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Title: Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source

Abstract

Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X-rays by spectral division using a near-perfect diamond thin-crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. In this report, the structure determination of a prototypical protein was performed using serial femtosecond crystallography simultaneously with a femtosecond time-resolved XANES studies of photoexcited spin transition dynamics in an iron spin-crossover system. The results of both experiments using the multiplexed beams are similar to those obtained separately, using a dedicated beam, with no significant differences in quality.

Authors:
 [1];  [1];  [2];  [3];  [2];  [1];  [1];  [2];  [1];  [1];  [1];  [1];  [2];  [1];  [2];  [2];  [4];  [1];  [1];  [4] more »;  [3];  [1];  [1];  [1];  [1] « less
  1. SLAC National Accelerator Laboratory, Menlo Park, CA (United States)
  2. Max-Planck Institute for Medical Research, Heidelberg (Germany)
  3. Technological Institute for Superhard and Novel Carbon Materials, Troitsk (Russia)
  4. Argonne National Lab. (ANL), Argonne, IL (United States)
Publication Date:
Research Org.:
SLAC National Accelerator Lab., Menlo Park, CA (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
1189942
Alternate Identifier(s):
OSTI ID: 1225049; OSTI ID: 1390944
Grant/Contract Number:  
AC02-06CH11357; AC03-76SF00515
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 22; Journal Issue: 3; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
43 PARTICLE ACCELERATORS; FEL; X-ray; multiplexing diamond; thin-crystal; 71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS

Citation Formats

Feng, Y., Alonso-Mori, R., Barends, T. R. M., Blank, V. D., Botha, S., Chollet, M., Damiani, D. S., Doak, R. B., Glownia, J. M., Koglin, J. M., Lemke, H. T., Messerschmidt, M., Nass, K., Nelson, S., Schlichting, I., Shoeman, R. L., Shvyd'ko, Yu. V., Sikorski, M., Song, S., Stoupin, S., Terentyev, S., Williams, G. J., Zhu, D., Robert, A., and Boutet, S. Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source. United States: N. p., 2015. Web. doi:10.1107/S1600577515003999.
Feng, Y., Alonso-Mori, R., Barends, T. R. M., Blank, V. D., Botha, S., Chollet, M., Damiani, D. S., Doak, R. B., Glownia, J. M., Koglin, J. M., Lemke, H. T., Messerschmidt, M., Nass, K., Nelson, S., Schlichting, I., Shoeman, R. L., Shvyd'ko, Yu. V., Sikorski, M., Song, S., Stoupin, S., Terentyev, S., Williams, G. J., Zhu, D., Robert, A., & Boutet, S. Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source. United States. doi:10.1107/S1600577515003999.
Feng, Y., Alonso-Mori, R., Barends, T. R. M., Blank, V. D., Botha, S., Chollet, M., Damiani, D. S., Doak, R. B., Glownia, J. M., Koglin, J. M., Lemke, H. T., Messerschmidt, M., Nass, K., Nelson, S., Schlichting, I., Shoeman, R. L., Shvyd'ko, Yu. V., Sikorski, M., Song, S., Stoupin, S., Terentyev, S., Williams, G. J., Zhu, D., Robert, A., and Boutet, S. Fri . "Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source". United States. doi:10.1107/S1600577515003999. https://www.osti.gov/servlets/purl/1189942.
@article{osti_1189942,
title = {Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source},
author = {Feng, Y. and Alonso-Mori, R. and Barends, T. R. M. and Blank, V. D. and Botha, S. and Chollet, M. and Damiani, D. S. and Doak, R. B. and Glownia, J. M. and Koglin, J. M. and Lemke, H. T. and Messerschmidt, M. and Nass, K. and Nelson, S. and Schlichting, I. and Shoeman, R. L. and Shvyd'ko, Yu. V. and Sikorski, M. and Song, S. and Stoupin, S. and Terentyev, S. and Williams, G. J. and Zhu, D. and Robert, A. and Boutet, S.},
abstractNote = {Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X-rays by spectral division using a near-perfect diamond thin-crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. In this report, the structure determination of a prototypical protein was performed using serial femtosecond crystallography simultaneously with a femtosecond time-resolved XANES studies of photoexcited spin transition dynamics in an iron spin-crossover system. The results of both experiments using the multiplexed beams are similar to those obtained separately, using a dedicated beam, with no significant differences in quality.},
doi = {10.1107/S1600577515003999},
journal = {Journal of Synchrotron Radiation (Online)},
number = 3,
volume = 22,
place = {United States},
year = {Fri Apr 10 00:00:00 EDT 2015},
month = {Fri Apr 10 00:00:00 EDT 2015}
}

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Works referenced in this record:

Characterization of top-quality type IIa synthetic diamonds for new X-ray optics
journal, May 2011

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Gas dynamic virtual nozzle for generation of microscopic droplet streams
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Diamond crystal optics for self-seeding of hard X-rays in X-ray free-electron lasers
journal, March 2013