Synthetic Development of Low Dimensional Materials

Men, Long; White, Miles A.; Andaraarachchi, Himashi; Rosales, Bryan A.; Vela, Javier

doi:10.1021/acs.chemmater.6b02906

Title: Synthetic Development of Low Dimensional Materials

Journal Article · Wed Nov 02 00:00:00 EDT 2016 · Chemistry of Materials

DOI:https://doi.org/10.1021/acs.chemmater.6b02906· OSTI ID:1342930

Men, Long ^[1]; White, Miles A. ^[2]; Andaraarachchi, Himashi ^[1]; Rosales, Bryan A. ^[2]; Vela, Javier ^[1]

Ames Lab. and Iowa State Univ., Ames, IA (United States). Dept. of Chemistry
Iowa State Univ., Ames, IA (United States). Dept. of Chemistry

Here, in this invited paper, we highlight some of our most recent work on the synthesis of low dimensional nanomaterials. Current graduate students and members of our group present four specific case systems: Nowotny-Juza phases, nickel phosphides, germanium-based core/shells, and organolead mixed-halide perovskites. Each system is accompanied by commentary from the student involved, which explains our motivation behind our work, as well as by a protocol detailing the key experimental considerations involved in their synthesis. We trust these and similar efforts by others and us will help further advance our understanding of the broader field of synthetic nanomaterials chemistry, while, at the same time, highlighting how important this area is to the development of new materials for technologically relevant applications.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Ames Lab., Ames, IA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF)

Grant/Contract Number:: AC02-07CH11358; 1253058

OSTI ID:: 1342930

Report Number(s):: IS-J-9037; TRN: US1701289

Journal Information:: Chemistry of Materials, Vol. 29, Issue 1; ISSN 0897-4756

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 17 works

Citation information provided by
Web of Science

References (80)

