skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: In situ observation of fracture processes in high-strength concretes and limestone using high-speed X-ray phase-contrast imaging

Journal Article · · Philosophical Transactions of the Royal Society. A, Mathematical, Physical and Engineering Sciences

The mechanical properties and fracture mechanisms of geomaterials and construction materials such as concrete are reported to be dependent on the loading rates. However, the in situ cracking inside such specimens cannot be visualized using traditional optical imaging methods since the materials are opaque. In this study, the in situ sub-surface failure/damage mechanisms in Cor-Tuf (a reactive powder concrete), a high-strength concrete (HSC) and Indiana limestone under dynamic loading were investigated using high-speed synchrotron X-ray phase-contrast imaging. Dynamic compressive loading was applied using a modified Kolsky bar and fracture images were recorded using a synchronized high-speed synchrotron X-ray imaging set-up. Three-dimensional synchrotron X-ray tomography was also performed to record the microstructure of the specimens before dynamic loading. In the Cor-Tuf and HSC specimens, two different modes of cracking were observed: straight cracking or angular cracking with respect to the direction of loading. In limestone, cracks followed the grain boundaries and voids, ultimately fracturing the specimen. Cracks in HSC were more tortuous than the cracks in Cor-Tuf specimens. The effects of the microstructure on the observed cracking behaviour are discussed. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’.

Research Organization:
Argonne National Laboratory (ANL), Argonne, IL (United States)
Sponsoring Organization:
USDOE Office of Science (SC)
DOE Contract Number:
AC02-06CH11357
OSTI ID:
1393945
Journal Information:
Philosophical Transactions of the Royal Society. A, Mathematical, Physical and Engineering Sciences, Vol. 375, Issue 2085; ISSN 1364-503X
Publisher:
The Royal Society Publishing
Country of Publication:
United States
Language:
English

References (18)

In-line holography and phase-contrast microtomography with high energy x-rays journal January 1999
TomoPy: a framework for the analysis of synchrotron tomographic data journal August 2014
Observation of Crack Propagation in Glass Using X-ray Phase Contrast Imaging journal October 2014
On the tortuosity of the fracture surface in concrete journal May 1997
Rate Effects in Uniaxial Dynamic Compression of Concrete journal January 1992
Feasibility study of propagation-based phase-contrast X-ray lung imaging on the Imaging and Medical beamline at the Australian Synchrotron journal January 2014
New pulverization parameter derived from indentation and dynamic compression of brittle microspheres journal October 2015
Phase-contrast imaging using polychromatic hard X-rays journal November 1996
Impact Behavior of Plain Concrete Loaded in Uniaxial Compression journal June 1995
Micromechanics of inelastic compaction in two allochemical limestones journal October 2012
In Situ Visual Observation of Fracture Processes in Several High-Performance Fibers journal February 2015
A Fracture toughness criterion for concrete journal January 1985
Crack classification in concrete based on acoustic emission journal December 2010
In situ damage assessment using synchrotron X-rays in materials loaded by a Hopkinson bar
  • Chen, Weinong W.; Hudspeth, Matthew C.; Claus, Ben
  • Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences, Vol. 372, Issue 2015 https://doi.org/10.1098/rsta.2013.0191
journal May 2014
The damage mechanics of brittle solids in compression journal May 1990
Experimental assessment of fracture of individual sand particles at different loading rates journal June 2014
High speed synchrotron x-ray phase contrast imaging of dynamic material response to split Hopkinson bar loading journal February 2013
NIH Image to ImageJ: 25 years of image analysis journal June 2012