Thickness measurements of nanoscale brine films on silica surfaces under geologic CO2 sequestration conditions using synchrotron X-ray fluorescence

Kim, Tae Wook; Tokunaga, Tetsu K.; Shuman, Derek B.; Sutton, Stephen R.; Newville, Matt; Lanzirotti, Antonio

doi:10.1029/2012WR012200

Title: Thickness measurements of nanoscale brine films on silica surfaces under geologic CO₂ sequestration conditions using synchrotron X-ray fluorescence

Authors:: Kim, Tae Wook; Tokunaga, Tetsu K.; Shuman, Derek B.; Sutton, Stephen R.; Newville, Matt; Lanzirotti, Antonio

Publication Date:: Sat Sep 01 00:00:00 EDT 2012

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Org.:: DOE - BASIC ENERGY SCIENCES

OSTI Identifier:: 1054002

Resource Type:: Journal Article

Journal Name:: Water Resources Research

Additional Journal Information:: Journal Volume: 48; Journal Issue: 9; Journal ID: ISSN 0043-1397

Publisher:: American Geophysical Union (AGU)

Country of Publication:: United States

Language:: ENGLISH

Citation Formats


                    Kim, Tae Wook, Tokunaga, Tetsu K., Shuman, Derek B., Sutton, Stephen R., Newville, Matt, and Lanzirotti, Antonio. Thickness measurements of nanoscale brine films on silica surfaces under geologic CO2 sequestration conditions using synchrotron X-ray fluorescence.  United States: N. p., 2012. 
        Web.  doi:10.1029/2012WR012200.

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                    Kim, Tae Wook, Tokunaga, Tetsu K., Shuman, Derek B., Sutton, Stephen R., Newville, Matt, & Lanzirotti, Antonio. Thickness measurements of nanoscale brine films on silica surfaces under geologic CO2 sequestration conditions using synchrotron X-ray fluorescence.  United States.  https://doi.org/10.1029/2012WR012200

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                    Kim, Tae Wook, Tokunaga, Tetsu K., Shuman, Derek B., Sutton, Stephen R., Newville, Matt, and Lanzirotti, Antonio. 2012.  
        "Thickness measurements of nanoscale brine films on silica surfaces under geologic CO2 sequestration conditions using synchrotron X-ray fluorescence".  United States.  https://doi.org/10.1029/2012WR012200.

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@article{osti_1054002,

  title        = {Thickness measurements of nanoscale brine films on silica surfaces under geologic CO2 sequestration conditions using synchrotron X-ray fluorescence},

  author       = {Kim, Tae Wook and Tokunaga, Tetsu K. and Shuman, Derek B. and Sutton, Stephen R. and Newville, Matt and Lanzirotti, Antonio},

  abstractNote = {},

  doi          = {10.1029/2012WR012200},

  url          = {https://www.osti.gov/biblio/1054002},
  journal      = {Water Resources Research},

  issn         = {0043-1397},

  number       = 9,

  volume       = 48,

  place        = {United States},

  year         = {Sat Sep 01 00:00:00 EDT 2012},

  month        = {Sat Sep 01 00:00:00 EDT 2012}

}

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https://doi.org/10.1029/2012WR012200

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CO ₂ Wettability of Sandstones: Addressing Conflicting Capillary Behaviors
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Title: Thickness measurements of nanoscale brine films on silica surfaces under geologic CO2 sequestration conditions using synchrotron X-ray fluorescence

Citation Formats

Moisture Characteristics of Hanford Gravels journal, January 2003

Fluid–Fluid and Solid–Fluid Interfacial Interactions in Petroleum Reservoirs journal, March 2001

CO2-H2O mixtures in the geological sequestration of CO2. I. Assessment and calculation of mutual solubilities from 12 to 100°C and up to 600 bar journal, August 2003

DLVO-Based Estimates of Adsorbed Water Film Thicknesses in Geologic CO 2 Reservoirs journal, May 2012

Hydraulic properties of adsorbed water films in unsaturated porous media: HYDRAULIC PROPERTIES OF ADSORBED WATER FILMS journal, June 2009

An Experimental Investigation of the Effect of Temperature on Recovery of Heavy Oil From Diatomite journal, June 2004

Unsaturated Hydraulic Conductivity of Structured Porous Media journal, January 2002

Numerical modeling of injection and mineral trapping of CO2 with H2S and SO2 in a sandstone formation journal, August 2007

Reactive transport modelling of CO 2 storage in saline aquifers to elucidate fundamental processes, trapping mechanisms and sequestration partitioning journal, January 2004

Stability of thin aqueous films on solid surfaces journal, March 1992

Object-oriented approach for the pore-scale simulation of DC electrical conductivity of two-phase saturated porous media journal, March 2008

Capillary Alteration of Caprocks by Acid Gases conference, April 2013

Analysis of Adsorption Behavior of Cations onto Quartz Surface by Electrical Double-layer Model journal, December 1999

Global and regional drivers of accelerating CO2 emissions journal, May 2007

Wettability: Fundamentals and Surface Forces journal, June 1991

Influence of Aqueous pH on the Interfacial Properties of Coal Tar journal, May 1999

