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Title: Magnetic agglomeration method for size control in the synthesis of magnetic nanoparticles

Patent ·
OSTI ID:1021904

A method for controlling the size of chemically synthesized magnetic nanoparticles that employs magnetic interaction between particles to control particle size and does not rely on conventional kinetic control of the reaction to control particle size. The particles are caused to reversibly agglomerate and precipitate from solution; the size at which this occurs can be well controlled to provide a very narrow particle size distribution. The size of particles is controllable by the size of the surfactant employed in the process; controlling the size of the surfactant allows magnetic control of the agglomeration and precipitation processes. Agglomeration is used to effectively stop particle growth to provide a very narrow range of particle sizes.

Research Organization:
Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC04-94AL85000
Assignee:
Sandia Corporation (Albuquerque, NM)
Patent Number(s):
7,972,410
Application Number:
12/364,261
OSTI ID:
1021904
Country of Publication:
United States
Language:
English

References (4)

Synthesis and characterization of surfactant-coated superparamagnetic monodispersed iron oxide nanoparticles journal January 2001
The preparation of magnetic nanoparticles for applications in biomedicine journal June 2003
Giant magnetic susceptibility enhancement in field-structured nanocomposites journal September 2008
Synthesis of highly magnetic iron nanoparticles suitable for field structuring using a β-diketone surfactant journal July 2004

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