Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces

Chen, Chen; Kang, Yijin; Huo, Ziyang; Zhu, Zhongwei; Huang, Wenyu; Xin, Huolin; Snyder, Joshua; Li, Dongguo; Herron, Jeffrey A.; Mavrikakis, Manos; Chi, Miaofang; More, Karren L.; Li, Yadong; Markovic, Nenad M.; Somorjai, Gabor A.; Yang, Peidong; Stamenkovic, Vojislav R.

doi:10.1126/science.1249061

Title: Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces

Journal Article · Fri Mar 21 00:00:00 EDT 2014 · Science

DOI:https://doi.org/10.1126/science.1249061· OSTI ID:1227053

Chen, Chen ^[1]; Kang, Yijin ^[2]; Huo, Ziyang ^[3]; Zhu, Zhongwei ^[3]; Huang, Wenyu ^[3]; Xin, Huolin ^[4]; Snyder, Joshua ^[2]; Li, Dongguo ^[2]; Herron, Jeffrey A. ^[5]; Mavrikakis, Manos ^[5]; Chi, Miaofang ^[6]; More, Karren L. ^[6]; Li, Yadong ^[7]; Markovic, Nenad M. ^[2]; Somorjai, Gabor A. ^[3]; Yang, Peidong ^[8]; Stamenkovic, Vojislav R. ^[2]

Univ. of California, Berkeley, CA (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Tsinghua Univ., Beijing (China)
Argonne National Lab. (ANL), Argonne, IL (United States)
Univ. of California, Berkeley, CA (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Univ. of Wisconsin, Madison, WI (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Tsinghua Univ., Beijing (China)
Univ. of California, Berkeley, CA (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); King Abdulaziz Univ., Jeddah (Saudia Arabia)

Control of structure at the atomic level can precisely and effectively tune catalytic properties of materials, enabling enhancement in both activity and durability. We synthesized a highly active and durable class of electrocatalysts by exploiting the structural evolution of platinum-nickel (Pt-Ni) bimetallic nanocrystals. The starting material, crystalline PtNi₃ polyhedra, transforms in solution by interior erosion into Pt₃Ni nanoframes with surfaces that offer three-dimensional molecular accessibility. The edges of the Pt-rich PtNi₃ polyhedra are maintained in the final Pt₃Ni nanoframes. Both the interior and exterior catalytic surfaces of this open-framework structure are composed of the nanosegregated Pt-skin structure, which exhibits enhanced oxygen reduction reaction (ORR) activity. The Pt₃Ni nanoframe catalysts achieved a factor of 36 enhancement in mass activity and a factor of 22 enhancement in specific activity, respectively, for this reaction (relative to state-of-the-art platinum-carbon catalysts) during prolonged exposure to reaction conditions.

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Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States). Environmental Molecular Sciences Laboratory (EMSL)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC05-76RL01830

