:

Programmable Nano-Bio Interfaces for Functional Biointegrated Devices
journal, April 2017

  • Cai, Pingqiang; Leow, Wan Ru; Wang, Xiaoyuan
  • Advanced Materials, Vol. 29, Issue 26
  • DOI: 10.1002/adma.201605529

Focused, Nanoscale Electron-Beam-Induced Deposition and Etching
journal, September 2006

  • Randolph, S. J.; Fowlkes, J. D.; Rack, P. D.
  • Critical Reviews in Solid State and Materials Sciences, Vol. 31, Issue 3
  • DOI: 10.1080/10408430600930438

Implementation and benchmark tests of the DFTB method and its application in the ONIOM method
journal, January 2009

  • Zheng, Guishan; Lundberg, Marcus; Jakowski, Jacek
  • International Journal of Quantum Chemistry, Vol. 109, Issue 9
  • DOI: 10.1002/qua.22002

The effect of local substrate motion on quantum hydrogen transfer in soybean lipoxygenase-1 modeled with QTES-DFTB dynamics
journal, October 2014


Fundamental Proximity Effects in Focused Electron Beam Induced Deposition
journal, December 2011

  • Plank, Harald; Smith, Daryl A.; Haber, Thomas
  • ACS Nano, Vol. 6, Issue 1
  • DOI: 10.1021/nn204237h

The Optical Properties of Metal Nanoparticles:  The Influence of Size, Shape, and Dielectric Environment
journal, January 2003

  • Kelly, K. Lance; Coronado, Eduardo; Zhao, Lin Lin
  • The Journal of Physical Chemistry B, Vol. 107, Issue 3
  • DOI: 10.1021/jp026731y

Gas-assisted focused electron beam and ion beam processing and fabrication
journal, January 2008

  • Utke, Ivo; Hoffmann, Patrik; Melngailis, John
  • Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures, Vol. 26, Issue 4
  • DOI: 10.1116/1.2955728

Aqueous Two-Phase System-Derived Biofilms for Bacterial Interaction Studies
journal, August 2012

  • Yaguchi, Toshiyuki; Dwidar, Mohammed; Byun, Chang Kyu
  • Biomacromolecules, Vol. 13, Issue 9
  • DOI: 10.1021/bm300500y

Helium ion microscope: A new tool for nanoscale microscopy and metrology
journal, January 2006

  • Ward, B. W.; Notte, John A.; Economou, N. P.
  • Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures, Vol. 24, Issue 6
  • DOI: 10.1116/1.2357967

Time-dependent quantum dynamical simulations of C 2 condensation under extreme conditions
journal, January 2012

  • Jakowski, Jacek; Irle, Stephan; Morokuma, Keiji
  • Phys. Chem. Chem. Phys., Vol. 14, Issue 18
  • DOI: 10.1039/C1CP22035G

A Study of Helium Ion Beam Substrate Interaction Volume on Nanomachining Profiles in Bulk Substrates and Thin Film Membranes
journal, July 2012


Electron-Beam-Induced Deposition of Platinum from a Liquid Precursor
journal, July 2009

  • Donev, Eugenii U.; Hastings, J. Todd
  • Nano Letters, Vol. 9, Issue 7
  • DOI: 10.1021/nl9012216

Bubble and Pattern Formation in Liquid Induced by an Electron Beam
journal, December 2013

  • Grogan, Joseph M.; Schneider, Nicholas M.; Ross, Frances M.
  • Nano Letters, Vol. 14, Issue 1
  • DOI: 10.1021/nl404169a

Controlled Growth of Nanoparticles from Solution with In Situ Liquid Transmission Electron Microscopy
journal, July 2011

  • Evans, James E.; Jungjohann, Katherine L.; Browning, Nigel D.
  • Nano Letters, Vol. 11, Issue 7
  • DOI: 10.1021/nl201166k

Shape control of CdSe nanocrystals
journal, March 2000

  • Peng, Xiaogang; Manna, Liberato; Yang, Weidong
  • Nature, Vol. 404, Issue 6773, p. 59-61
  • DOI: 10.1038/35003535

Observation of Single Colloidal Platinum Nanocrystal Growth Trajectories
journal, June 2009


A nanoscale three-dimensional Monte Carlo simulation of electron-beam-induced deposition with gas dynamics
journal, June 2007


Modeling Charge Transfer in Fullerene Collisions via Real-Time Electron Dynamics
journal, May 2012

  • Jakowski, Jacek; Irle, Stephan; Sumpter, Bobby G.
  • The Journal of Physical Chemistry Letters, Vol. 3, Issue 11
  • DOI: 10.1021/jz3004377

Liouville–von Neumann molecular dynamics
journal, June 2009

  • Jakowski, Jacek; Morokuma, Keiji
  • The Journal of Chemical Physics, Vol. 130, Issue 22
  • DOI: 10.1063/1.3152120

Water Radiolysis: Influence of Oxide Surfaces on H2 Production under Ionizing Radiation
journal, February 2011


Self-consistent-charge density-functional tight-binding method for simulations of complex materials properties
journal, September 1998

  • Elstner, M.; Porezag, D.; Jungnickel, G.
  • Physical Review B, Vol. 58, Issue 11, p. 7260-7268
  • DOI: 10.1103/PhysRevB.58.7260

Direct in Situ Determination of the Mechanisms Controlling Nanoparticle Nucleation and Growth
journal, September 2012

  • Woehl, Taylor J.; Evans, James E.; Arslan, Ilke
  • ACS Nano, Vol. 6, Issue 10
  • DOI: 10.1021/nn303371y

Microfluidic Confinement of Single Cells of Bacteria in Small Volumes Initiates High-Density Behavior of Quorum Sensing and Growth and Reveals Its Variability
journal, July 2009