Mysteries of TOPSe Revealed: Insights into Quantum Dot Nucleation Evans, Christopher M.; Evans, Meagan E.; Krauss, Todd D. Journal of the American Chemical Society, Vol. 132, Issue 32, p. 10973-10975 https://doi.org/10.1021/ja103805s	journal	August 2010
The Trouble with TOPO; Identification of Adventitious Impurities Beneficial to the Growth of Cadmium Selenide Quantum Dots, Rods, and Wires Wang, Fudong; Tang, Rui; Buhro, William E. Nano Letters, Vol. 8, Issue 10 https://doi.org/10.1021/nl801692g	journal	October 2008
Multiple Wurtzite Twinning in CdTe Nanocrystals Induced by Methylphosphonic Acid Carbone, Luigi; Kudera, Stefan; Carlino, Elvio Journal of the American Chemical Society, Vol. 128, Issue 3 https://doi.org/10.1021/ja054893c	journal	January 2006
Mechanistic Study of Precursor Evolution in Colloidal Group II−VI Semiconductor Nanocrystal Synthesis Liu, Haitao; Owen, Jonathan S.; Alivisatos, A. Paul Journal of the American Chemical Society, Vol. 129, Issue 2 https://doi.org/10.1021/ja0656696	journal	January 2007
Die Verbindungen LiMgP, LiZnP und LiZnAs Nowotny, H.; Bachmayer, K. Monatshefte f�r Chemie, Vol. 81, Issue 4 https://doi.org/10.1007/BF00906437	journal	January 1950
Die ternären Nitride LiMgN und LiZnN. 16. Mitteilung über Metallamide und Metallnitride Juza, Robert; Hund, Franz Zeitschrift für anorganische Chemie, Vol. 257, Issue 1-3 https://doi.org/10.1002/zaac.19482570101	journal	August 1948
Electronic structure of LiZnN: Interstitial insertion rule Carlsson, A. E.; Zunger, Alex; Wood, D. M. Physical Review B, Vol. 32, Issue 2 https://doi.org/10.1103/PhysRevB.32.1386	journal	July 1985
I-II-V half-Heusler compounds for optoelectronics: Ab initio calculations Kieven, David; Klenk, Reiner; Naghavi, Shahab Physical Review B, Vol. 81, Issue 7 https://doi.org/10.1103/PhysRevB.81.075208	journal	February 2010
First principles study of thermoelectric properties of Li-based half-Heusler alloys Yadav, Manoj K.; Sanyal, Biplab Journal of Alloys and Compounds, Vol. 622 https://doi.org/10.1016/j.jallcom.2014.10.025	journal	February 2015
Preparation and properties of radio-frequency-sputtered half-Heusler films for use in solar cells Kieven, D.; Grimm, A.; Beleanu, A. Thin Solid Films, Vol. 519, Issue 6 https://doi.org/10.1016/j.tsf.2010.10.045	journal	January 2011
Systematical, experimental investigations on LiMg Z ( Z = P, As, Sb) wide band gap semiconductors Beleanu, Andreea; Mondeshki, Mihail; Juan, Quin Journal of Physics D: Applied Physics, Vol. 44, Issue 47 https://doi.org/10.1088/0022-3727/44/47/475302	journal	November 2011
Half-Heusler compounds: novel materials for energy and spintronic applications Casper, F.; Graf, T.; Chadov, S. Semiconductor Science and Technology, Vol. 27, Issue 6 https://doi.org/10.1088/0268-1242/27/6/063001	journal	April 2012
Got LiZnP? Solution phase synthesis of filled tetrahedral semiconductors in the nanoregime White, Miles A.; Thompson, Michelle J.; Miller, Gordon J. Chemical Communications, Vol. 52, Issue 17 https://doi.org/10.1039/C5CC09635A	journal	January 2016
Phase-Pure Crystalline Zinc Phosphide Nanoparticles: Synthetic Approaches and Characterization Mobarok, Md Hosnay; Luber, Erik J.; Bernard, Guy M. Chemistry of Materials, Vol. 26, Issue 5 https://doi.org/10.1021/cm500557f	journal	February 2014
Trioctylphosphine A General Phosphorus Source for the Low-Temperature Conversion of Metals into Metal Phosphides Henkes, Amanda E.; Schaak, Raymond E. Chemistry of Materials, Vol. 19, Issue 17, p. 4234-4242 https://doi.org/10.1021/cm071021w	journal	August 2007
Converting Metals into Phosphides A General Strategy for the Synthesis of Metal Phosphide Nanocrystals Henkes, Amanda E.; Vasquez, Yolanda; Schaak, Raymond E. Journal of the American Chemical Society, Vol. 129, Issue 7, p. 1896-1897 https://doi.org/10.1021/ja068502l	journal	February 2007
