Integrated Data Collection Analysis (IDCA) Program - AN and Bullseye Smokeless Powder
Abstract
The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of ammonium nitrate (AN) mixed with Bullseye® smokeless powder (Gunpowder). The participants found the AN/Gunpowder to: 1) have a range of sensitivity to impact, comparable to or less than RDX, 2) be fairly insensitive to friction as measured by BAM and ABL, 3) have a range for ESD, from insensitive to more sensitive than PETN, and 4) have thermal sensitivity about the same as PETN and Gunpowder. This effort, funded by the Department of Homeland Security (DHS), is putting the issues of safe handling of these materials in perspective with standard military explosives. The study is adding SSST testing results for a broad suite of different HMEs to the literature. Ultimately the study has the potential to suggest new guidelines and methods and possibly establish the SSST testing accuracies needed when developing safe handling practices for HMEs. Each participating testing laboratory uses identical test materials and preparation methods. Note, however, the test procedures differ among the laboratories. The testing performers involvedmore »
- Authors:
-
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Naval Surface Warfare Center (NSWC), Indian Head, MD (United States)
- Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
- Bureau of Alcohol, Tobacco, and Firearms, Redstone Arsenal, AL (United States)
- Applied Research Associates, Tyndall Air Force Base, FL (United States)
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Publication Date:
- Research Org.:
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1297659
- Report Number(s):
- LLNL-TR-641024
- DOE Contract Number:
- AC52-07NA27344
- Resource Type:
- Technical Report
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY
Citation Formats
Sandstrom, Mary M., Brown, Geoffrey W., Preston, Daniel N., Pollard, Colin J., Warner, Kirstin F., Sorensen, Daniel N., Remmers, Daniel L., Phillips, Jason J., Shelley, Timothy J., Reyes, Jose A., Hsu, Peter C., and Reynolds, John G. Integrated Data Collection Analysis (IDCA) Program - AN and Bullseye Smokeless Powder. United States: N. p., 2013.
Web. doi:10.2172/1297659.
Sandstrom, Mary M., Brown, Geoffrey W., Preston, Daniel N., Pollard, Colin J., Warner, Kirstin F., Sorensen, Daniel N., Remmers, Daniel L., Phillips, Jason J., Shelley, Timothy J., Reyes, Jose A., Hsu, Peter C., & Reynolds, John G. Integrated Data Collection Analysis (IDCA) Program - AN and Bullseye Smokeless Powder. United States. doi:10.2172/1297659.
Sandstrom, Mary M., Brown, Geoffrey W., Preston, Daniel N., Pollard, Colin J., Warner, Kirstin F., Sorensen, Daniel N., Remmers, Daniel L., Phillips, Jason J., Shelley, Timothy J., Reyes, Jose A., Hsu, Peter C., and Reynolds, John G. Wed .
"Integrated Data Collection Analysis (IDCA) Program - AN and Bullseye Smokeless Powder". United States.
doi:10.2172/1297659. https://www.osti.gov/servlets/purl/1297659.
