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Method and device to synthesize boron nitride nanotubes and related nanoparticles

Patent ·
OSTI ID:1264425

Methods and apparatus for producing chemical nanostructures having multiple elements, such as boron and nitride, e.g. boron nitride nanotubes, are disclosed. The method comprises creating a plasma jet, or plume, such as by an arc discharge. The plasma plume is elongated and has a temperature gradient along its length. It extends along its length into a port connector area having ports for introduction of feed materials. The feed materials include the multiple elements, which are introduced separately as fluids or powders at multiple ports along the length of the plasma plume, said ports entering the plasma plume at different temperatures. The method further comprises modifying a temperature at a distal portion of or immediately downstream of said plasma plume; and collecting said chemical nanostructures after said modifying.

Research Organization:
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC02-05CH11231
Assignee:
The Regents of the University of California (Oakland, CA)
Patent Number(s):
9,394,632
Application Number:
13/635,897
OSTI ID:
1264425
Country of Publication:
United States
Language:
English

References (12)

Hydrogen-Catalyzed, Pilot-Scale Production of Small-Diameter Boron Nitride Nanotubes and Their Macroscopic Assemblies journal May 2014
Effective precursor for high yield synthesis of pure BN nanotubes journal July 2005
Nanotubes in boron nitride laser heated at high pressure journal September 1996
Synthesis, Structural and Mechanical Characterization of Amorphous and Crystalline Boron Nanobelts journal January 2008
Boron Nitride Nanotubes with Reduced Numbers of Layers Synthesized by Arc Discharge journal June 1996
Synthesis of boron nitride nanotubes from carbon nanotubes by a substitution reaction journal November 1998
A solid-state process for formation of boron nitride nanotubes journal May 1999
Boron nitride nanotubes, webs, and coexisting amorphous phase formed by the plasma jet method journal August 1999
CVD Growth of Boron Nitride Nanotubes journal July 2000
Scaled Synthesis of Boron Nitride Nanotubes, Nanoribbons, and Nanococoons Using Direct Feedstock Injection into an Extended-Pressure, Inductively-Coupled Thermal Plasma journal July 2014
Mass-production of boron nitride double-wall nanotubes and nanococoons journal January 2000
Boron Nitride Nanotubes Are Noncytotoxic and Can Be Functionalized for Interaction with Proteins and Cells journal January 2009

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