Formation of Hollow Ni ₂ P Nanoparticles Based on the Nanoscale Kirkendall Effect Chiang, Ray-Kuang; Chiang, Ray-Tung Inorganic Chemistry, Vol. 46, Issue 2 https://doi.org/10.1021/ic061846s	journal	January 2007
Recent developments in synthetic approaches to transition metal phosphide nanoparticles for magnetic and catalytic applications Brock, Stephanie L.; Senevirathne, Keerthi Journal of Solid State Chemistry, Vol. 181, Issue 7 https://doi.org/10.1016/j.jssc.2008.03.012	journal	July 2008
Nanoscaled Metal Borides and Phosphides: Recent Developments and Perspectives Carenco, Sophie; Portehault, David; Boissière, Cédric Chemical Reviews, Vol. 113, Issue 10, p. 7981-8065 https://doi.org/10.1021/cr400020d	journal	June 2013
Polytypism and Unique Site Preference in LiZnSb: A Superior Thermoelectric Reveals Its True Colors White, Miles A.; Miller, Gordon J.; Vela, Javier Journal of the American Chemical Society, Vol. 138, Issue 44 https://doi.org/10.1021/jacs.6b10054	journal	October 2016
Organometallic Chemistry. XII. ¹ The Thermal Decomposition of n-Butyllithium, a Kinetic Study ^2,3 Finnegan, R. A.; Kutta, H. W. The Journal of Organic Chemistry, Vol. 30, Issue 12 https://doi.org/10.1021/jo01023a038	journal	December 1965
Metal Phosphides: Preparation, Characterization and Catalytic Reactivity Prins, Roel; Bussell, Mark E. Catalysis Letters, Vol. 142, Issue 12 https://doi.org/10.1007/s10562-012-0929-7	journal	November 2012
Nanostructured Nickel Phosphide as an Electrocatalyst for the Hydrogen Evolution Reaction Popczun, Eric J.; McKone, James R.; Read, Carlos G. Journal of the American Chemical Society, Vol. 135, Issue 25 https://doi.org/10.1021/ja403440e	journal	June 2013
Nanostructured hydrotreating catalysts for electrochemical hydrogen evolution Morales-Guio, Carlos G.; Stern, Lucas-Alexandre; Hu, Xile Chemical Society Reviews, Vol. 43, Issue 18 https://doi.org/10.1039/C3CS60468C	journal	January 2014
Phase-Programmed Nanofabrication: Effect of Organophosphite Precursor Reactivity on the Evolution of Nickel and Nickel Phosphide Nanocrystals Andaraarachchi, Himashi P.; Thompson, Michelle J.; White, Miles A. Chemistry of Materials, Vol. 27, Issue 23 https://doi.org/10.1021/acs.chemmater.5b03506	journal	November 2015
Study of electrochemical and photoelectrochemical properties of nickel phosphide semiconductors Sharon, Maheshwar; Tamizhmani, G.; Levy-Clement, Claude Solar Cells, Vol. 26, Issue 4 https://doi.org/10.1016/0379-6787(89)90089-6	journal	September 1989
The Chemical Vapor Deposition of Nickel Phosphide or Selenide Thin Films from a Single Precursor Panneerselvam, Arunkumar; Malik, Mohammad. A.; Afzaal, Mohammad Journal of the American Chemical Society, Vol. 130, Issue 8 https://doi.org/10.1021/ja078202j	journal	February 2008
Electrosynthesis of nickel phosphides on the basis of white phosphorus Budnikova, Yu. H.; Tazeev, D. I.; Trofimov, B. A. Electrochemistry Communications, Vol. 6, Issue 7 https://doi.org/10.1016/j.elecom.2004.05.007	journal	July 2004
Low-Temperature Solvothermal Synthesis of Phosphorus-Rich Transition-Metal Phosphides Barry, Brian M.; Gillan, Edward G. Chemistry of Materials, Vol. 20, Issue 8 https://doi.org/10.1021/cm703095z	journal	March 2008
A simple mild hydrothermal route for the synthesis of nickel phosphide powders Liu, Zongyi; Huang, Xiang; Zhu, Zhibin Ceramics International, Vol. 36, Issue 3 https://doi.org/10.1016/j.ceramint.2009.12.015	journal	April 2010
A General and Flexible Synthesis of Transition-Metal Polyphosphides via PCl ₃ Elimination Barry, Brian M.; Gillan, Edward G. Chemistry of Materials, Vol. 21, Issue 19 https://doi.org/10.1021/cm9010663	journal	October 2009
Generalized Synthesis of Metal Phosphide Nanorods via Thermal Decomposition of Continuously Delivered Metal−Phosphine Complexes Using a Syringe Pump Park, Jongnam; Koo, Bonil; Yoon, Ki Youl Journal of the American Chemical Society, Vol. 127, Issue 23 https://doi.org/10.1021/ja0427496	journal	June 2005
