High strength air-dried aerogels

Patent · Tue Nov 06 00:00:00 EST 2012

OSTI ID:1080443

Coronado, Paul R.; Satcher, Jr., Joe H.

A method for the preparation of high strength air-dried organic aerogels. The method involves the sol-gel polymerization of organic gel precursors, such as resorcinol with formaldehyde (RF) in aqueous solvents with R/C ratios greater than about 1000 and R/F ratios less than about 1:2.1. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be air dried at ambient temperatures and pressures. The method significantly reduces the time and/or energy required to produce a dried aerogel compared to conventional methods using either supercritical solvent extraction. The air dried gel exhibits typically less than 5% shrinkage.

• Research Organization: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
• Sponsoring Organization: USDOE
• DOE Contract Number: W-7405-ENG-48
• Assignee: Lawrence Livermore National Security, LLC (Livermore, CA)
• Patent Number(s): 8,304,465
• Application Number: 11/335,297
• OSTI ID: 1080443
• Country of Publication: United States
• Language: English

Related Subjects

36 MATERIALS SCIENCE