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Title: Synthesis of 5-Hydroxymethylfurural from Carbohydrates using Large-Pore Mesoporous Tin Phosphate

; ; ; ;
Publication Date:
Research Org.:
Energy Frontier Research Centers (EFRC) (United States). Center for Direct Catalytic Conversion of Biomass to Biofuels (C3Bio)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
OSTI Identifier:
DOE Contract Number:  
Resource Type:
Journal Article
Journal Name:
Additional Journal Information:
Journal Volume: 7; Journal Issue: 3; Related Information: C3Bio partners with Purdue University (lead); Argonne National Laboratory; National Renewable Energy Laboratory; Northeastern University; University of Tennessee; Journal ID: ISSN 1864-5631
ChemPubSoc Europe
Country of Publication:
United States
catalysis (homogeneous), catalysis (heterogeneous), biofuels (including algae and biomass), bio-inspired, materials and chemistry by design, synthesis (self-assembly), synthesis (scalable processing)

Citation Formats

Dutta, Arghya, Gupta, Dinesh, Patra, Astam K., Saha, Basudeb, and Bhaumik, Asim. Synthesis of 5-Hydroxymethylfurural from Carbohydrates using Large-Pore Mesoporous Tin Phosphate. United States: N. p., 2014. Web. doi:10.1002/cssc.201300766.
Dutta, Arghya, Gupta, Dinesh, Patra, Astam K., Saha, Basudeb, & Bhaumik, Asim. Synthesis of 5-Hydroxymethylfurural from Carbohydrates using Large-Pore Mesoporous Tin Phosphate. United States. doi:10.1002/cssc.201300766.
Dutta, Arghya, Gupta, Dinesh, Patra, Astam K., Saha, Basudeb, and Bhaumik, Asim. Tue . "Synthesis of 5-Hydroxymethylfurural from Carbohydrates using Large-Pore Mesoporous Tin Phosphate". United States. doi:10.1002/cssc.201300766.
title = {Synthesis of 5-Hydroxymethylfurural from Carbohydrates using Large-Pore Mesoporous Tin Phosphate},
author = {Dutta, Arghya and Gupta, Dinesh and Patra, Astam K. and Saha, Basudeb and Bhaumik, Asim},
abstractNote = {},
doi = {10.1002/cssc.201300766},
journal = {ChemSusChem},
issn = {1864-5631},
number = 3,
volume = 7,
place = {United States},
year = {2014},
month = {1}

Works referenced in this record:

Quantitative SAXS Analysis of the P123/Water/Ethanol Ternary Phase Diagram
journal, August 2006

  • Soni, S. S.; Brotons, G.; Bellour, M.
  • The Journal of Physical Chemistry B, Vol. 110, Issue 31
  • DOI: 10.1021/jp062159p

Simple Chemical Transformation of Lignocellulosic Biomass into Furans for Fuels and Chemicals
journal, February 2009

  • Binder, Joseph B.; Raines, Ronald T.
  • Journal of the American Chemical Society, Vol. 131, Issue 5, p. 1979-1985
  • DOI: 10.1021/ja808537j

High selective production of 5-hydroymethylfurfural from fructose by a solid heteropolyacid catalyst
journal, June 2011

Biopolymer templated porous TiO2: An efficient catalyst for the conversion of unutilized sugars derived from hemicellulose
journal, September 2012

Production of Liquid Alkanes by Aqueous-Phase Processing of Biomass-Derived Carbohydrates
journal, June 2005

  • Huber, George W.; Chheda, Juben N.; Barrett, Christopher J.
  • Science, Vol. 308, Issue 5727, p. 1446-1450
  • DOI: 10.1126/science.1111166

The effect of solvent addition on fructose dehydration to 5-hydroxymethylfurfural in biphasic system over zeolites
journal, March 2012

Hierarchically Structured Porous Materials for Energy Conversion and Storage
journal, July 2012

  • Li, Yu; Fu, Zheng-Yi; Su, Bao-Lian
  • Advanced Functional Materials, Vol. 22, Issue 22
  • DOI: 10.1002/adfm.201200591

Characterization of the Porous Structure of SBA-15
journal, July 2000

  • Kruk, Michal; Jaroniec, Mietek; Ko, Chang Hyun
  • Chemistry of Materials, Vol. 12, Issue 7
  • DOI: 10.1021/cm000164e

Synergy of boric acid and added salts in the catalytic dehydration of hexoses to 5-hydroxymethylfurfural in water
journal, January 2011

  • Hansen, Thomas S.; Mielby, Jerrik; Riisager, Anders
  • Green Chem., Vol. 13, Issue 1
  • DOI: 10.1039/C0GC00355G

Self-assembly of mesoporous TiO2 nanospheres via aspartic acid templating pathway and its catalytic application for 5-hydroxymethyl-furfural synthesis
journal, January 2011

  • De, Sudipta; Dutta, Saikat; Patra, Astam K.
  • Journal of Materials Chemistry, Vol. 21, Issue 43
  • DOI: 10.1039/c1jm13229f

Catalytic Conversion of Carbohydrates into 5-Hydroxymethylfurfural by Germanium(IV) Chloride in Ionic Liquids
journal, December 2010

Conversion of mono/di/polysaccharides into furan compounds using 1-alkyl-3-methylimidazolium ionic liquids
journal, July 2009

Cubic Mesoporous Silica with Large Controllable Entrance Sizes and Advanced Adsorption Properties
journal, July 2003

