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Title: Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics

Abstract

Fabrication and results of high-resolution X-ray topography characterization of diamond single-crystal plates with large surface area (10 mm × 10 mm) and (111) crystal surface orientation for applications in high-heat-load X-ray crystal optics are reported. The plates were fabricated by laser-cutting of the (111) facets of diamond crystals grown using high-pressure high-temperature methods. The intrinsic crystal quality of a selected 3 mm × 7 mm crystal region of one of the studied samples was found to be suitable for applications in wavefront-preserving high-heat-load crystal optics. Wavefront characterization was performed using sequential X-ray diffraction topography in the pseudo plane wave configuration and data analysis using rocking-curve topography. In conclusion, the variations of the rocking-curve width and peak position measured with a spatial resolution of 13 µm × 13 µm over the selected region were found to be less than 1 µrad.

Authors:
 [1];  [2];  [2];  [3];  [3]
  1. Argonne National Lab. (ANL), Argonne, IL (United States)
  2. Euclid Techlabs LLC, Solon, OH (United States)
  3. New Diamond Technology LLC, St. Petersburg (Russia)
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22), Scientific User Facilities Division; Argonne National Laboratory, Advanced Photon Source
OSTI Identifier:
1392112
Grant/Contract Number:  
AC02-06CH11357
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Volume: 23; Journal Issue: 5; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; X-ray monochromator; high heat load; diamond crystal; wavefront preservation

Citation Formats

Stoupin, Stanislav, Antipov, Sergey, Butler, James E., Kolyadin, Alexander V., and Katrusha, Andrey. Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics. United States: N. p., 2016. Web. doi:10.1107/S1600577516011796.
Stoupin, Stanislav, Antipov, Sergey, Butler, James E., Kolyadin, Alexander V., & Katrusha, Andrey. Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics. United States. https://doi.org/10.1107/S1600577516011796
Stoupin, Stanislav, Antipov, Sergey, Butler, James E., Kolyadin, Alexander V., and Katrusha, Andrey. Wed . "Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics". United States. https://doi.org/10.1107/S1600577516011796. https://www.osti.gov/servlets/purl/1392112.
@article{osti_1392112,
title = {Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics},
author = {Stoupin, Stanislav and Antipov, Sergey and Butler, James E. and Kolyadin, Alexander V. and Katrusha, Andrey},
abstractNote = {Fabrication and results of high-resolution X-ray topography characterization of diamond single-crystal plates with large surface area (10 mm × 10 mm) and (111) crystal surface orientation for applications in high-heat-load X-ray crystal optics are reported. The plates were fabricated by laser-cutting of the (111) facets of diamond crystals grown using high-pressure high-temperature methods. The intrinsic crystal quality of a selected 3 mm × 7 mm crystal region of one of the studied samples was found to be suitable for applications in wavefront-preserving high-heat-load crystal optics. Wavefront characterization was performed using sequential X-ray diffraction topography in the pseudo plane wave configuration and data analysis using rocking-curve topography. In conclusion, the variations of the rocking-curve width and peak position measured with a spatial resolution of 13 µm × 13 µm over the selected region were found to be less than 1 µrad.},
doi = {10.1107/S1600577516011796},
url = {https://www.osti.gov/biblio/1392112}, journal = {Journal of Synchrotron Radiation (Online)},
issn = {1600-5775},
number = 5,
volume = 23,
place = {United States},
year = {2016},
month = {8}
}

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Cited by: 3 works
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Works referenced in this record:

μm-resolved high resolution X-ray diffraction imaging for semiconductor quality control
journal, April 2000


Test of a high-heat-load double-crystal diamond monochromator at the Advanced Photon Source
journal, December 1997

  • Fernandez, P. B.; Graber, T.; Lee, W. -K
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 400, Issue 2-3
  • https://doi.org/10.1016/S0168-9002(97)01014-0

Multiple station beamline at an undulator X-ray source
journal, November 1994


Performance of a beam-multiplexing diamond crystal monochromator at the Linac Coherent Light Source
journal, June 2014


Large Defect-Free Synthetic Type IIa Diamond Crystals Synthesized via High Pressure and High Temperature
journal, September 2012


Strain mapping with parts-per-million resolution in synthetic type-Ib diamond plates
journal, November 2005


Diamond double-crystal monochromator at SPring-8
conference, October 2012


HPHT growth and x-ray characterization of high-quality type IIa diamond
journal, August 2009


All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source
journal, August 2014


Diamond Double-Crystal Monochromator for SPring-8 Undulator Beamlines
conference, January 2007

  • Yabashi, M.; Goto, S.; Shimizu, Y.
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings
  • https://doi.org/10.1063/1.2436212

Diamond crystal optics for self-seeding of hard X-rays in X-ray free-electron lasers
journal, March 2013


A diamond double‐crystal transmission monochromator for the TROIKA II station at ESRF
journal, September 1996