Wettability alteration and oil recovery by water imbibition at elevated temperatures journal, June 2006

The Role of Attractive and Repulsive Forces in the Formation of Tactoids, Thixotropic Gels, Protein Crystals and Coacervates journal, December 1938

Liquid retention and interfacial area in variably saturated porous media: Upscaling from single-pore to sample-scale model journal, October 1999

Wettability alteration of caprock minerals by carbon dioxide journal, May 2007

Experimental evaluation of mixed fluid reactions between supercritical carbon dioxide and NaCl brine: Relevance to the integrity of a geologic carbon repository journal, April 2005

Physicochemical controls on adsorbed water film thickness in unsaturated geological media: PHYSICOCHEMICAL CONTROLS ON ADSORBED WATER FILM THICKNESS journal, August 2011

Externally controlled pressure and temperature microreactor for in situ x-ray diffraction, visual and spectroscopic reaction investigations under supercritical and subcritical conditions journal, January 2005

Quantifying the Dimensions of Nanoscale Organic Surface Layers in Natural Waters journal, February 2007

Reservoir Simulation of CO<sub>2</sub> Storage in Aquifers journal, September 2005

Pore-Scale Analysis of Evaporation and Condensation Dynamics in Porous Media journal, September 2010

Transient film flow on rough fracture surfaces journal, July 2000

Capillary pressure and heterogeneity for the CO2/water system in sandstone rocks at reservoir conditions journal, March 2012

Vapor adsorption on mica and silicon: entropy effects, layering, and surface forces journal, April 1992

Geological storage of carbon dioxide by residual gas and solubility trapping journal, January 2008

Measurement of Critical Disjoining Pressure for Dewetting of Solid Surfaces journal, August 1996

X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92 journal, July 1993

CO2-H2O mixtures in the geological sequestration of CO2. II. Partitioning in chloride brines at 12–100°C and up to 600 bar journal, July 2005

Water film flow along fracture surfaces of porous rock journal, June 1997

Interaction of unequal double layers at constant charge journal, April 1975

Adsorption and capillary condensation on rough surfaces journal, June 1978

Thickness and structure of the water film deposited from vapour on calcite surfaces journal, November 2010

A new high pressure sapphire nuclear magnetic resonance cell journal, January 1996

Wettability estimation of low-permeability, siliceous shale using surface forces journal, December 2010

Seismic properties of pore fluids journal, November 1992

Mechanical strength of sapphire windows under pressure journal, August 1994

Preliminary indications from atomic force microscopy of the presence of rapidly-formed nanoscale films on aquifer material surfaces journal, August 2009

At the limit of polychromatic microdiffraction journal, October 2009

Aqueous Wetting Films on Fused Quartz journal, June 1999

Ellipsometry as a tool to study the adsorption behavior of synthetic and biopolymers at the air-water interface journal, July 1978

Spectroscopic Ellipsometry Investigation of the Swelling of Poly(Dimethylsiloxane) Thin Films with High Pressure Carbon Dioxide journal, February 2001

Dewetting of Silica Surfaces upon Reactions with Supercritical CO 2 and Brine: Pore-Scale Studies in Micromodels journal, March 2012

Interfacial Tension between CO 2 , Freshwater, and Brine in the Range of Pressure from (2 to 27) MPa, Temperature from (20 to 125) °C, and Water Salinity from (0 to 334 000) mg·L −1 journal, March 2009

Physically-based network modeling of multiphase flow in intermediate-wet porous media journal, June 1998

Closure of random elastic surfaces in contact journal, June 1985

The effects of substrate roughness on ultrathin water films journal, June 1989

Influence of Electrical Surface Charges on the Wetting Properties of Crude Oils journal, August 1989

In Situ Infrared Spectroscopic Study of Forsterite Carbonation in Wet Supercritical CO 2 journal, July 2011

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Interrelationship between water film thicknesses and contact angles and a model for CO 2 adhesion journal, April 2019

Title: Thickness measurements of nanoscale brine films on silica surfaces under geologic CO₂ sequestration conditions using synchrotron X-ray fluorescence

Moisture Characteristics of Hanford Gravels
journal, January 2003

Fluid–Fluid and Solid–Fluid Interfacial Interactions in Petroleum Reservoirs
journal, March 2001

CO₂-H₂O mixtures in the geological sequestration of CO₂. I. Assessment and calculation of mutual solubilities from 12 to 100°C and up to 600 bar
journal, August 2003

DLVO-Based Estimates of Adsorbed Water Film Thicknesses in Geologic CO ₂ Reservoirs
journal, May 2012

Hydraulic properties of adsorbed water films in unsaturated porous media: HYDRAULIC PROPERTIES OF ADSORBED WATER FILMS
journal, June 2009

An Experimental Investigation of the Effect of Temperature on Recovery of Heavy Oil From Diatomite
journal, June 2004

Unsaturated Hydraulic Conductivity of Structured Porous Media
journal, January 2002

Numerical modeling of injection and mineral trapping of CO2 with H2S and SO2 in a sandstone formation
journal, August 2007

