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Title: Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

Journal Article · · Physical Review Letters
 [1];  [1];  [2];  [2];  [3];  [4];  [3];  [1];  [1]
  1. Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
  2. Aix-Marseille Univ., and CNRS/IN2P3, Marseille (France)
  3. Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
  4. European Synchrotron Radiation Facility (ESRF), Grenoble (France)

Here, we present and demonstrate a formalism by which three-dimensional (3D) Bragg x-ray coherent diffraction imaging (BCDI) can be implemented without moving the sample by scanning the energy of the incident x-ray beam. This capability is made possible by introducing a 3D Fourier transform that accounts for x-ray wavelength variability. We also demonstrate the approach by inverting coherent Bragg diffraction patterns from a gold nanocrystal measured with an x-ray energy scan. Furthermore, variable-wavelength BCDI will expand the breadth of feasible in situ 3D strain imaging experiments towards more diverse materials environments, especially where sample manipulation is difficult.

Research Organization:
Argonne National Laboratory (ANL), Argonne, IL (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
AC02-06CH11357
OSTI ID:
1352631
Alternate ID(s):
OSTI ID: 1333338
Journal Information:
Physical Review Letters, Vol. 117, Issue 22; ISSN 0031-9007
Publisher:
American Physical Society (APS)Copyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 24 works
Citation information provided by
Web of Science

References (24)

Imaging transient melting of a nanocrystal using an X-ray laser journal June 2015
Nanobeam X-Ray Scattering journal January 2013
Partial coherence effects on the imaging of small crystals using coherent x-ray diffraction journal November 2001
Noise models for low counting rate coherent diffraction imaging journal January 2012
Three-dimensional mapping of a deformation field inside a nanocrystal journal July 2006
Differential stress induced by thiol adsorption on facetted nanocrystals journal September 2011
Signature of dislocations and stacking faults of face-centred cubic nanocrystals in coherent X-ray diffraction patterns: a numerical study journal April 2015
Maximum-likelihood refinement for coherent diffractive imaging journal June 2012
Mathematical Methods in Image Reconstruction book January 2001
Coherent X-ray diffraction imaging of strain at the nanoscale journal April 2009
Core–shell strain structure of zeolite microcrystals journal July 2013
Topological defect dynamics in operando battery nanoparticles journal June 2015
Anomalous coherent diffraction of core-shell nano-objects: A methodology for determination of composition and strain fields journal January 2013
Elastic strain engineering for unprecedented materials properties journal February 2014
Utilizing broadband X-rays in a Bragg coherent X-ray diffraction imaging experiment journal July 2016
Invited Article: A unified evaluation of iterative projection algorithms for phase retrieval journal January 2007
Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction journal October 2001
Orientation variation of surface strain journal September 2007
Efficient modeling of Bragg coherent x-ray nanobeam diffraction journal January 2015
In situ three-dimensional reciprocal-space mapping during mechanical deformation journal July 2012
Three-dimensional diffraction mapping by tuning the X-ray energy journal March 2011
Lensless imaging using broadband X-ray sources journal June 2011
Phase retrieval algorithms: a comparison journal January 1982
Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction text January 2001

Cited By (6)

Variable‐Wavelength Quick Scanning Nanofocused X‐Ray Microscopy for In Situ Strain and Tilt Mapping journal January 2020
Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies journal March 2018
Multi-wavelength Bragg coherent X-ray diffraction imaging of Au particles journal February 2020
X-ray microscopy journal February 2017
X-ray microscopy journal July 1965
Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies text January 2017

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