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Title: Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210

Abstract

This data package contains the K Basin sludge characterization results obtained by Pacific Northwest National Laboratory during processing and analysis of four sludge core samples collected from Engineered Container SCS-CON-210 in 2010 as requested by CH2M Hill Plateau Remediation Company. Sample processing requirements, analytes of interest, detection limits, and quality control sample requirements are defined in the KBC-33786, Rev. 2. The core processing scope included reconstitution of a sludge core sample distributed among four to six 4-L polypropylene bottles into a single container. The reconstituted core sample was then mixed and subsampled to support a variety of characterization activities. Additional core sludge subsamples were combined to prepare a container composite. The container composite was fractionated by wet sieving through a 2,000 micron mesh and a 500-micron mesh sieve. Each sieve fraction was sampled to support a suite of analyses. The core composite analysis scope included density determination, radioisotope analysis, and metals analysis, including the Waste Isolation Pilot Plant Hazardous Waste Facility Permit metals (with the exception of mercury). The container composite analysis included most of the core composite analysis scope plus particle size distribution, particle density, rheology, and crystalline phase identification. A summary of the received samples, core sample reconstitutionmore » and subsampling activities, container composite preparation and subsampling activities, physical properties, and analytical results are presented. Supporting data and documentation are provided in the appendices. There were no cases of sample or data loss and all of the available samples and data are reported as required by the Quality Assurance Project Plan/Sampling and Analysis Plan.« less

Authors:
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Publication Date:
Research Org.:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1095442
Report Number(s):
PNNL-20650 Rev. 2
830403000
DOE Contract Number:
AC05-76RL01830
Resource Type:
Technical Report
Country of Publication:
United States
Language:
English
Subject:
K Basin; sludge; core sampling; tank waste

Citation Formats

Fountain, Matthew S., Fiskum, Sandra K., Baldwin, David L., Daniel, Richard C., Bos, Stanley J., Burns, Carolyn A., Carlson, Clark D., Coffey, Deborah S., Delegard, Calvin H., Edwards, Matthew K., Greenwood, Lawrence R., Neiner, Doinita, Oliver, Brian M., Pool, Karl N., Schmidt, Andrew J., Shimskey, Rick W., Sinkov, Sergey I., Snow, Lanee A., Soderquist, Chuck Z., Thompson, Christopher J., Trang-Le, Truc LT, and Urie, Michael W. Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210. United States: N. p., 2013. Web. doi:10.2172/1095442.
Fountain, Matthew S., Fiskum, Sandra K., Baldwin, David L., Daniel, Richard C., Bos, Stanley J., Burns, Carolyn A., Carlson, Clark D., Coffey, Deborah S., Delegard, Calvin H., Edwards, Matthew K., Greenwood, Lawrence R., Neiner, Doinita, Oliver, Brian M., Pool, Karl N., Schmidt, Andrew J., Shimskey, Rick W., Sinkov, Sergey I., Snow, Lanee A., Soderquist, Chuck Z., Thompson, Christopher J., Trang-Le, Truc LT, & Urie, Michael W. Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210. United States. doi:10.2172/1095442.
Fountain, Matthew S., Fiskum, Sandra K., Baldwin, David L., Daniel, Richard C., Bos, Stanley J., Burns, Carolyn A., Carlson, Clark D., Coffey, Deborah S., Delegard, Calvin H., Edwards, Matthew K., Greenwood, Lawrence R., Neiner, Doinita, Oliver, Brian M., Pool, Karl N., Schmidt, Andrew J., Shimskey, Rick W., Sinkov, Sergey I., Snow, Lanee A., Soderquist, Chuck Z., Thompson, Christopher J., Trang-Le, Truc LT, and Urie, Michael W. Tue . "Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210". United States. doi:10.2172/1095442. https://www.osti.gov/servlets/purl/1095442.
@article{osti_1095442,
title = {Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210},
author = {Fountain, Matthew S. and Fiskum, Sandra K. and Baldwin, David L. and Daniel, Richard C. and Bos, Stanley J. and Burns, Carolyn A. and Carlson, Clark D. and Coffey, Deborah S. and Delegard, Calvin H. and Edwards, Matthew K. and Greenwood, Lawrence R. and Neiner, Doinita and Oliver, Brian M. and Pool, Karl N. and Schmidt, Andrew J. and Shimskey, Rick W. and Sinkov, Sergey I. and Snow, Lanee A. and Soderquist, Chuck Z. and Thompson, Christopher J. and Trang-Le, Truc LT and Urie, Michael W.},
abstractNote = {This data package contains the K Basin sludge characterization results obtained by Pacific Northwest National Laboratory during processing and analysis of four sludge core samples collected from Engineered Container SCS-CON-210 in 2010 as requested by CH2M Hill Plateau Remediation Company. Sample processing requirements, analytes of interest, detection limits, and quality control sample requirements are defined in the KBC-33786, Rev. 2. The core processing scope included reconstitution of a sludge core sample distributed among four to six 4-L polypropylene bottles into a single container. The reconstituted core sample was then mixed and subsampled to support a variety of characterization activities. Additional core sludge subsamples were combined to prepare a container composite. The container composite was fractionated by wet sieving through a 2,000 micron mesh and a 500-micron mesh sieve. Each sieve fraction was sampled to support a suite of analyses. The core composite analysis scope included density determination, radioisotope analysis, and metals analysis, including the Waste Isolation Pilot Plant Hazardous Waste Facility Permit metals (with the exception of mercury). The container composite analysis included most of the core composite analysis scope plus particle size distribution, particle density, rheology, and crystalline phase identification. A summary of the received samples, core sample reconstitution and subsampling activities, container composite preparation and subsampling activities, physical properties, and analytical results are presented. Supporting data and documentation are provided in the appendices. There were no cases of sample or data loss and all of the available samples and data are reported as required by the Quality Assurance Project Plan/Sampling and Analysis Plan.},
doi = {10.2172/1095442},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Sep 10 00:00:00 EDT 2013},
month = {Tue Sep 10 00:00:00 EDT 2013}
}

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