Reactive transport modelling of CO ₂ storage in saline aquifers to elucidate fundamental processes, trapping mechanisms and sequestration partitioning
journal, January 2004

Stability of thin aqueous films on solid surfaces
journal, March 1992

Object-oriented approach for the pore-scale simulation of DC electrical conductivity of two-phase saturated porous media
journal, March 2008

Capillary Alteration of Caprocks by Acid Gases
conference, April 2013

Analysis of Adsorption Behavior of Cations onto Quartz Surface by Electrical Double-layer Model
journal, December 1999

Global and regional drivers of accelerating CO2 emissions
journal, May 2007

Wettability: Fundamentals and Surface Forces
journal, June 1991

Influence of Aqueous pH on the Interfacial Properties of Coal Tar
journal, May 1999

Wettability alteration and oil recovery by water imbibition at elevated temperatures
journal, June 2006

The Role of Attractive and Repulsive Forces in the Formation of Tactoids, Thixotropic Gels, Protein Crystals and Coacervates
journal, December 1938

Liquid retention and interfacial area in variably saturated porous media: Upscaling from single-pore to sample-scale model
journal, October 1999

Wettability alteration of caprock minerals by carbon dioxide
journal, May 2007

Experimental evaluation of mixed fluid reactions between supercritical carbon dioxide and NaCl brine: Relevance to the integrity of a geologic carbon repository
journal, April 2005

Physicochemical controls on adsorbed water film thickness in unsaturated geological media: PHYSICOCHEMICAL CONTROLS ON ADSORBED WATER FILM THICKNESS
journal, August 2011

Externally controlled pressure and temperature microreactor for in situ x-ray diffraction, visual and spectroscopic reaction investigations under supercritical and subcritical conditions
journal, January 2005

Quantifying the Dimensions of Nanoscale Organic Surface Layers in Natural Waters
journal, February 2007

Reservoir Simulation of CO<sub>2</sub> Storage in Aquifers
journal, September 2005

Pore-Scale Analysis of Evaporation and Condensation Dynamics in Porous Media
journal, September 2010

Transient film flow on rough fracture surfaces
journal, July 2000

Capillary pressure and heterogeneity for the CO2/water system in sandstone rocks at reservoir conditions
journal, March 2012

Vapor adsorption on mica and silicon: entropy effects, layering, and surface forces
journal, April 1992

Geological storage of carbon dioxide by residual gas and solubility trapping
journal, January 2008

Measurement of Critical Disjoining Pressure for Dewetting of Solid Surfaces
journal, August 1996

X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92
journal, July 1993

CO2-H2O mixtures in the geological sequestration of CO2. II. Partitioning in chloride brines at 12–100°C and up to 600 bar
journal, July 2005

Water film flow along fracture surfaces of porous rock
journal, June 1997

Interaction of unequal double layers at constant charge
journal, April 1975

Adsorption and capillary condensation on rough surfaces
journal, June 1978

Thickness and structure of the water film deposited from vapour on calcite surfaces
journal, November 2010

A new high pressure sapphire nuclear magnetic resonance cell
journal, January 1996

Wettability estimation of low-permeability, siliceous shale using surface forces
journal, December 2010

Seismic properties of pore fluids
journal, November 1992

Mechanical strength of sapphire windows under pressure
journal, August 1994

Preliminary indications from atomic force microscopy of the presence of rapidly-formed nanoscale films on aquifer material surfaces
journal, August 2009

At the limit of polychromatic microdiffraction
journal, October 2009

Aqueous Wetting Films on Fused Quartz
journal, June 1999

Ellipsometry as a tool to study the adsorption behavior of synthetic and biopolymers at the air-water interface
journal, July 1978

Spectroscopic Ellipsometry Investigation of the Swelling of Poly(Dimethylsiloxane) Thin Films with High Pressure Carbon Dioxide
journal, February 2001

Dewetting of Silica Surfaces upon Reactions with Supercritical CO ₂ and Brine: Pore-Scale Studies in Micromodels
journal, March 2012

Interfacial Tension between CO ₂ , Freshwater, and Brine in the Range of Pressure from (2 to 27) MPa, Temperature from (20 to 125) °C, and Water Salinity from (0 to 334 000) mg·L ⁻¹
journal, March 2009

Physically-based network modeling of multiphase flow in intermediate-wet porous media
journal, June 1998

Closure of random elastic surfaces in contact
journal, June 1985

The effects of substrate roughness on ultrathin water films
journal, June 1989

Influence of Electrical Surface Charges on the Wetting Properties of Crude Oils
journal, August 1989

In Situ Infrared Spectroscopic Study of Forsterite Carbonation in Wet Supercritical CO ₂
journal, July 2011

CO ₂ Wettability of Sandstones: Addressing Conflicting Capillary Behaviors
journal, January 2019

Pore‐Scale Modeling of Fluid‐Fluid Interfacial Area in Variably Saturated Porous Media Containing Microscale Surface Roughness
journal, January 2020

Interrelationship between water film thicknesses and contact angles and a model for CO ₂ adhesion
journal, April 2019