  • Boedicker, James Q.; Vincent, Meghan E.; Ismagilov, Rustem F.
  • Angewandte Chemie International Edition, Vol. 48, Issue 32
  • DOI: 10.1002/anie.200901550

Applications of magnetic nanoparticles in biomedicine
journal, June 2003

  • Pankhurst, Q. A.; Connolly, J.; Jones, S. K.
  • Journal of Physics D: Applied Physics, Vol. 36, Issue 13
  • DOI: 10.1088/0022-3727/36/13/201

Factors influencing quantitative liquid (scanning) transmission electron microscopy
journal, January 2014

  • Abellan, P.; Woehl, T. J.; Parent, L. R.
  • Chem. Commun., Vol. 50, Issue 38
  • DOI: 10.1039/C3CC48479C

In Situ Mitigation of Subsurface and Peripheral Focused Ion Beam Damage via Simultaneous Pulsed Laser Heating
journal, February 2016


Direct-write liquid phase transformations with a scanning transmission electron microscope
journal, January 2016

  • Unocic, Raymond R.; Lupini, Andrew R.; Borisevich, Albina Y.
  • Nanoscale, Vol. 8, Issue 34
  • DOI: 10.1039/C6NR04994J

Synthesis and surface engineering of iron oxide nanoparticles for biomedical applications
journal, June 2005


Highly conductive and pure gold nanostructures grown by electron beam induced deposition
journal, September 2016

  • Shawrav, Mostafa M.; Taus, Philipp; Wanzenboeck, Heinz D.
  • Scientific Reports, Vol. 6, Issue 1
  • DOI: 10.1038/srep34003

Electron–Water Interactions and Implications for Liquid Cell Electron Microscopy
journal, September 2014

  • Schneider, Nicholas M.; Norton, Michael M.; Mendel, Brian J.
  • The Journal of Physical Chemistry C, Vol. 118, Issue 38
  • DOI: 10.1021/jp507400n

Anchoring Semiconductor and Metal Nanoparticles on a Two-Dimensional Catalyst Mat. Storing and Shuttling Electrons with Reduced Graphene Oxide
journal, February 2010

  • Lightcap, Ian V.; Kosel, Thomas H.; Kamat, Prashant V.
  • Nano Letters, Vol. 10, Issue 2
  • DOI: 10.1021/nl9035109

3D printing of microscopic bacterial communities
journal, October 2013

  • Connell, J. L.; Ritschdorff, E. T.; Whiteley, M.
  • Proceedings of the National Academy of Sciences, Vol. 110, Issue 46
  • DOI: 10.1073/pnas.1309729110

Electrochemical Properties of Carbon Nanoparticles Entrapped in a Silica Matrix
journal, January 2008

  • Bok, Sangho; Lubguban, Arnold A.; Gao, Yuanfang
  • Journal of The Electrochemical Society, Vol. 155, Issue 5
  • DOI: 10.1149/1.2868772

Directing Matter: Toward Atomic-Scale 3D Nanofabrication
journal, May 2016


Binding energies, lifetimes and implications of bulk and interface solvated electrons in water
journal, March 2010

  • Siefermann, Katrin R.; Liu, Yaxing; Lugovoy, Evgeny
  • Nature Chemistry, Vol. 2, Issue 4
  • DOI: 10.1038/nchem.580

Radiolysis of Neutral Water by Cyclotron Produced Deuterons and Helium Ions 1
journal, April 1959

  • Schwarz, Harold A.; Caffrey, James M.; Scholes, George
  • Journal of the American Chemical Society, Vol. 81, Issue 8
  • DOI: 10.1021/ja01517a008

Quantum Trajectory-Electronic Structure Approach for Exploring Nuclear Effects in the Dynamics of Nanomaterials
journal, November 2013

  • Garashchuk, Sophya; Jakowski, Jacek; Wang, Lei
  • Journal of Chemical Theory and Computation, Vol. 9, Issue 12
  • DOI: 10.1021/ct4006147

Quantitative Description of Crystal Nucleation and Growth from in Situ Liquid Scanning Transmission Electron Microscopy
journal, October 2015


Quantum Dot Solar Cells. Harvesting Light Energy with CdSe Nanocrystals Molecularly Linked to Mesoscopic TiO 2 Films
journal, February 2006

  • Robel, István; Subramanian, Vaidyanathan; Kuno, Masaru
  • Journal of the American Chemical Society, Vol. 128, Issue 7
  • DOI: 10.1021/ja056494n

Nanoparticles as Recyclable Catalysts: The Frontier between Homogeneous and Heterogeneous Catalysis
journal, December 2005

  • Astruc, Didier; Lu, Feng; Aranzaes, Jaime Ruiz
  • Angewandte Chemie International Edition, Vol. 44, Issue 48
  • DOI: 10.1002/anie.200500766

Confinement-induced quorum sensing of individual Staphylococcus aureus bacteria
journal, November 2009

  • Carnes, Eric C.; Lopez, DeAnna M.; Donegan, Niles P.
  • Nature Chemical Biology, Vol. 6, Issue 1
  • DOI: 10.1038/nchembio.264

Substrate effects on the electron-beam-induced deposition of platinum from a liquid precursor
journal, January 2011

  • Donev, Eugenii U.; Schardein, Gregory; Wright, John C.
  • Nanoscale, Vol. 3, Issue 7
  • DOI: 10.1039/c1nr10026b

Spatial resolution limits in electron-beam-induced deposition
journal, October 2005

  • Silvis-Cividjian, N.; Hagen, C. W.; Kruit, P.
  • Journal of Applied Physics, Vol. 98, Issue 8
  • DOI: 10.1063/1.2085307