Small Angle X-ray Scattering for Nanoparticle Research

Li, Tao; Senesi, Andrew J.; Lee, Byeongdu

doi:10.1021/acs.chemrev.5b00690

Title: Small Angle X-ray Scattering for Nanoparticle Research

Journal Article · Thu Apr 07 00:00:00 EDT 2016 · Chemical Reviews

DOI:https://doi.org/10.1021/acs.chemrev.5b00690· OSTI ID:1391950

Li, Tao ^[1]; Senesi, Andrew J. ^[1]; Lee, Byeongdu ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States)

X-ray scattering is a structural characterization tool that has impacted diverse fields of study. It is unique in its ability to examine materials in real time and under realistic sample environments, enabling researchers to understand morphology at nanometer and ångström length scales using complementary small and wide angle X-ray scattering (SAXS, WAXS), respectively. Herein, we focus on the use of SAXS to examine nanoscale particulate systems. We provide a theoretical foundation for X-ray scattering, considering both form factor and structure factor, as well as the use of correlation functions, which may be used to determine a particle’s size, size distribution, shape, and organization into hierarchal structures. The theory is expanded upon with contemporary use cases. Both transmission and reflection (grazing incidence) geometries are addressed, as well the combination of SAXS with other X-ray and non-X ray characterization tools. Furthermore, we conclude with an examination of several key areas of research where X-rays scattering has played a pivotal role, including in situ nanoparticle synthesis, nanoparticle assembly, and in operando studies of catalysts and energy storage materials. Throughout this review we highlight the unique capabilities of X-ray scattering for structural characterization of materials in their native environment.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1391950

Journal Information:: Chemical Reviews, Vol. 116, Issue 18; ISSN 0009-2665

Publisher:: American Chemical SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 547 works

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Supraferromagnetic correlations in clusters of magnetic nanoflowers Bender, Philipp; Honecker, Dirk; Barquín, Luis Fernández arXiv https://doi.org/10.48550/arxiv.1907.02752	text	January 2019
Monodisperse Iron Oxide Nanoparticles by Thermal Decomposition: Elucidating Particle Formation by Second-Resolved in Situ Small-Angle X-ray Scattering Lassenberger, A.; Grünewald, T. A.; van Oostrum, P. D. J. Chemistry of Materials, Vol. 29, Issue 10 https://doi.org/10.1021/acs.chemmater.7b01207	journal	May 2017
Magnetic Nanocomposites and Their Incorporation into Higher Order Biosynthetic Functional Architectures Watt, John; Collins, Aaron M.; Vreeland, Erika C. ACS Omega, Vol. 3, Issue 1 https://doi.org/10.1021/acsomega.7b02031	journal	January 2018
Probing intermediates of the induction period prior to nucleation and growth of semiconductor quantum dots Liu, Mingyang; Wang, Kun; Wang, Linxi Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/ncomms15467	journal	June 2017
Large Scale Solid-state Synthesis of Catalytically Active Fe3O4@M (M = Au, Ag and Au-Ag alloy) Core-shell Nanostructures Nalluri, Srinivasa Rao; Nagarjuna, Ravikiran; Patra, Dinabandhu Scientific Reports, Vol. 9, Issue 1 https://doi.org/10.1038/s41598-019-43116-7	journal	April 2019
Scattering properties and internal structure of magnetic filament brushes Pyanzina, Elena S.; Sánchez, Pedro A.; Cerdà, Joan J. Soft Matter, Vol. 13, Issue 14 https://doi.org/10.1039/c6sm02606k	journal	January 2017
Synchrotron Scattering Methods for Nanomaterials and Soft Matter Research Narayanan, Theyencheri; Konovalov, Oleg Materials, Vol. 13, Issue 3 https://doi.org/10.3390/ma13030752	journal	February 2020
Quantitative Structural Analysis of Polystyrene Nanoparticles Using Synchrotron X-ray Scattering and Dynamic Light Scattering Wong, Jia Chyi; Xiang, Li; Ngoi, Kuan Hoon Polymers, Vol. 12, Issue 2 https://doi.org/10.3390/polym12020477	journal	February 2020
Exact Crystalline Structure Recovery in X-ray Crystallography from Coded Diffraction Patterns Pinilla, Samuel; Bacca, Jorge; Vargas, Cesar arXiv https://doi.org/10.48550/arxiv.1907.03547	preprint	January 2019

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