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Title: Microstructure and Mechanical Properties of a Novel Rapidly Solidified, High-Temperature Al-Alloy

Abstract

Rapid solidification (RS) processing, as a production method, offers a variety of unique properties based on far-from-equilibrium microstructures obtained through rapid cooling rates. In this study, we seek to investigate the microstructures and properties of a novel Al-alloy specifically designed for high temperature mechanical stability. Synthesis of, AlFe11.4Si1.8V1.6Mn0.9 (wt. %), was performed by two approaches: rotating cup atomization (“shot”) and melt spinning (“flake”). These methods were chosen because of their ability to produce alloys with tailored microstructures due to their inherent differences in cooling rate. The as-solidified precursor materials were microstructurally characterized with electron microscopy. The results show that the higher cooling rate flake material exhibited the formation of nanocrystalline regions as well additional phase morphologies not seen in the shot material. Secondary dendritic branching in the flake material was on the order of 0.1-0.25µm whereas branching in the shot material was 0.5-1.0µm. Consolidated and extruded material from both precursor materials was mechanically evaluated at both ambient and high (300°C) temperature. The consolidated RS flake material is shown to exhibit higher strengths than the shot material. The ultimate tensile strength of the melt spun flake was reported as 544.2MPa at room temperature and 298.0MPa at 300°C. These results forecast themore » ability to design alloys and processing approaches with unique non-equilibrium microstructures with robust mechanical properties at elevated temperatures.« less

Authors:
; ; ; ;
Publication Date:
Research Org.:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1243202
Report Number(s):
PNNL-SA-112327
Journal ID: ISSN 1044-5803; VT0504000
DOE Contract Number:  
AC05-76RL01830
Resource Type:
Journal Article
Resource Relation:
Journal Name: Materials Characterization; Journal Volume: 112
Country of Publication:
United States
Language:
English
Subject:
Rapid Solidification; Aluminum; Alloy; Microstructure; Phase Decomposition

Citation Formats

Overman, Nicole R., Mathaudhu, Suveen, Choi, Jung-Pyung, Roosendaal, Timothy J., and Pitman, Stan G.. Microstructure and Mechanical Properties of a Novel Rapidly Solidified, High-Temperature Al-Alloy. United States: N. p., 2016. Web. doi:10.1016/j.matchar.2015.12.015.
Overman, Nicole R., Mathaudhu, Suveen, Choi, Jung-Pyung, Roosendaal, Timothy J., & Pitman, Stan G.. Microstructure and Mechanical Properties of a Novel Rapidly Solidified, High-Temperature Al-Alloy. United States. doi:10.1016/j.matchar.2015.12.015.
Overman, Nicole R., Mathaudhu, Suveen, Choi, Jung-Pyung, Roosendaal, Timothy J., and Pitman, Stan G.. Fri . "Microstructure and Mechanical Properties of a Novel Rapidly Solidified, High-Temperature Al-Alloy". United States. doi:10.1016/j.matchar.2015.12.015.
@article{osti_1243202,
title = {Microstructure and Mechanical Properties of a Novel Rapidly Solidified, High-Temperature Al-Alloy},
author = {Overman, Nicole R. and Mathaudhu, Suveen and Choi, Jung-Pyung and Roosendaal, Timothy J. and Pitman, Stan G.},
abstractNote = {Rapid solidification (RS) processing, as a production method, offers a variety of unique properties based on far-from-equilibrium microstructures obtained through rapid cooling rates. In this study, we seek to investigate the microstructures and properties of a novel Al-alloy specifically designed for high temperature mechanical stability. Synthesis of, AlFe11.4Si1.8V1.6Mn0.9 (wt. %), was performed by two approaches: rotating cup atomization (“shot”) and melt spinning (“flake”). These methods were chosen because of their ability to produce alloys with tailored microstructures due to their inherent differences in cooling rate. The as-solidified precursor materials were microstructurally characterized with electron microscopy. The results show that the higher cooling rate flake material exhibited the formation of nanocrystalline regions as well additional phase morphologies not seen in the shot material. Secondary dendritic branching in the flake material was on the order of 0.1-0.25µm whereas branching in the shot material was 0.5-1.0µm. Consolidated and extruded material from both precursor materials was mechanically evaluated at both ambient and high (300°C) temperature. The consolidated RS flake material is shown to exhibit higher strengths than the shot material. The ultimate tensile strength of the melt spun flake was reported as 544.2MPa at room temperature and 298.0MPa at 300°C. These results forecast the ability to design alloys and processing approaches with unique non-equilibrium microstructures with robust mechanical properties at elevated temperatures.},
doi = {10.1016/j.matchar.2015.12.015},
journal = {Materials Characterization},
number = ,
volume = 112,
place = {United States},
year = {Fri Feb 12 00:00:00 EST 2016},
month = {Fri Feb 12 00:00:00 EST 2016}
}