Shape-Programmed Nanofabrication: Understanding the Reactivity of Dichalcogenide Precursors Guo, Yijun; Alvarado, Samuel R.; Barclay, Joshua D. ACS Nano, Vol. 7, Issue 4 https://doi.org/10.1021/nn400596e	journal	April 2013
Molecular Control of the Nanoscale: Effect of Phosphine–Chalcogenide Reactivity on CdS–CdSe Nanocrystal Composition and Morphology Ruberu, T. Purnima A.; Albright, Haley R.; Callis, Brandon ACS Nano, Vol. 6, Issue 6 https://doi.org/10.1021/nn301182h	journal	April 2012
A tunable library of substituted thiourea precursors to metal sulfide nanocrystals Hendricks, M. P.; Campos, M. P.; Cleveland, G. T. Science, Vol. 348, Issue 6240 https://doi.org/10.1126/science.aaa2951	journal	June 2015
Molecular Chemistry to the Fore: New Insights into the Fascinating World of Photoactive Colloidal Semiconductor Nanocrystals Vela, Javier The Journal of Physical Chemistry Letters, Vol. 4, Issue 4 https://doi.org/10.1021/jz302100r	journal	February 2013
25th Anniversary Article: Exploring Nanoscaled Matter from Speciation to Phase Diagrams: Metal Phosphide Nanoparticles as a Case of Study Carenco, Sophie; Portehault, David; Boissière, Cédric Advanced Materials, Vol. 26, Issue 3 https://doi.org/10.1002/adma.201303198	journal	December 2013
Chemical Routes for Production of Transition-Metal Phosphides on the Nanoscale: Implications for Advanced Magnetic and Catalytic Materials Brock, Stephanie L.; Perera, Susanthri C.; Stamm, Kimber L. Chemistry - A European Journal, Vol. 10, Issue 14 https://doi.org/10.1002/chem.200305775	journal	July 2004
Synthetic Levers Enabling Independent Control of Phase, Size, and Morphology in Nickel Phosphide Nanoparticles Muthuswamy, Elayaraja; Savithra, Galbokka H. Layan; Brock, Stephanie L. ACS Nano, Vol. 5, Issue 3, p. 2402-2411 https://doi.org/10.1021/nn1033357	journal	February 2011
Steric effects of phosphorus ligands in organometallic chemistry and homogeneous catalysis Tolman, Chadwick A. Chemical Reviews, Vol. 77, Issue 3, p. 313-348 https://doi.org/10.1021/cr60307a002	journal	June 1977
All-Inorganic Germanium Nanocrystal Films by Cationic Ligand Exchange Wheeler, Lance M.; Nichols, Asa W.; Chernomordik, Boris D. Nano Letters, Vol. 16, Issue 3 https://doi.org/10.1021/acs.nanolett.5b05192	journal	January 2016
Near-Infrared Photoluminescence Enhancement in Ge/CdS and Ge/ZnS Core/Shell Nanocrystals: Utilizing IV/II–VI Semiconductor Epitaxy Guo, Yijun; Rowland, Clare E.; Schaller, Richard D. ACS Nano, Vol. 8, Issue 8, p. 8334-8343 https://doi.org/10.1021/nn502792m	journal	July 2014
Achieving direct band gap in germanium through integration of Sn alloying and external strain Gupta, Suyog; Magyari-Köpe, Blanka; Nishi, Yoshio Journal of Applied Physics, Vol. 113, Issue 7 https://doi.org/10.1063/1.4792649	journal	February 2013
Size and Bandgap Control in the Solution-Phase Synthesis of Near-Infrared-Emitting Germanium Nanocrystals Ruddy, Daniel A.; Johnson, Justin C.; Smith, E. Ryan ACS Nano, Vol. 4, Issue 12, p. 7459-7466 https://doi.org/10.1021/nn102728u	journal	November 2010
Nanocrystalline Group IV Alloy Semiconductors: Synthesis and Characterization of Ge _{1– x} Sn _x Quantum Dots for Tunable Bandgaps Esteves, Richard J. Alan; Ho, Minh Q.; Arachchige, Indika U. Chemistry of Materials, Vol. 27, Issue 5 https://doi.org/10.1021/cm503983b	journal	February 2015
Sn _x Ge _{1– x} Alloy Nanocrystals: A First Step toward Solution-Processed Group IV Photovoltaics Ramasamy, Karthik; Kotula, Paul G.; Fidler, Andrew F. Chemistry of Materials, Vol. 27, Issue 13 https://doi.org/10.1021/acs.chemmater.5b01041	journal	June 2015
Microwave-Assisted Ge _{1– x} Sn _x Nanowire Synthesis: Precursor Species and Growth Regimes Seifner, Michael S.; Biegger, Felix; Lugstein, Alois Chemistry of Materials, Vol. 27, Issue 17 https://doi.org/10.1021/acs.chemmater.5b02757	journal	August 2015
“Giant” Multishell CdSe Nanocrystal Quantum Dots with Suppressed Blinking Chen, Yongfen; Vela, Javier; Htoon, Han Journal of the American Chemical Society, Vol. 130, Issue 15 https://doi.org/10.1021/ja711379k	journal	April 2008
