Methods for synthesizing alane without the formation of adducts and free of halides

Zidan, Ragaiy; Knight, Douglas A; Dinh, Long V

Title: Methods for synthesizing alane without the formation of adducts and free of halides

Patent · Tue Feb 19 00:00:00 EST 2013

OSTI ID:1082922

Zidan, Ragaiy; Knight, Douglas A; Dinh, Long V

A process is provided to synthesize an alane without the formation of alane adducts as a precursor. The resulting product is a crystallized .alpha.-alane and is a highly stable product and is free of halides.

View Patent

Cite

Export

Save

Research Organization:: Savannah River National Laboratory (SRNL), Aiken, SC (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC09-08SR22470

Assignee:: Savannah River Nuclear Solutions, LLC (Aiken, SC)

Patent Number(s):: 8,377,415

Application Number:: 13/313,472

OSTI ID:: 1082922

Country of Publication:: United States

Language:: English

References (10)

Process for Preparing Crystalline, Non-solvated Aluminum Hydride Schmidt, Donald L.; Diesen, Ronald W. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3840654 US Patent Document 3,840,654	patent	October 1974
Stabilized aluminum hydride polymorphs Petrie, Mark A.; Bottaro, Jeffrey C.; Schmitt, Robert J. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6617064 US Patent Document 6,617,064	patent	September 2003
Method for synthesizing aluminum hydride Klapdor, Astrid; Knott, Wilfried; Windbiel, Dagmar https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5670129 US Patent Document 5,670,129	patent	September 1997
Hydrogen storage materials and method of making by dry homogenation Jensen, Craig M.; Zidan, Ragaiy https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6471935 US Patent Document 6,471,935	patent	October 2002
Direct synthesis of catalyzed hydride compounds Gross, Karl J.; Majzoub, Eric https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6793909 US Patent Document 6,793,909	patent	September 2004
Method of fabrication of complex alkali metal hydrides Zaluska, Alicja; Zaluski, Leszek; Strom-Olsen, John https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6251349 US Patent Document 6,251,349	patent	June 2001
Direct crystallization of aluminum hydride from toluene-ether Scruggs, James A. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3801657 US Patent Document 3801657	patent	April 1974
Characterisation of mechanochemically synthesised alane (AlH3) nanoparticles Paskevicius, M.; Sheppard, D. A.; Buckley, C. E. Journal of Alloys and Compounds, Vol. 487, Issue 1-2 https://doi.org/10.1016/j.jallcom.2009.07.124	journal	November 2009
A Process for Preparing Lithium Aluminum Hydride-Aluminum Hydride Complexes Brower, Frank M.; Daniels, Arthur L.; Fujioka, George S. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3816192 US Patent Document 3816192	patent	June 1974
Stable hydrocarbon solutions of aluminum hydride Hoffman, Doyt K.; Bach, Ricardo O.; Kamienski, Conrad W. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4006095 US Patent Document 4,006,095	patent	February 1977

Similar Records

Formation of high quality alane

Patent · Tue Sep 27 00:00:00 EDT 2022 · OSTI ID:1082922

Zidan, Ragaiy; McWhorter, Christopher S.; Ward, Patrick A.

Mechanochemical solid/liquid reaction in formation of alane

Patent · Tue Nov 27 00:00:00 EST 2018 · OSTI ID:1082922

Zidan, Ragaiy; Ward, Patrick A.

CsI-Antisolvent Adduct Formation in All-Inorganic Metal Halide Perovskites

Journal Article · Fri Jan 31 00:00:00 EST 2020 · Advanced Energy Materials · OSTI ID:1082922

Moot, Taylor; Marshall, Ashley R.; Wheeler, Lance M.; +9 more

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Title: Methods for synthesizing alane without the formation of adducts and free of halides

Citation Formats

References (10)

Similar Records

Related Subjects