  • Fan, Jie; Yu, Chengzhong; Gao, Feng
  • Angewandte Chemie International Edition, Vol. 42, Issue 27
  • DOI: 10.1002/anie.200351027

Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism
journal, October 1992

  • Kresge, C. T.; Leonowicz, M. E.; Roth, W. J.
  • Nature, Vol. 359, Issue 6397, p. 710-712
  • DOI: 10.1038/359710a0

Fructose Dehydration to 5-Hydroxymethylfurfural over Solid Acid Catalysts in a Biphasic System
journal, July 2012

  • Ordomsky, Vitaly V.; van der Schaaf, John; Schouten, Jaap C.
  • ChemSusChem, Vol. 5, Issue 9
  • DOI: 10.1002/cssc.201200072

One-Pot Conversions of Lignocellulosic and Algal Biomass into Liquid Fuels
journal, May 2012

Microwave assisted conversion of carbohydrates and biopolymers to 5-hydroxymethylfurfural with aluminium chloride catalyst in water
journal, January 2011

  • De, Sudipta; Dutta, Saikat; Saha, Basudeb
  • Green Chemistry, Vol. 13, Issue 10
  • DOI: 10.1039/c1gc15550d

Generalized syntheses of large-pore mesoporous metal oxides with semicrystalline frameworks
journal, November 1998

  • Yang, Peidong; Zhao, Dongyuan; Margolese, David I.
  • Nature, Vol. 396, Issue 6707
  • DOI: 10.1038/24132

Effect of Acid on the Aggregation of Poly(ethylene oxide)−Poly(propylene oxide)−Poly(ethylene oxide) Block Copolymers
journal, November 2006

  • Yang, Bin; Guo, Chen; Chen, Shu
  • The Journal of Physical Chemistry B, Vol. 110, Issue 46
  • DOI: 10.1021/jp0634149

Synthesis of Organically Templated Nanoporous Tin(II/IV) Phosphate for Radionuclide and Metal Sequestration
journal, March 2006

  • Wellman, Dawn M.; Mattigod, Shas V.; Parker, Kent E.
  • Inorganic Chemistry, Vol. 45, Issue 6
  • DOI: 10.1021/ic051949v

Catalytical conversion of fructose and glucose into 5-hydroxymethylfurfural in hot compressed water by microwave heating
journal, July 2008

Design of solid catalysts for the conversion of biomass
journal, January 2009

  • Rinaldi, Roberto; Schüth, Ferdi
  • Energy & Environmental Science, Vol. 2, Issue 6
  • DOI: 10.1039/b902668a

Direct conversion of cellulose and lignocellulosic biomass into chemicals and biofuel with metal chloride catalysts
journal, April 2012

Proteins in Mesoporous Silicates
journal, October 2008

  • Hudson, Sarah; Cooney, Jakki; Magner, Edmond
  • Angewandte Chemie International Edition, Vol. 47, Issue 45, p. 8582-8594
  • DOI: 10.1002/anie.200705238

Microwave assisted rapid conversion of carbohydrates into 5-hydroxymethylfurfural catalyzed by mesoporous TiO2 nanoparticles
journal, December 2011

Developments in Nanostructured Cathode Materials for High-Performance Lithium-Ion Batteries
journal, June 2008

Gas Adsorption Characterization of Ordered Organic−Inorganic Nanocomposite Materials
journal, October 2001

  • Kruk, Michal; Jaroniec, Mietek
  • Chemistry of Materials, Vol. 13, Issue 10
  • DOI: 10.1021/cm0101069

Self-adjusted synthesis of ordered stable mesoporous minerals by acid–base pairs
journal, February 2003

  • Tian, Bozhi; Liu, Xiaoying; Tu, Bo
  • Nature Materials, Vol. 2, Issue 3, p. 159-163
  • DOI: 10.1038/nmat838

Metal Chlorides in Ionic Liquid Solvents Convert Sugars to 5-Hydroxymethylfurfural
journal, June 2007

Conversion of carbohydrates and lignocellulosic biomass into 5-hydroxymethylfurfural using AlCl3·6H2O catalyst in a biphasic solvent system
journal, January 2012

  • Yang, Yu; Hu, Chang-wei; Abu-Omar, Mahdi M.
  • Green Chem., Vol. 14, Issue 2, p. 509-513
  • DOI: 10.1039/C1GC15972K

The Preparation of Alkyltriinethylaininonium–Kaneinite Complexes and Their Conversion to Microporous Materials
journal, April 1990

  • Yanagisawa, Tsuneo; Shimizu, Toshio; Kuroda, Kazuyuki
  • Bulletin of the Chemical Society of Japan, Vol. 63, Issue 4
  • DOI: 10.1246/bcsj.63.988

Advances in conversion of hemicellulosic biomass to furfural and upgrading to biofuels
journal, January 2012

  • Dutta, Saikat; De, Sudipta; Saha, Basudeb
  • Catalysis Science & Technology, Vol. 2, Issue 10
  • DOI: 10.1039/c2cy20235b

Ordered mesoporous tin oxide and tin phosphate synthesized by nanocasting strategy
journal, November 2010

Triblock Copolymer Syntheses of Mesoporous Silica with Periodic 50 to 300 Angstrom Pores
journal, January 1998

Solvent Effects on Fructose Dehydration to 5-Hydroxymethylfurfural in Biphasic Systems Saturated with Inorganic Salts
journal, January 2009