Unique Challenges Accompany Thick-Shell CdSe/nCdS ( n > 10) Nanocrystal Synthesis Guo, Yijun; Marchuk, Kyle; Sampat, Siddharth The Journal of Physical Chemistry C, Vol. 116, Issue 4 https://doi.org/10.1021/jp210949v	journal	January 2012
Mapping the Optical Properties of CdSe/CdS Heterostructure Nanocrystals: The Effects of Core Size and Shell Thickness van Embden, Joel; Jasieniak, Jacek; Mulvaney, Paul Journal of the American Chemical Society, Vol. 131, Issue 40 https://doi.org/10.1021/ja9030209	journal	October 2009
Almost always bright Efros, Alexander L. Nature Materials, Vol. 7, Issue 8 https://doi.org/10.1038/nmat2239	journal	August 2008
Infrared-Active Heterostructured Nanocrystals with Ultralong Carrier Lifetimes Lee, Doh C.; Robel, István; Pietryga, Jeffrey M. Journal of the American Chemical Society, Vol. 132, Issue 29 https://doi.org/10.1021/ja102716p	journal	July 2010
Large-Scale Synthesis of Nearly Monodisperse CdSe/CdS Core/Shell Nanocrystals Using Air-Stable Reagents via Successive Ion Layer Adsorption and Reaction Li, J. Jack; Wang, Y. Andrew; Guo, Wenzhuo Journal of the American Chemical Society, Vol. 125, Issue 41, p. 12567-12575 https://doi.org/10.1021/ja0363563	journal	October 2003
Cesium-containing triple cation perovskite solar cells: improved stability, reproducibility and high efficiency Saliba, Michael; Matsui, Taisuke; Seo, Ji-Youn Energy & Environmental Science, Vol. 9, Issue 6 https://doi.org/10.1039/C5EE03874J	journal	January 2016
Highly Tunable Colloidal Perovskite Nanoplatelets through Variable Cation, Metal, and Halide Composition Weidman, Mark C.; Seitz, Michael; Stranks, Samuel D. ACS Nano, Vol. 10, Issue 8 https://doi.org/10.1021/acsnano.6b03496	journal	July 2016
Metal-halide perovskites for photovoltaic and light-emitting devices Stranks, Samuel D.; Snaith, Henry J. Nature Nanotechnology, Vol. 10, Issue 5 https://doi.org/10.1038/nnano.2015.90	journal	May 2015
Spectral Features and Charge Dynamics of Lead Halide Perovskites: Origins and Interpretations Sum, Tze Chien; Mathews, Nripan; Xing, Guichuan Accounts of Chemical Research, Vol. 49, Issue 2 https://doi.org/10.1021/acs.accounts.5b00433	journal	January 2016
Fundamental physics behind high-efficiency organo-metal halide perovskite solar cells Hsiao, Yu-Che; Wu, Ting; Li, Mingxing Journal of Materials Chemistry A, Vol. 3, Issue 30 https://doi.org/10.1039/C5TA01376C	journal	January 2015
Advancements in perovskite solar cells: photophysics behind the photovoltaics Sum, Tze Chien; Mathews, Nripan Energy Environ. Sci., Vol. 7, Issue 8 https://doi.org/10.1039/C4EE00673A	journal	January 2014
The emergence of perovskite solar cells Green, Martin A.; Ho-Baillie, Anita; Snaith, Henry J. Nature Photonics, Vol. 8, Issue 7, p. 506-514 https://doi.org/10.1038/nphoton.2014.134	journal	July 2014
Photon recycling in lead iodide perovskite solar cells Pazos-Outon, L. M.; Szumilo, M.; Lamboll, R. Science, Vol. 351, Issue 6280 https://doi.org/10.1126/science.aaf1168	journal	March 2016
Identifying defect-tolerant semiconductors with high minority-carrier lifetimes: beyond hybrid lead halide perovskites Brandt, Riley E.; Stevanović, Vladan; Ginley, David S. MRS Communications, Vol. 5, Issue 2 https://doi.org/10.1557/mrc.2015.26	journal	May 2015
Shape Evolution and Single Particle Luminescence of Organometal Halide Perovskite Nanocrystals Zhu, Feng; Men, Long; Guo, Yijun ACS Nano, Vol. 9, Issue 3 https://doi.org/10.1021/nn507020s	journal	February 2015
Perovskite energy funnels for efficient light-emitting diodes Yuan, Mingjian; Quan, Li Na; Comin, Riccardo Nature Nanotechnology, Vol. 11, Issue 10 https://doi.org/10.1038/nnano.2016.110	journal	June 2016
Highly Efficient Perovskite-Quantum-Dot Light-Emitting Diodes by Surface Engineering Pan, Jun; Quan, Li Na; Zhao, Yongbiao Advanced Materials, Vol. 28, Issue 39 https://doi.org/10.1002/adma.201600784	journal	August 2016
