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Title: Quantitative 13C NMR characterization of fast pyrolysis oils

Abstract

Quantitative 13C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Furthermore, modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.

Authors:
 [1];  [1];  [1]
  1. National Renewable Energy Lab. (NREL), Golden, CO (United States)
Publication Date:
Research Org.:
National Renewable Energy Lab. (NREL), Golden, CO (United States)
Sponsoring Org.:
USDOE Office of Energy Efficiency and Renewable Energy (EERE), Bioenergy Technologies Office (EE-3B)
OSTI Identifier:
1332485
Report Number(s):
NREL/JA-5100-67305
Journal ID: ISSN 2046-2069; RSCACL
Grant/Contract Number:  
AC36-08GO28308
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
RSC Advances
Additional Journal Information:
Journal Volume: 6; Journal Issue: 104; Journal ID: ISSN 2046-2069
Publisher:
Royal Society of Chemistry
Country of Publication:
United States
Language:
English
Subject:
09 BIOMASS FUELS; pyrolysis; NMR; 13C; catalytic fast pyrolysis

Citation Formats

Happs, Renee M., Lisa, Kristina, and Ferrell, III, Jack R. Quantitative 13C NMR characterization of fast pyrolysis oils. United States: N. p., 2016. Web. doi:10.1039/C6RA24044E.
Happs, Renee M., Lisa, Kristina, & Ferrell, III, Jack R. Quantitative 13C NMR characterization of fast pyrolysis oils. United States. doi:10.1039/C6RA24044E.
Happs, Renee M., Lisa, Kristina, and Ferrell, III, Jack R. Thu . "Quantitative 13C NMR characterization of fast pyrolysis oils". United States. doi:10.1039/C6RA24044E. https://www.osti.gov/servlets/purl/1332485.
@article{osti_1332485,
title = {Quantitative 13C NMR characterization of fast pyrolysis oils},
author = {Happs, Renee M. and Lisa, Kristina and Ferrell, III, Jack R.},
abstractNote = {Quantitative 13C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Furthermore, modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.},
doi = {10.1039/C6RA24044E},
journal = {RSC Advances},
number = 104,
volume = 6,
place = {United States},
year = {Thu Oct 20 00:00:00 EDT 2016},
month = {Thu Oct 20 00:00:00 EDT 2016}
}

Journal Article:
Free Publicly Available Full Text
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Cited by: 1 work
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Works referenced in this record:

Review of fast pyrolysis of biomass and product upgrading
journal, March 2012


Pyrolysis of Wood/Biomass for Bio-oil: A Critical Review
journal, May 2006

  • Mohan, Dinesh; Pittman,, Charles U.; Steele, Philip H.
  • Energy & Fuels, Vol. 20, Issue 3, p. 848-889
  • DOI: 10.1021/ef0502397

Overview of Applications of Biomass Fast Pyrolysis Oil
journal, March 2004

  • Czernik, S.; Bridgwater, A. V.
  • Energy & Fuels, Vol. 18, Issue 2, p. 590-598
  • DOI: 10.1021/ef034067u