@article{osti_1297659,
title = {Integrated Data Collection Analysis (IDCA) Program - AN and Bullseye Smokeless Powder},
author = {Sandstrom, Mary M. and Brown, Geoffrey W. and Preston, Daniel N. and Pollard, Colin J. and Warner, Kirstin F. and Sorensen, Daniel N. and Remmers, Daniel L. and Phillips, Jason J. and Shelley, Timothy J. and Reyes, Jose A. and Hsu, Peter C. and Reynolds, John G.},
abstractNote = {The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of ammonium nitrate (AN) mixed with Bullseye® smokeless powder (Gunpowder). The participants found the AN/Gunpowder to: 1) have a range of sensitivity to impact, comparable to or less than RDX, 2) be fairly insensitive to friction as measured by BAM and ABL, 3) have a range for ESD, from insensitive to more sensitive than PETN, and 4) have thermal sensitivity about the same as PETN and Gunpowder. This effort, funded by the Department of Homeland Security (DHS), is putting the issues of safe handling of these materials in perspective with standard military explosives. The study is adding SSST testing results for a broad suite of different HMEs to the literature. Ultimately the study has the potential to suggest new guidelines and methods and possibly establish the SSST testing accuracies needed when developing safe handling practices for HMEs. Each participating testing laboratory uses identical test materials and preparation methods. Note, however, the test procedures differ among the laboratories. The testing performers involved are Lawrence Livermore National Laboratory (LLNL), Los Alamos National Laboratory (LANL), Indian Head Division, Naval Surface Warfare Center, (NSWC IHD), Sandia National Laboratories (SNL), and Air Force Research Laboratory (AFRL/RXQL). These tests are conducted as a proficiency study in order to establish some consistency in test protocols, procedures, and experiments and to compare results when these testing variables cannot be made consistent. Keywords: Small-scale safety testing, proficiency test, impact-, friction-, spark discharge-, thermal testing, round-robin test, safety testing protocols, HME, RDX, potassium perchlorate, potassium chlorate, sodium chlorate, sugar, dodecane, PETN, carbon, ammonium nitrate, Gunpowder, Bullseye® smokeless powder.},
doi = {10.2172/1297659},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Wed Jul 17 00:00:00 EDT 2013},
month = {Wed Jul 17 00:00:00 EDT 2013}
}
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The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of Bullseye ® smokeless powder (Gunpowder). The participants found the Gunpowder: 1) to have a range of sensitivity to impact, from less than RDX to almost as sensitive as PETN, 2) to be moderately sensitive to BAM and ABL friction, 3) have a range for ESD, from insensitive to more sensitive than PETN, and 4) to have thermal sensitivity about themore »
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Integrated Data Collection Analysis (IDCA) Program — IDCA Quarterly Program Review, September 14 and 15, 2010
The IDCA conducted a program review at Los Alamos National Laboratory, September 14 and 15, 2010. The review was divided into three parts: 1) an update on the current status of the program, 2) an information exchange and discussion on technical details for current issues and future planning, and 3) a tour of the SSST testing facilities at LANL. The meeting started with an update from DHS by Laura Parker and a restating of some of the objectives of the Proficiency Test of which the IDCA is currently engaged. This update was followed by a discussion of some high levelmore » -
Integrated Data Collection Analysis (IDCA) Program - Statistical Analysis of RDX Standard Data Sets
The Integrated Data Collection Analysis (IDCA) program is conducting a Proficiency Test for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are statistical analyses of the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of the RDX Type II Class 5 standard. The material was tested as a well-characterized standard several times during the proficiency study to assess differences among participants and the range of results that may arise for well-behaved explosive materials. The analyses show that there are detectable differences among the results from IDCA participants. While these differences are statisticallymore » -
Integrated Data Collection Analysis (IDCA) Program — RDX Standard Data Sets
The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of the RDX Type II Class 5 standard, for a third and fourth time in the Proficiency Test and averaged with the analysis results from the first and second time. The results, from averaging all four sets (1, 2, 3 and 4) of data suggest a material to have slightly more impact sensitivity, more BAM friction sensitivity, less ABL friction sensitivity,more » -
Integrated Data Collection Analysis (IDCA) Program - RDX Type II Class 5 Standard, Data Set 1
This document describes the results of the first reference sample material—RDX Type II Class 5—examined in the proficiency study for small-scale safety and thermal (SSST) testing of explosive materials for the Integrated Data Collection Analysis (IDCA) Program. The IDCA program is conducting proficiency testing on homemade explosives (HMEs). The reference sample materials are being studied to establish the accuracy of traditional explosives safety testing for each performing laboratory. These results will be used for comparison to results from testing HMEs. This effort, funded by the Department of Homeland Security (DHS), ultimately will put the issues of safe handling of thesemore »