OSTI ID:: 1227053

Journal Information:: Science, Vol. 343, Issue 6177; ISSN 0036-8075

Publisher:: AAAS

Country of Publication:: United States

Language:: English

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Hollow nanoparticles as emerging electrocatalysts for renewable energy conversion reactions Park, Jongsik; Kwon, Taehyun; Kim, Jun Chemical Society Reviews, Vol. 47, Issue 22 https://doi.org/10.1039/c8cs00336j	journal	January 2018
Synthesis of germanium–platinum nanoparticles as high-performance catalysts for spray-deposited large-area dye-sensitized solar cells (DSSC) and the hydrogen evolution reaction (HER) Lim, Suh-Ciuan; Hsiao, Ming-Cheng; Lu, Ming-De Nanoscale, Vol. 10, Issue 35 https://doi.org/10.1039/c8nr03983f	journal	January 2018
Direct fabrication of bi-metallic PdRu nanorod assemblies for electrochemical ammonia synthesis Wang, Hongjing; Li, Yinghao; Yang, Dandan Nanoscale, Vol. 11, Issue 12 https://doi.org/10.1039/c8nr10398d	journal	January 2019
Carved nanoframes of cobalt–iron bimetal phosphide as a bifunctional electrocatalyst for efficient overall water splitting Lian, Yuebin; Sun, Hao; Wang, Xuebin Chemical Science, Vol. 10, Issue 2 https://doi.org/10.1039/c8sc03877e	journal	January 2019
Morphology evolution of fcc Ru nanoparticles under hydrogen atmosphere Liu, Lili; Yu, Mengting; Hou, Bo Nanoscale, Vol. 11, Issue 16 https://doi.org/10.1039/c9nr01611b	journal	January 2019
Ultrasmall MoP encapsulated in nitrogen-doped carbon hybrid frameworks for highly efficient hydrogen evolution reaction in both acid and alkaline solutions Huang, Xiaokang; Wang, Xiang; Jiang, Pengbo Inorganic Chemistry Frontiers, Vol. 6, Issue 6 https://doi.org/10.1039/c9qi00279k	journal	January 2019
Rational design and synthesis of noble-metal nanoframes for catalytic and photonic applications Wang, Xue; Ruditskiy, Aleksey; Xia, Younan National Science Review, Vol. 3, Issue 4 https://doi.org/10.1093/nsr/nww062	journal	September 2016
Atomic-level structure engineering of metal oxides for high-rate oxygen intercalation pseudocapacitance Ling, Tao; Da, Pengfei; Zheng, Xueli Science Advances, Vol. 4, Issue 10 https://doi.org/10.1126/sciadv.aau6261	journal	October 2018
Analysis of H 2 /Air Polarization Curves: The Influence of Low Pt Loading and Fabrication Process Yu, Haoran; Bonville, Leonard; Maric, Radenka Journal of The Electrochemical Society, Vol. 165, Issue 5 https://doi.org/10.1149/2.0261805jes	journal	January 2018
Metal Catalysts for Heterogeneous Catalysis: From Single Atoms to Nanoclusters and Nanoparticles Liu, Lichen; Corma, Avelino Chemical Reviews, Vol. 118, Issue 10 https://doi.org/10.1021/acs.chemrev.7b00776	journal	April 2018
Thermal Properties and Segregation Behavior of Pt Nanowires Modified with Au, Ag, and Pd Atoms: A Classical Molecular Dynamics Study Gambu, Thobani G.; Terranova, Umberto; Santos-Carballal, David The Journal of Physical Chemistry C, Vol. 123, Issue 33 https://doi.org/10.1021/acs.jpcc.9b02730	journal	July 2019
Atomically Resolved Anisotropic Electrochemical Shaping of Nano-electrocatalyst Ruiz-Zepeda, Francisco; Gatalo, Matija; Pavlišič, Andraž Nano Letters, Vol. 19, Issue 8 https://doi.org/10.1021/acs.nanolett.9b00918	journal	April 2019
Tuning the Electrocatalytic Performance of Ionic Liquid Modified Pt Catalysts for the Oxygen Reduction Reaction via Cationic Chain Engineering Zhang, Gui-Rong; Wolker, Thomas; Sandbeck, Daniel J. S. ACS Catalysis, Vol. 8, Issue 9 https://doi.org/10.1021/acscatal.8b02018	journal	July 2018
