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Title: Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions

Abstract

The formation and evolution of ceria nanoparticles during hydrothermal synthesis was investigated by in-situ total scattering and powder diffraction. The nucleation of pristine crystalline ceria nanoparticles originated from previously unknown cerium dimer complexes. The nanoparticle growth was highly accelerated under supercritical conditions.

Authors:
; ; ; ; ; ; ; ; ; ;  [1];  [2]
  1. (Aarhus)
  2. (
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Org.:
FOREIGNNSF
OSTI Identifier:
1051113
Resource Type:
Journal Article
Journal Name:
Angew. Chem. Int. Ed.
Additional Journal Information:
Journal Volume: 51; Journal Issue: (36) ; 09, 2012; Journal ID: ISSN 1433-7851
Country of Publication:
United States
Language:
ENGLISH
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; CERIUM; DIFFRACTION; DIMERS; HYDROTHERMAL SYNTHESIS; NUCLEATION; SCATTERING

Citation Formats

Tyrsted, Christoffer, Ørnsbjerg, #8197, Jensen, Kirsten Marie, Bøjesen, Espen Drath, Lock, Nina, Christensen, Mogens, Billinge, Simon J.L., Brummerstedt, #8197, Iversen, Bo, and Columbia). Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions. United States: N. p., 2012. Web. doi:10.1002/anie.201204747.
Tyrsted, Christoffer, Ørnsbjerg, #8197, Jensen, Kirsten Marie, Bøjesen, Espen Drath, Lock, Nina, Christensen, Mogens, Billinge, Simon J.L., Brummerstedt, #8197, Iversen, Bo, & Columbia). Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions. United States. doi:10.1002/anie.201204747.
Tyrsted, Christoffer, Ørnsbjerg, #8197, Jensen, Kirsten Marie, Bøjesen, Espen Drath, Lock, Nina, Christensen, Mogens, Billinge, Simon J.L., Brummerstedt, #8197, Iversen, Bo, and Columbia). Tue . "Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions". United States. doi:10.1002/anie.201204747.
@article{osti_1051113,
title = {Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions},
author = {Tyrsted, Christoffer and Ørnsbjerg and #8197 and Jensen, Kirsten Marie and Bøjesen, Espen Drath and Lock, Nina and Christensen, Mogens and Billinge, Simon J.L. and Brummerstedt and #8197 and Iversen, Bo and Columbia)},
abstractNote = {The formation and evolution of ceria nanoparticles during hydrothermal synthesis was investigated by in-situ total scattering and powder diffraction. The nucleation of pristine crystalline ceria nanoparticles originated from previously unknown cerium dimer complexes. The nanoparticle growth was highly accelerated under supercritical conditions.},
doi = {10.1002/anie.201204747},
journal = {Angew. Chem. Int. Ed.},
issn = {1433-7851},
number = (36) ; 09, 2012,
volume = 51,
place = {United States},
year = {2012},
month = {10}
}