Construction of a quartz spherical analyzer: application to high-resolution analysis of the Ni Kα emission spectrum

Honnicke, Marcelo Goncalves; Bianco, Leonardo M.; Ceppi, Sergio A.; Cusatis, Cesar; Huang, XianRong; Cai, Yong Q.; Stutz, Guillermo E.

doi:10.1107/S1600576716010633

Title: Construction of a quartz spherical analyzer: application to high-resolution analysis of the Ni Kα emission spectrum

Journal Article · Wed Aug 10 00:00:00 EDT 2016 · Journal of Applied Crystallography (Online)

DOI:https://doi.org/10.1107/S1600576716010633· OSTI ID:1340372

Honnicke, Marcelo Goncalves ^[1]; Bianco, Leonardo M. ^[2]; Ceppi, Sergio A. ^[3]; Cusatis, Cesar ^[4]; Huang, XianRong ^[5];

^[6]; Stutz, Guillermo E. ^[7]

Universidade Federal da Integracao Latino-Americana (Brazil). Instituto de Ciencias da Vida e da Natureza
Universidad Nacional de Cordoba (Argentina). Facultad de Matematica, Astronomia y Fisica
Universidad Nacional de Cordoba (Argentina). Facultad de Matematica, Astronomia y Fisica ; Instituto de Fisica E. Gaviola, CONICET-UNC (Argentina)
Universidade Federal do Parana (Brazil). Departamento de Fisica
Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
Brookhaven National Lab. (BNL), Upton, NY (United States). National Synchrotron Light Source II
Universidad Nacional de Cordoba (Argentina). Facultad de Matematica, Astronomia y Fisica ; Instituto de Fisica E. Gaviola, CONICET-UNC (Argentina)

The construction and characterization of a focusing X-ray spherical analyzer based on α-quartz 4$$\overline{4}$$04 are presented. For this study, the performance of the analyzer was demonstrated by applying it to a high-resolution X-ray spectroscopy study of theKα_1,2emission spectrum of Ni. An analytical representation based on physical grounds was assumed to model the shape of the X-ray emission lines. Satellite structures assigned to 3dspectator hole transitions were resolved and determined as well as their relative contribution to the emission spectrum. The present results on 1s^-13d^-1shake probabilities support a recently proposed calculation framework based on a multi-configuration atomic model.

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Research Organization:: Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC00112704; AC02-06CH11357

OSTI ID:: 1340372

Report Number(s):: BNL-112494-2016-JA; TRN: US1701731

Journal Information:: Journal of Applied Crystallography (Online), Vol. 49, Issue 5; ISSN 1600-5767

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 5 works

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