Parabolic single-crystal diamond lenses for coherent x-ray imaging
Abstract
We demonstrate parabolic single-crystal diamond compound refractive lenses designed for coherent x-ray imaging resilient to extreme thermal and radiation loading expected from next generation light sources. To ensure the preservation of coherence and resilience, the lenses are manufactured from the highest-quality single-crystalline synthetic diamond material grown by a high-pressure high-temperature technique. Picosecond laser milling is applied to machine lenses to parabolic shapes with a ≃1 μm precision and surface roughness. The compound refractive lens comprised of six lenses with a radius of curvature R=200 μm at the vertex of the parabola and a geometrical aperture A=900 μm focuses 10 keV x-ray photons from an undulator source at the Advanced Photon Source facility to a focal spot size of ≃20×90 μm2 with a gain factor of ≃50-100.
- Authors:
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1221683
- Alternate Identifier(s):
- OSTI ID: 1221644; OSTI ID: 1420523
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Journal Article: Published Article
- Journal Name:
- Applied Physics Letters
- Additional Journal Information:
- Journal Name: Applied Physics Letters Journal Volume: 107 Journal Issue: 11; Journal ID: ISSN 0003-6951
- Publisher:
- American Institute of Physics
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 43 PARTICLE ACCELERATORS; diamond; lenses; photons; single crystals; x-ray imaging
Citation Formats
Terentyev, Sergey, Blank, Vladimir, Polyakov, Sergey, Zholudev, Sergey, Snigirev, Anatoly, Polikarpov, Maxim, Kolodziej, Tomasz, Qian, Jun, Zhou, Hua, and Shvyd'ko, Yuri. Parabolic single-crystal diamond lenses for coherent x-ray imaging. United States: N. p., 2015.
Web. doi:10.1063/1.4931357.
Terentyev, Sergey, Blank, Vladimir, Polyakov, Sergey, Zholudev, Sergey, Snigirev, Anatoly, Polikarpov, Maxim, Kolodziej, Tomasz, Qian, Jun, Zhou, Hua, & Shvyd'ko, Yuri. Parabolic single-crystal diamond lenses for coherent x-ray imaging. United States. https://doi.org/10.1063/1.4931357
Terentyev, Sergey, Blank, Vladimir, Polyakov, Sergey, Zholudev, Sergey, Snigirev, Anatoly, Polikarpov, Maxim, Kolodziej, Tomasz, Qian, Jun, Zhou, Hua, and Shvyd'ko, Yuri. 2015.
"Parabolic single-crystal diamond lenses for coherent x-ray imaging". United States. https://doi.org/10.1063/1.4931357.
@article{osti_1221683,
title = {Parabolic single-crystal diamond lenses for coherent x-ray imaging},
author = {Terentyev, Sergey and Blank, Vladimir and Polyakov, Sergey and Zholudev, Sergey and Snigirev, Anatoly and Polikarpov, Maxim and Kolodziej, Tomasz and Qian, Jun and Zhou, Hua and Shvyd'ko, Yuri},
abstractNote = {We demonstrate parabolic single-crystal diamond compound refractive lenses designed for coherent x-ray imaging resilient to extreme thermal and radiation loading expected from next generation light sources. To ensure the preservation of coherence and resilience, the lenses are manufactured from the highest-quality single-crystalline synthetic diamond material grown by a high-pressure high-temperature technique. Picosecond laser milling is applied to machine lenses to parabolic shapes with a ≃1 μm precision and surface roughness. The compound refractive lens comprised of six lenses with a radius of curvature R=200 μm at the vertex of the parabola and a geometrical aperture A=900 μm focuses 10 keV x-ray photons from an undulator source at the Advanced Photon Source facility to a focal spot size of ≃20×90 μm2 with a gain factor of ≃50-100.},
doi = {10.1063/1.4931357},
url = {https://www.osti.gov/biblio/1221683},
journal = {Applied Physics Letters},
issn = {0003-6951},
number = 11,
volume = 107,
place = {United States},
year = {Mon Sep 14 00:00:00 EDT 2015},
month = {Mon Sep 14 00:00:00 EDT 2015}
}
Web of Science
Works referenced in this record:
A compound refractive lens for focusing high-energy X-rays
journal, November 1996
- Snigirev, A.; Kohn, V.; Snigireva, I.
- Nature, Vol. 384, Issue 6604
Imaging by parabolic refractive lenses in the hard X-ray range
journal, November 1999
- Lengeler, Bruno; Schroer, Christian; Tümmler, Johannes
- Journal of Synchrotron Radiation, Vol. 6, Issue 6
Hard x-ray nanoprobe based on refractive x-ray lenses
journal, September 2005
- Schroer, C. G.; Kurapova, O.; Patommel, J.
- Applied Physics Letters, Vol. 87, Issue 12
Focusing Hard X Rays to Nanometer Dimensions by Adiabatically Focusing Lenses
journal, February 2005
- Schroer, C. G.; Lengeler, B.
- Physical Review Letters, Vol. 94, Issue 5
High-Resolution Transmission X-ray Microscopy: A New Tool for Mesoscopic Materials
journal, June 2010
- Bosak, Alexey; Snigireva, Irina; Napolskii, Kirill S.
- Advanced Materials, Vol. 22, Issue 30
In situ hard X-ray microscopy of self-assembly in colloidal suspensions
journal, January 2013
- Byelov, Dmytro V.; Meijer, Janne-Mieke; Snigireva, Irina
- RSC Advances, Vol. 3, Issue 36
High-energy-resolution x-ray optics with refractive collimators
journal, July 2000
- Chumakov, A. I.; Rüffer, R.; Leupold, O.