Harnessing Defect-Tolerance at the Nanoscale: Highly Luminescent Lead Halide Perovskite Nanocrystals in Mesoporous Silica Matrixes Dirin, Dmitry N.; Protesescu, Loredana; Trummer, David Nano Letters, Vol. 16, Issue 9 https://doi.org/10.1021/acs.nanolett.6b02688	journal	August 2016
Organometal halide perovskite solar cells: degradation and stability Berhe, Taame Abraha; Su, Wei-Nien; Chen, Ching-Hsiang Energy & Environmental Science, Vol. 9, Issue 2 https://doi.org/10.1039/C5EE02733K	journal	January 2016
Enhanced UV-light stability of planar heterojunction perovskite solar cells with caesium bromide interface modification Li, Wenzhe; Zhang, Wei; Van Reenen, Stephan Energy & Environmental Science, Vol. 9, Issue 2 https://doi.org/10.1039/C5EE03522H	journal	January 2016
Oxygen Degradation in Mesoporous Al ₂ O ₃ /CH ₃ NH ₃ PbI _3- _x Cl _x Perovskite Solar Cells: Kinetics and Mechanisms Pearson, Andrew J.; Eperon, Giles E.; Hopkinson, Paul E. Advanced Energy Materials, Vol. 6, Issue 13 https://doi.org/10.1002/aenm.201600014	journal	April 2016
High-Performance Perovskite Solar Cells with Enhanced Environmental Stability Based on Amphiphile-Modified CH ₃ NH ₃ PbI ₃ Bi, Dongqin; Gao, Peng; Scopelliti, Rosario Advanced Materials, Vol. 28, Issue 15 https://doi.org/10.1002/adma.201505255	journal	February 2016
Enhancing the Stability of CH ₃ NH ₃ PbBr ₃ Quantum Dots by Embedding in Silica Spheres Derived from Tetramethyl Orthosilicate in “Waterless” Toluene Huang, Shouqiang; Li, Zhichun; Kong, Long Journal of the American Chemical Society, Vol. 138, Issue 18 https://doi.org/10.1021/jacs.5b13101	journal	April 2016
Hydrophobic Organic Hole Transporters for Improved Moisture Resistance in Metal Halide Perovskite Solar Cells Leijtens, Tomas; Giovenzana, Tommaso; Habisreutinger, Severin N. ACS Applied Materials & Interfaces, Vol. 8, Issue 9 https://doi.org/10.1021/acsami.5b10093	journal	February 2016
Entropic stabilization of mixed A-cation ABX ₃ metal halide perovskites for high performance perovskite solar cells Yi, Chenyi; Luo, Jingshan; Meloni, Simone Energy & Environmental Science, Vol. 9, Issue 2 https://doi.org/10.1039/C5EE03255E	journal	January 2016
Reversible Halide Exchange Reaction of Organometal Trihalide Perovskite Colloidal Nanocrystals for Full-Range Band Gap Tuning Jang, Dong Myung; Park, Kidong; Kim, Duk Hwan Nano Letters, Vol. 15, Issue 8 https://doi.org/10.1021/acs.nanolett.5b01430	journal	July 2015
Chemical Management for Colorful, Efficient, and Stable Inorganic–Organic Hybrid Nanostructured Solar Cells Noh, Jun Hong; Im, Sang Hyuk; Heo, Jin Hyuck Nano Letters, Vol. 13, Issue 4, p. 1764-1769 https://doi.org/10.1021/nl400349b	journal	March 2013
Persistent Dopants and Phase Segregation in Organolead Mixed-Halide Perovskites Rosales, Bryan A.; Men, Long; Cady, Sarah D. Chemistry of Materials, Vol. 28, Issue 19 https://doi.org/10.1021/acs.chemmater.6b01874	journal	August 2016
Solid state 207Pb NMR spectroscopy Dybowski, Cecil; Neue, Guenther Progress in Nuclear Magnetic Resonance Spectroscopy, Vol. 41, Issue 3-4 https://doi.org/10.1016/S0079-6565(02)00005-5	journal	December 2002
The Relationship between ²⁰⁷ Pb NMR Chemical Shift and Solid-State Structure in Pb(II) Compounds Dmitrenko, O.; Bai, Shi; Beckmann, Peter A. The Journal of Physical Chemistry A, Vol. 112, Issue 14 https://doi.org/10.1021/jp711182z	journal	March 2008
Empirical Correlations between ²⁰⁷ Pb NMR Chemical Shifts and Structure in Solids Fayon, F.; Farnan, I.; Bessada, C. Journal of the American Chemical Society, Vol. 119, Issue 29 https://doi.org/10.1021/ja963593f	journal	July 1997
Thermodynamic Origin of Photoinstability in the CH ₃ NH ₃ Pb(I _{1– x} Br _x ) ₃ Hybrid Halide Perovskite Alloy Brivio, Federico; Caetano, Clovis; Walsh, Aron The Journal of Physical Chemistry Letters, Vol. 7, Issue 6 https://doi.org/10.1021/acs.jpclett.6b00226	journal	March 2016

