skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Synthesis and synchrotron characterisation of novel dual-template of hydroxyapatite scaffolds with controlled size porous distribution

Abstract

Hydroxyapatite (HAP) scaffolds with a hierarchical porous architecture were prepared by a new dual-template (corn starch and cetyltrimethylammonium bromide (CTAB) surfactant) used to cast HAP nanoparticles and development scaffolds with size hierarchical porous distribution. The Powder X-Ray diffraction (XRD) results showed that only the HAP crystalline phase is present in the samples after calcination; the Scanning Electron Microscopy (SEM) combined with Small Angle (SAXS) and Ultra-Small Angle X-ray Scattering (USAXS) techniques showed that the porous arrangement is promoted by needle-like HAP nanoparticles, and that the pore size distributions depend on the drip-order of the calcium and the phosphate solutions during the template preparation stage.

Authors:
; ; ; ; ;
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); National Science Foundation (NSF)
OSTI Identifier:
1373889
DOE Contract Number:  
AC02-06CH11357
Resource Type:
Journal Article
Resource Relation:
Journal Name: Materials Letters; Journal Volume: 190
Country of Publication:
United States
Language:
English
Subject:
Nanoparticles; biomaterials; porous materials

Citation Formats

Lima, Thiago A. R. M., Ilavsky, Jan, Hammons, Joshua, Sarmento, Victor H. V., Rey, José F. Q., and Valerio, Mário E. G.. Synthesis and synchrotron characterisation of novel dual-template of hydroxyapatite scaffolds with controlled size porous distribution. United States: N. p., 2017. Web. doi:10.1016/j.matlet.2016.12.121.
Lima, Thiago A. R. M., Ilavsky, Jan, Hammons, Joshua, Sarmento, Victor H. V., Rey, José F. Q., & Valerio, Mário E. G.. Synthesis and synchrotron characterisation of novel dual-template of hydroxyapatite scaffolds with controlled size porous distribution. United States. doi:10.1016/j.matlet.2016.12.121.
Lima, Thiago A. R. M., Ilavsky, Jan, Hammons, Joshua, Sarmento, Victor H. V., Rey, José F. Q., and Valerio, Mário E. G.. Wed . "Synthesis and synchrotron characterisation of novel dual-template of hydroxyapatite scaffolds with controlled size porous distribution". United States. doi:10.1016/j.matlet.2016.12.121.
@article{osti_1373889,
title = {Synthesis and synchrotron characterisation of novel dual-template of hydroxyapatite scaffolds with controlled size porous distribution},
author = {Lima, Thiago A. R. M. and Ilavsky, Jan and Hammons, Joshua and Sarmento, Victor H. V. and Rey, José F. Q. and Valerio, Mário E. G.},
abstractNote = {Hydroxyapatite (HAP) scaffolds with a hierarchical porous architecture were prepared by a new dual-template (corn starch and cetyltrimethylammonium bromide (CTAB) surfactant) used to cast HAP nanoparticles and development scaffolds with size hierarchical porous distribution. The Powder X-Ray diffraction (XRD) results showed that only the HAP crystalline phase is present in the samples after calcination; the Scanning Electron Microscopy (SEM) combined with Small Angle (SAXS) and Ultra-Small Angle X-ray Scattering (USAXS) techniques showed that the porous arrangement is promoted by needle-like HAP nanoparticles, and that the pore size distributions depend on the drip-order of the calcium and the phosphate solutions during the template preparation stage.},
doi = {10.1016/j.matlet.2016.12.121},
journal = {Materials Letters},
number = ,
volume = 190,
place = {United States},
year = {Wed Mar 01 00:00:00 EST 2017},
month = {Wed Mar 01 00:00:00 EST 2017}
}