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Method and apparatus for in-situ drying investigation and optimization of slurry drying methodology

Patent ·
OSTI ID:1252198

A method of drying casted slurries that includes calculating drying conditions from an experimental model for a cast slurry and forming a cast film. An infrared heating probe is positioned on one side of the casted slurry and a thermal probe is positioned on an opposing side of the casted slurry. The infrared heating probe may control the temperature of the casted slurry during drying. The casted slurry may be observed with an optical microscope, while applying the drying conditions from the experimental model. Observing the casted slurry includes detecting the incidence of micro-structural changes in the casted slurry during drying to determine if the drying conditions from the experimental model are optimal.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-00OR22725
Assignee:
UT-BATTELLE, LLC (Oak Ridge, TN)
Patent Number(s):
9,337,470
Application Number:
13/656,020
OSTI ID:
1252198
Country of Publication:
United States
Language:
English

References (6)

A study of lithium ion intercalation induced fracture of silicon particles used as anode material in Li-ion battery journal October 2011
The evaporation coefficient of water: a review journal August 1997
Advanced Lithium Battery Cathodes Using Dispersed Carbon Fibers as the Current Collector journal January 2011
Microwave Processing of Ceramics: Guidelines Used at the Oak Ridge National Laboratory journal January 1992
Diffusion-Induced Stress, Interfacial Charge Transfer, and Criteria for Avoiding Crack Initiation of Electrode Particles journal January 2010
Evaporation into vacuum: Mass flux from momentum flux and the Hertz–Knudsen relation revisited journal February 2009

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