On-Chip in Situ Monitoring of Competitive Interfacial Anionic Chemisorption as a Descriptor for Oxygen Reduction Kinetics Ding, Mengning; Zhong, Guangyan; Zhao, Zipeng ACS Central Science, Vol. 4, Issue 5 https://doi.org/10.1021/acscentsci.8b00082	journal	April 2018
Dealloying of Nitrogen-Introduced Pt–Co Alloy Nanoparticles: Preferential Core–Shell Formation with Enhanced Activity for Oxygen Reduction Reaction Takahashi, Shuntaro; Takahashi, Naoki; Todoroki, Naoto ACS Omega, Vol. 1, Issue 6 https://doi.org/10.1021/acsomega.6b00412	journal	December 2016
Exceptional Oxygen Reduction Reaction Activity and Durability of Platinum–Nickel Nanowires through Synthesis and Post-Treatment Optimization Alia, Shaun M.; Ngo, Chilan; Shulda, Sarah ACS Omega, Vol. 2, Issue 4 https://doi.org/10.1021/acsomega.7b00054	journal	April 2017
Interfacial Structure of PtNi Surface Alloy on Pt(111) Electrode for Oxygen Reduction Reaction Kumeda, Tomoaki; Otsuka, Naoto; Tajiri, Hiroo ACS Omega, Vol. 2, Issue 5 https://doi.org/10.1021/acsomega.7b00301	journal	May 2017
Programming ORR Activity of Ni/NiO_x@Pd Electrocatalysts via Controlling Depth of Surface-Decorated Atomic Pt Clusters Bhalothia, Dinesh; Chou, Jyh-Pin; Yan, Che ACS Omega, Vol. 3, Issue 8 https://doi.org/10.1021/acsomega.8b01234	journal	August 2018
Facile Synthesis of PtCu Alloy/Graphene Oxide Hybrids as Improved Electrocatalysts for Alkaline Fuel Cells Liu, Taiyang; Li, Chaozhong; Yuan, Qiang ACS Omega, Vol. 3, Issue 8 https://doi.org/10.1021/acsomega.8b01347	journal	August 2018
In Situ Construction of Small Pt NPs Embedded in 3D Spherical Porous Carbon as an Electrocatalyst for Liquid Fuel Oxidation with High Performance Ding, Tao; Zhang, Li; Li, Huanran ACS Omega, Vol. 3, Issue 12 https://doi.org/10.1021/acsomega.8b02584	journal	December 2018
In situ inward epitaxial growth of bulk macroporous single crystals Chen, Chenlong; Sun, Shujing; Chou, Mitch M. C. Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/s41467-017-02197-6	journal	December 2017
A self-supporting bimetallic Au@Pt core-shell nanoparticle electrocatalyst for the synergistic enhancement of methanol oxidation Tan, Changhui; Sun, Yinghui; Zheng, Jianzhong Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/s41598-017-06639-5	journal	July 2017
Recent developments of nano-structured materials as the catalysts for oxygen reduction reaction Kang, SungYeon; Kim, HuiJung; Chung, Yong-Ho Nano Convergence, Vol. 5, Issue 1 https://doi.org/10.1186/s40580-018-0144-3	journal	April 2018
Engineering Ru@Pt Core-Shell Catalysts for Enhanced Electrochemical Oxygen Reduction Mass Activity and Stability Jackson, Ariel; Strickler, Alaina; Higgins, Drew Nanomaterials, Vol. 8, Issue 1 https://doi.org/10.3390/nano8010038	journal	January 2018
Solution-Grown Dendritic Pt-Based Ternary Nanostructures for Enhanced Oxygen Reduction Reaction Functionality Leteba, Gerard; Mitchell, David; Levecque, Pieter Nanomaterials, Vol. 8, Issue 7 https://doi.org/10.3390/nano8070462	journal	June 2018
Nanostructure Optimization of Platinum-Based Nanomaterials for Catalytic Applications Duan, Sibin; Du, Zhe; Fan, Hongsheng Nanomaterials, Vol. 8, Issue 11 https://doi.org/10.3390/nano8110949	journal	November 2018
Direct Spectroscopy for Probing the Critical Role of Partial Covalency in Oxygen Reduction Reaction for Cobalt-Manganese Spinel Oxides Long, Xinghui; Yu, Pengfei; Zhang, Nian Nanomaterials, Vol. 9, Issue 4 https://doi.org/10.3390/nano9040577	journal	April 2019

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