- Applied Physics Letters, Vol. 77, Issue 1
X-ray transfocators: focusing devices based on compound refractive lenses
journal, December 2010
- Vaughan, Gavin B. M.; Wright, Jonathan P.; Bytchkov, Aleksei
- Journal of Synchrotron Radiation, Vol. 18, Issue 2
X-ray harmonics rejection on third-generation synchrotron sources using compound refractive lenses
journal, March 2014
- Polikarpov, Maxim; Snigireva, Irina; Snigirev, Anatoly
- Journal of Synchrotron Radiation, Vol. 21, Issue 3
Refractive x-ray lenses
journal, May 2005
- Lengeler, Bruno; Schroer, Christian G.; Kuhlmann, Marion
- Journal of Physics D: Applied Physics, Vol. 38, Issue 10A
Thermo-mechanical analysis and design optimization of front-end compound refractive lens
conference, November 2004
- Zhang, Lin; Snigirev, Anatoly A.; Snigireva, Irina I.
- Optical Science and Technology, the SPIE 49th Annual Meeting, SPIE Proceedings
Thermal Expansion of Diamond at Low Temperatures
journal, February 2010
- Stoupin, Stanislav; Shvyd’ko, Yuri V.
- Physical Review Letters, Vol. 104, Issue 8
Ultraprecise studies of the thermal expansion coefficient of diamond using backscattering x-ray diffraction
journal, March 2011
- Stoupin, Stanislav; Shvyd’ko, Yuri V.
- Physical Review B, Vol. 83, Issue 10
Diamond monochromator for high heat flux synchrotron x-ray beams
conference, February 1993
- Khounsary, Ali M.; Smither, Robert K.; Davey, Steve
- San Diego '92, SPIE Proceedings
Diamond crystal X-ray optics for high-power-density synchrotron radiation beams
journal, June 1993
- Berman, Lonny E.; Hastings, J. B.; Peter Siddons, D.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 329, Issue 3
Diamond single crystals: the ultimate monochromator material for high-power x-ray beams
journal, February 1995
- Freund, Andreas K.
- Optical Engineering, Vol. 34, Issue 2
Test of a high-heat-load double-crystal diamond monochromator at the Advanced Photon Source
journal, December 1997
- Fernandez, P. B.; Graber, T.; Lee, W. -K
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 400, Issue 2-3
Near-100% Bragg reflectivity of X-rays
journal, August 2011
- Shvyd'ko, Yuri; Stoupin, Stanislav; Blank, Vladimir
- Nature Photonics, Vol. 5, Issue 9
Demonstration of self-seeding in a hard-X-ray free-electron laser
journal, August 2012
- Amann, J.; Berg, W.; Blank, V.
- Nature Photonics, Vol. 6, Issue 10, p. 693-698
Hybrid diamond-silicon angular-dispersive x-ray monochromator with 0.25-meV energy bandwidth and high spectral efficiency
journal, January 2013
- Stoupin, S.; Shvyd’ko, Y. V.; Shu, D.
- Optics Express, Vol. 21, Issue 25, p. 30932-30946
All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source
journal, August 2014
- Stoupin, S.; Terentyev, S. A.; Blank, V. D.
- Journal of Applied Crystallography, Vol. 47, Issue 4, p. 1329-1336
Large-acceptance diamond planar refractive lenses manufactured by laser cutting
journal, January 2015
- Polikarpov, Maxim; Snigireva, Irina; Morse, John
- Journal of Synchrotron Radiation, Vol. 22, Issue 1
HPHT growth and x-ray characterization of high-quality type IIa diamond
journal, August 2009
- Burns, R. C.; Chumakov, A. I.; Connell, S. H.
- Journal of Physics: Condensed Matter, Vol. 21, Issue 36
Characterization of top-quality type IIa synthetic diamonds for new X-ray optics
journal, May 2011
- Polyakov, S. N.; Denisov, V. N.; Kuzmin, N. V.
- Diamond and Related Materials, Vol. 20, Issue 5-6, p. 726-728
Large Defect-Free Synthetic Type IIa Diamond Crystals Synthesized via High Pressure and High Temperature
journal, September 2012
- Sumiya, Hitoshi; Tamasaku, Kenji
- Japanese Journal of Applied Physics, Vol. 51, Issue 9R
The influence of crystallization temperature and boron concentration in growth environment on its distribution in growth sectors of type IIb diamond
journal, April 2007
- Blank, V. D.; Kuznetsov, M. S.; Nosukhin, S. A.
- Diamond and Related Materials, Vol. 16, Issue 4-7
Basic Energy Sciences Synchrotron Radiation Center Undulator Sector at the Advanced Photon Source
journal, July 2001
- Beno, M. A.; Jennings, G.; Engbretson, M.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 467-468
X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92
journal, July 1993
- Henke, B. L.; Gullikson, E. M.; Davis, J. C.
- Atomic Data and Nuclear Data Tables, Vol. 54, Issue 2, p. 181-342
Energy-dispersive phase plate for magnetic circular dichroism experiments in the X-ray range
journal, June 1994
- Giles, C.; Malgrange, C.; Goulon, J.
- Journal of Applied Crystallography, Vol. 27, Issue 3
Transparent Nondiffracting Polarization Rotation Regime: A Synchrotron X-ray Study
journal, July 1995
- Bloch, J. M.; Baysal, M. A.; Travis, A. B.
- Physical Review Letters, Vol. 75, Issue 2