Cited By (2)

The Accelerating World of Graphdiynes Sakamoto, Ryota; Fukui, Naoya; Maeda, Hiroaki Advanced Materials, Vol. 31, Issue 42 https://doi.org/10.1002/adma.201804211	journal	June 2019
Structural Engineering of Low‐Dimensional Metal–Organic Frameworks: Synthesis, Properties, and Applications Liu, Wenxian; Yin, Ruilian; Xu, Xilian Advanced Science, Vol. 6, Issue 12 https://doi.org/10.1002/advs.201802373	journal	April 2019

Similar Records

Final Report: Biological and Synthetic Nanostructures Controlled at the Atomistic Level

Technical Report · Wed Feb 21 00:00:00 EST 2007 · OSTI ID:1342930

Williamson, A; van Buuren, T

Sensitivity-Enhanced ²⁰⁷Pb Solid-State NMR Spectroscopy for the Rapid, Non-Destructive Characterization of Organolead Halide Perovskites

Journal Article · Tue Sep 18 00:00:00 EDT 2018 · Chemistry of Materials · OSTI ID:1342930

Hanrahan, Michael P.; Men, Long; Rosales, Bryan A.; +2 more

Persistent dopants and phase segregation in organolead mixed-halide perovskites

Journal Article · Mon Jul 25 00:00:00 EDT 2016 · Chemistry of Materials · OSTI ID:1342930

Rosales, Bryan A.; Men, Long; Cady, Sarah D.; +3 more

Related Subjects

36 MATERIALS SCIENCE
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Title: Synthetic Development of Low Dimensional Materials

Citation Formats

References (80)

Cited By (2)

Similar Records

Related Subjects