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Title: Correlation of Thermally Induced Pores with Microstructural Features Using High Energy X-rays

Abstract

Combined application of a near-field High Energy Diffraction Microscopy measurement of crystal lattice orientation fields and a tomographic measurement of pore distributions in a sintered nickel-based superalloy sample allows pore locations to be correlated with microstructural features. Measurements were carried out at the Advanced Photon Source beamline 1-ID using an X-ray energy of 65 keV for each of the measurement modes. The nickel superalloy sample was prepared in such a way as to generate significant thermally induced porosity. A three-dimensionally resolved orientation map is directly overlaid with the tomographically determined pore map through a careful registration procedure. The data are shown to reliably reproduce the expected correlations between specific microstructural features (triple lines and quadruple nodes) and pore positions. With the statistics afforded by the 3D data set, we conclude that within statistical limits, pore formation does not depend on the relative orientations of the grains. The experimental procedures and analysis tools illustrated are being applied to a variety of materials problems in which local heterogeneities can affect materials properties.

Authors:
; ; ; ; ; ; ;
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
Air Force Research Laboratory (AFRL); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
OSTI Identifier:
1392466
DOE Contract Number:
AC02-06CH11357
Resource Type:
Journal Article
Resource Relation:
Journal Name: Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science; Journal Volume: 47; Journal Issue: 11
Country of Publication:
United States
Language:
English

Citation Formats

Menasche, David B., Shade, Paul A., Lind, Jonathan, Li, Shiu Fai, Bernier, Joel V., Kenesei, Peter, Schuren, Jay C., and Suter, Robert M. Correlation of Thermally Induced Pores with Microstructural Features Using High Energy X-rays. United States: N. p., 2016. Web. doi:10.1007/s11661-016-3712-3.
Menasche, David B., Shade, Paul A., Lind, Jonathan, Li, Shiu Fai, Bernier, Joel V., Kenesei, Peter, Schuren, Jay C., & Suter, Robert M. Correlation of Thermally Induced Pores with Microstructural Features Using High Energy X-rays. United States. doi:10.1007/s11661-016-3712-3.
Menasche, David B., Shade, Paul A., Lind, Jonathan, Li, Shiu Fai, Bernier, Joel V., Kenesei, Peter, Schuren, Jay C., and Suter, Robert M. Mon . "Correlation of Thermally Induced Pores with Microstructural Features Using High Energy X-rays". United States. doi:10.1007/s11661-016-3712-3.
@article{osti_1392466,
title = {Correlation of Thermally Induced Pores with Microstructural Features Using High Energy X-rays},
author = {Menasche, David B. and Shade, Paul A. and Lind, Jonathan and Li, Shiu Fai and Bernier, Joel V. and Kenesei, Peter and Schuren, Jay C. and Suter, Robert M.},
abstractNote = {Combined application of a near-field High Energy Diffraction Microscopy measurement of crystal lattice orientation fields and a tomographic measurement of pore distributions in a sintered nickel-based superalloy sample allows pore locations to be correlated with microstructural features. Measurements were carried out at the Advanced Photon Source beamline 1-ID using an X-ray energy of 65 keV for each of the measurement modes. The nickel superalloy sample was prepared in such a way as to generate significant thermally induced porosity. A three-dimensionally resolved orientation map is directly overlaid with the tomographically determined pore map through a careful registration procedure. The data are shown to reliably reproduce the expected correlations between specific microstructural features (triple lines and quadruple nodes) and pore positions. With the statistics afforded by the 3D data set, we conclude that within statistical limits, pore formation does not depend on the relative orientations of the grains. The experimental procedures and analysis tools illustrated are being applied to a variety of materials problems in which local heterogeneities can affect materials properties.},
doi = {10.1007/s11661-016-3712-3},
journal = {Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science},
number = 11,
volume = 47,
place = {United States},
year = {Mon Aug 29 00:00:00 EDT 2016},
month = {Mon Aug 29 00:00:00 EDT 2016}
}