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Title: Quantitative Total and Diffuse Reflectance Laboratory Measurements for Remote, Standoff, and Point Sensing

Conference ·
DOI:https://doi.org/10.1117/12.2054116· OSTI ID:1159020

Methods for making total and diffuse directional/hemispherical reflectance measurements in the shortwave to longwave infrared using an integrating sphere are described. The sphere is a commercial, off-the-shelf optical device with its sample port at the bottom, which is essential for examining powdered samples without using a cover glass. The reflectance spectra of recently-developed National Institute of Standards and Technology (NIST, USA) infrared reflectance standards have been measured using the sphere. Reflectance spectra of other materials such as Spectralon and Infragold were also measured. The relative systematic error for the total reflectance measurements is estimated to be on the order of 3%, and random measurement error for multiple samples of each material is on the order of 0.5%.

Research Organization:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-76RL01830
OSTI ID:
1159020
Report Number(s):
PNNL-SA-103272; NN2001000
Resource Relation:
Conference: Chemical, Biological, Radiological, Nuclear, and Explosives (CBRNE) Sensing XV, May 5, 2014, Baltimore, Maryland. Proceedings of the SPIE, 9073:Paper No. 907303
Country of Publication:
United States
Language:
English