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Title: Development of a Rubber-Based Product Using a Mixture Experiment: A Challenging Case Study

Journal Article · · Progress in Rubber, Plastics, and Recycling Technology, 29(3):123-149
OSTI ID:1087807

Many products used in daily life are made by blending two or more components. The properties of such products typically depend on the relative proportions of the components. Experimental design, modeling, and data analysis methods for mixture experiments provide for efficiently determining the component proportions that will yield a product with desired properties. This article presents a case study of the work performed to develop a new rubber formulation for an o-ring (a circular gasket) with requirements specified on 10 product properties. Each step of the study is discussed, including: 1) identifying the objective of the study and requirements for properties of the o-ring, 2) selecting the components to vary and specifying the component constraints, 3) constructing a mixture experiment design, 4) measuring the responses and assessing the data, 5) developing property-composition models, 6) selecting the new product formulation, and 7) confirming the selected formulation in manufacturing. The case study includes some challenging and new aspects, which are discussed in the article.

Research Organization:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-76RL01830
OSTI ID:
1087807
Report Number(s):
PNNL-SA-85221
Journal Information:
Progress in Rubber, Plastics, and Recycling Technology, 29(3):123-149, Journal Name: Progress in Rubber, Plastics, and Recycling Technology, 29(3):123-149
Country of Publication:
United States
Language:
English